Olive oil extraction optimization of ‘Galega Vulgar’ fruits by response surface methodology

New strategies to attain better yields, without compromising olive oil quality, are necessary in olive oil extraction. To improve virgin olive oil yield, several processing aids (talc, calcium carbonate, salt, enzymes) have already been tested. ‘Galega Vulgar’, one of the most abundant Portuguese cultivar for olive oil, usually gives difficult pastes in the malaxation step, which represents a loss of income. The present work aimed to optimize olive oil extraction, at laboratory-scale, from fruits of ‘Galega Vulgar’ cultivar in 2016 (ripening index=4; moisture content=62 % and fat content (FW) =15.8 %) with the addition of processing aids (ProZym® and natural microtalc FC8-AW), using response surface methodologies (RSM). The combined effects of the concentrations of natural microtalc (MT) and of the enzyme preparation (E) on the oil extraction yield (Y), extractability index (IE), the concentration of total phenols (TPH), chlorophyll pigments (CP), as well as on chemical quality criteria parameters of the extracted olive oil, were investigated by RSM. A Central Composite Rotatable Design (CCRD) was followed, as a function of the contents of enzyme preparation (0-0.12 %, v/w) and of natural microtalc (0-0.46 %, w/w). For ‘Galega Vulgar’ olives, the highest extractability was obtained with simultaneous addition of enzymes between 0.02 and 0.08 % (v/w) and of microtalc (0.45-0.50 %, w/w).info:eu-repo/semantics/publishedVersio

Ácidos fenólicos, alcoóis fenológicos, secoiridoides, flavonoides e tocoferóis em azeites virgens.

Comunicação da qual só está disponível o resumo.As características excepcionais do azeite virgem extra devem-se não só ao seu perfil em ácidos gordos mas também à presença de compostos de natureza fenólica que contribuem para o seu valor nutricional. Os estudos mais actuais evidenciam diversos benefícios para a saúde destes compostos, o que levou a União Europeia a aprovar uma alegação nutricional em 2012 sobre “polifenóis do azeite”. Os compostos fenólicos do azeite virgem apresentam também propriedades sensoriais, nomeadamente pela sua contribuição para o sabor amargo. Além disso, contribuem para a estabilidade oxidativa do azeite, pelo que, quando presentes em elevada quantidade, aumentam o seu tempo de vida. A sua avaliação nos azeites pode vir a ter uma importância fundamental para a diferenciação de azeites de elevada qualidade nutricional e sensorial. No presente trabalho, estudaram-se os compostos fenólicos de natureza hidrofílica e lipofílica, em azeites provenientes das cultivares ‘Cobrançosa’ e ‘Galega Vulgar’. Por HPLC-FLD, foram quantificados alfa, beta e gama tocoferóis (fenóis lipofílicos). Nos azeites de ambas as cultivares, os teores de alfa-tocoferol foram sempre superiores a 200 mg kg-1, apresentando os azeites ‘Galega Vulgar’ maiores teores de gama tocoferol. Relativamente ao perfil em compostos fenólicos (hidrofílicos), avaliados por HPLCDAD, foi possível quantificar os teores de hidroxitirosol, tirosol, ácido vanílico, vanilina, ácido o-cumárico, luteolina e apigenina. Identificou-se ainda a presença de 3,4-DHPEA-EDA, p-HPEA-EDA, 3,4-DHPEA-EA e p-HPEA-EA. O composto fenólico maioritário nos azeites foi o 3,4-DHPEA-EDA, representando em alguns azeites mais de 50 % do total de compostos fenólicos. Foram encontrados baixos teores de hidroxitirosol e tirosol, como é expectável em azeites recentemente extraídos. Os azeites ‘Cobrançosa’ apresentaram, em geral, teores mais elevados de flavonóides.info:eu-repo/semantics/publishedVersio

Ensaios experimentais para avaliar a utilização de adjuvantes tecnológicos na extracção de azeite virgem.

Comunicação da qual só está disponível o resumo.No processamento de produtos vegetais, a utilização de adjuvantes tecnológicos para melhorar o rendimento e a qualidade dos alimentos tem uma vasta aplicação industrial. No entanto, no processo de extracção de azeite virgem a utilização de adjuvantes tecnológicos tem ainda uma utilização muito residual. Por sua vez, tal aplicação pode ter uma importância determinante no aumento do rendimento industrial, nomeadamente quando no lagar se apresentam azeitonas com características de pastas de difícil extração. No presente trabalho apresentam-se alguns ensaios realizados no lagar experimental do Laboratório de Tecnologia Alimentar da ESACB, aplicando diferentes sistemas enzimáticos e microtalco natural na operação de termobatedura. Os ensaios realizaram-se com azeitona das cultivares ‘Galega Vulgar’ e ‘Cobrançosa’ colhidas com índices de maturação bem definidos. A extracção de azeite foi efectuada em equipamento constituído por moinho de martelos (3000 rpm), termobatedeira (50 rpm) e centrifugadora (3500 rpm). Apresentam-se ainda resultados de optimização das condições de operação do equipamento utilizando um delineamento Placket-Burman para seleccionar as variáveis significativas, seguido por um delineamento descrito por uma matriz central compósita rotativa (CCRD) em função dessas variáveis. Avaliaram-se o rendimento e o índice de extractabilidade da azeitona; no azeite, avaliaram-se os critérios de qualidade, os fenóis totais e os pigmentos clorofilinos. As respostas relacionadas com o rendimento de extracção podem ser descritas por modelos polinomiais de segundo grau com um elevado ajuste aos dados experimentais (r> 0,8). Em todos os ensaios efectuados com adição de adjuvantes, verificou-se um aumento no rendimento e consequentemente do índice de extractabilidade, relativamente aos ensaios sem qualquer adjuvante de extracção. Os ensaios permitem concluir que a adição de adjuvantes tecnológicos não provocou quaisquer alterações nos teores de compostos fenólicos, nos pigmentos clorofilinos nem nos parâmetros de qualidade dos azeites obtidos.info:eu-repo/semantics/publishedVersio

Influence of olive anthracnose and olive fruit fly on bioactive compounds of Cobrançosa olive oils

Phenolic compounds are the most important bioactive compounds in olives and since 2012 a health claim can be declared for the olive oil if it contains more than 5 mg of hydroxytyrosol (Hyt) and its derivatives per 20 g of oil1. In turn, β-carotene is a precursor of vitamin A that essentially functions in many biological processes including vision. However, the presence of bioactive compounds in olive oils depends on cultivar, agro-ecological conditions, harvest time, post-harvest, extraction technology and storage.This study was funded by the FCT, Portugal (research project PTDC/ASP-PLA/28547/2017).info:eu-repo/semantics/publishedVersio

Avaliação do efeito de campos eléctricos pulsados no rendimento e na presença de compostos bioactivos no azeite virgem.

Avaliação do efeito de campos eléctricos pulsados no rendimento e na presença de compostos bioactivos no azeite virgem.info:eu-repo/semantics/publishedVersio

Development of Cobrançosa "functional olive oils" by co-processing techniques

The aim of this work was to develop "functional olive oils" by co-processing techniques of ‘Cobrançosa’ olives with the addition of Thymus citriodorus (TL, lemon thyme) and T. mastichina L. (TM) from organic agriculture. The “functional olive oils” were prepared by: (i) thyme addition to the olives during the unit operations of crushing or malaxation, and (ii) implementation of ultrasound before the malaxation of the olive paste.This work was funded by national funds through FCT – Fundação para a Ciência e a Tecnologia, I.P., under the project UIDB/04129/2020 of LEAF-Linking Landscape, Environment, Agriculture and Food, Research Unit. (OLIVETHY exploratory project)info:eu-repo/semantics/publishedVersio

Non-Perturbative QCD Treatment of High-Energy Hadron-Hadron Scattering

Total cross-sections and logarithmic slopes of the elastic scattering cross-sections for different hadronic processes are calculated in the framework of the model of the stochastic vacuum. The relevant parameters of this model, a correlation length and the gluon condensate, are determined from scattering data, and found to be in very good agreement with values coming from completely different sources of information. A parameter-free relation is given between total cross-sections and slope parameters, which is shown to be remarkably valid up to the highest energies for which data exist.Comment: 60 pages, Heidelberg preprin

Search for direct production of charginos and neutralinos in events with three leptons and missing transverse momentum in √s = 7 TeV pp collisions with the ATLAS detector

A search for the direct production of charginos and neutralinos in final states with three electrons or muons and missing transverse momentum is presented. The analysis is based on 4.7 fb−1 of proton–proton collision data delivered by the Large Hadron Collider and recorded with the ATLAS detector. Observations are consistent with Standard Model expectations in three signal regions that are either depleted or enriched in Z-boson decays. Upper limits at 95% confidence level are set in R-parity conserving phenomenological minimal supersymmetric models and in simplified models, significantly extending previous results

Jet size dependence of single jet suppression in lead-lead collisions at sqrt(s(NN)) = 2.76 TeV with the ATLAS detector at the LHC

Measurements of inclusive jet suppression in heavy ion collisions at the LHC provide direct sensitivity to the physics of jet quenching. In a sample of lead-lead collisions at sqrt(s) = 2.76 TeV corresponding to an integrated luminosity of approximately 7 inverse microbarns, ATLAS has measured jets with a calorimeter over the pseudorapidity interval |eta| < 2.1 and over the transverse momentum range 38 < pT < 210 GeV. Jets were reconstructed using the anti-kt algorithm with values for the distance parameter that determines the nominal jet radius of R = 0.2, 0.3, 0.4 and 0.5. The centrality dependence of the jet yield is characterized by the jet "central-to-peripheral ratio," Rcp. Jet production is found to be suppressed by approximately a factor of two in the 10% most central collisions relative to peripheral collisions. Rcp varies smoothly with centrality as characterized by the number of participating nucleons. The observed suppression is only weakly dependent on jet radius and transverse momentum. These results provide the first direct measurement of inclusive jet suppression in heavy ion collisions and complement previous measurements of dijet transverse energy imbalance at the LHC.Comment: 15 pages plus author list (30 pages total), 8 figures, 2 tables, submitted to Physics Letters B. All figures including auxiliary figures are available at http://atlas.web.cern.ch/Atlas/GROUPS/PHYSICS/PAPERS/HION-2011-02

Search for a W' boson decaying to a bottom quark and a top quark in pp collisions at sqrt(s) = 7 TeV

Results are presented from a search for a W' boson using a dataset corresponding to 5.0 inverse femtobarns of integrated luminosity collected during 2011 by the CMS experiment at the LHC in pp collisions at sqrt(s)=7 TeV. The W' boson is modeled as a heavy W boson, but different scenarios for the couplings to fermions are considered, involving both left-handed and right-handed chiral projections of the fermions, as well as an arbitrary mixture of the two. The search is performed in the decay channel W' to t b, leading to a final state signature with a single lepton (e, mu), missing transverse energy, and jets, at least one of which is tagged as a b-jet. A W' boson that couples to fermions with the same coupling constant as the W, but to the right-handed rather than left-handed chiral projections, is excluded for masses below 1.85 TeV at the 95% confidence level. For the first time using LHC data, constraints on the W' gauge coupling for a set of left- and right-handed coupling combinations have been placed. These results represent a significant improvement over previously published limits.Comment: Submitted to Physics Letters B. Replaced with version publishe