167 research outputs found
Ionic liquid catalyzed one pot green synthesis of isoxazolone derivatives via multicomponent reaction
459-464A series of 3-methyl-4-((3-aryl-1-phenyl-1H-pyrazol-4-yl)methylene)isoxazol-5(4H)-one derivatives have been efficiently synthesized by environmentally benign, one-pot three component condensation of substituted 1,3-diaryl-1H-pyrazole-4-carboxyaldehyde, β-keto ester and hydroxyl amine hydrochloride in the presence of ionic liquid [HNMP][HSO4] as a catalyst in ethanol. These derivatives have been synthesized by conventional, ultrasound and microwave irradiation methods. The combination of ionic liquid with ultrasound as well as microwave irradiation makes the protocol fascinating and environmentally benign. In addition, it has several benefits such as simple work-up procedure, clean reaction profile, short reaction time and good yields
Study of Properties of Al LM-25/SIC fabricated by using Stir Casting Method and Wear Analysis by RSM
Aluminum MMC’s are widely used in various applications because of their higher mechanical and physical properties when compared with their base Al alloy. This paper focuses on the change in mechanical properties of various Al/SiC composites fabricated by using stir casting method. Effect of SiC reinforcement in different Al alloys on mechanical properties like hardness, tensile strength, wear test, percentage elongation, residual stress measurements are discussed in detail. For this purpose various reinforcement of SiC with 0,4,8 percent weight and different particle sizes are considered along with Al alloys. Variations in process parameters of stir casting are also made and taken into consideration
Variation in the Interactions among soil K+, Ca++, Mg++ and Na+ ions as influenced by the variety and rootstock in grape
A nutritional survey was conducted to study the influence of variety and rootstock on interactionamong K+, Ca++, Mg++and Na+ ions in grape during 2012-14. Soil cation contents did not correlatewith their respective contents in petioles indicating a strong antagonism among them. Quadraticrelationship of soil cations with the absorption (ratio of petiole content to soil content) of otherions revealed that the antagonism among cations was observed in case of soil K+ with Ca++ andNa+ absorption on 110R and Dog Ridge rootstocks, soil Ca+ with K+ and Mg++ and Na+ in Sonakavariety and Na+ in own rooted vines, soil Mg++ with Ca++ and Na+ also in own rooted vines; andNa++ with Ca++ and Mg++ respectively in 2A clone and Dog Ridge. Contrarily, increased absorptionof K+ by soil Ca++ on 110R, Na+ and K+ by soil Mg++ respectively in Sonaka and 110R, and Ca++by soil Na+ on Dog Ridge was also observed. All the soil cations together influenced K+ absorptionmost in Sonaka followed by Mg++ absorption in 2A clone, but Ca++ absorption on Dog Ridgefollowed by K+ on 110R
Modulation of Sn concentration in ZnO nanorod array: intensification on the conductivity and humidity sensing properties
Tin (Sn)-doped zinc oxide (ZnO) nanorod arrays (TZO) were synthesized onto aluminum-doped ZnO-coated glass substrate via a facile sonicated sol–gel immersion method for humidity sensor applications. These nanorod arrays were grown at different Sn concentrations ranging from 0.6 to 3 at.%. X-ray diffraction patterns showed that the deposited TZO arrays exhibited a wurtzite structure. The stress/strain condition of the ZnO film metamorphosed from tensile strain/compressive stress to compressive strain/tensile stress when the Sn concentrations increased. Results indicated that 1 at.% Sn doping of TZO, which has the lowest tensile stress of 0.14 GPa, generated the highest conductivity of 1.31 S cm− 1. In addition, 1 at.% Sn doping of TZO possessed superior sensitivity to a humidity of 3.36. These results revealed that the optimum performance of a humidity-sensing device can be obtained mainly by controlling the amount of extrinsic element in a ZnO film
Seroepidemiology of pandemic influenza A (H1N1) 2009 virus infections in Pune, India
<p>Abstract</p> <p>Background</p> <p>In India, Pune was one of the badly affected cities during the influenza A (H1N1) 2009 pandemic. We undertook serosurveys among the risk groups and general population to determine the extent of pandemic influenza A (H1N1) 2009 virus infections.</p> <p>Methods</p> <p>Pre-pandemic sera from the archives, collected during January 2005 to March 2009, were assayed for the determination of baseline seropositivity. Serosurveys were undertaken among the risk groups such as hospital staff, general practitioners, school children and staff and general population between 15<sup>th </sup>August and 11<sup>th </sup>December 2009. In addition, the PCR-confirmed pandemic influenza A (H1N1) 2009 cases and their household contacts were also investigated. Haemagglutination-inhibition (HI) assays were performed using turkey red blood cells employing standard protocols. A titre of ≥1:40 was considered seropositive.</p> <p>Results</p> <p>Only 2 (0.9%) of the 222 pre-pandemic sera were positive. The test-retest reliability of HI assay in 101 sera was 98% for pandemic H1N1, 93.1% for seasonal H1N1 and 94% for seasonal H3N2. The sera from 48 (73.8%) of 65 PCR-confirmed pandemic H1N1 cases in 2009 were positive. Seropositivity among general practitioners increased from 4.9% in August to 9.4% in November and 15.1% in December. Among hospital staff, seropositivity increased from 2.8% in August to 12% in November. Seropositivity among the schools increased from 2% in August to 10.7% in September. The seropositivity among students (25%) was higher than the school staff in September. In a general population survey in October 2009, seropositivity was higher in children (9.1%) than adults (4.3%). The 15-19 years age group showed the highest seropositivity of 20.3%. Seropositivity of seasonal H3N2 (55.3%) and H1N1 (26.4%) was higher than pandemic H1N1 (5.7%) (n = 2328). In households of 74 PCR-confirmed pandemic H1N1 cases, 25.6% contacts were seropositive. Almost 90% pandemic H1N1 infections were asymptomatic or mild. Considering a titre cut off of 1:10, seropositivity was 1.5-3 times as compared to 1:40.</p> <p>Conclusions</p> <p>Pandemic influenza A (H1N1) 2009 virus infection was widespread in all sections of community. However, infection was significantly higher in school children and general practitioners. Hospital staff had the lowest infections suggesting the efficacy of infection-control measures.</p
Magnetic compensation, field-dependent magnetization reversal, and complex magnetic ordering in Co
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Track A Basic Science
Peer Reviewedhttps://deepblue.lib.umich.edu/bitstream/2027.42/138319/1/jia218438.pd
Minimal information for studies of extracellular vesicles 2018 (MISEV2018):a position statement of the International Society for Extracellular Vesicles and update of the MISEV2014 guidelines
The last decade has seen a sharp increase in the number of scientific publications describing physiological and pathological functions of extracellular vesicles (EVs), a collective term covering various subtypes of cell-released, membranous structures, called exosomes, microvesicles, microparticles, ectosomes, oncosomes, apoptotic bodies, and many other names. However, specific issues arise when working with these entities, whose size and amount often make them difficult to obtain as relatively pure preparations, and to characterize properly. The International Society for Extracellular Vesicles (ISEV) proposed Minimal Information for Studies of Extracellular Vesicles (“MISEV”) guidelines for the field in 2014. We now update these “MISEV2014” guidelines based on evolution of the collective knowledge in the last four years. An important point to consider is that ascribing a specific function to EVs in general, or to subtypes of EVs, requires reporting of specific information beyond mere description of function in a crude, potentially contaminated, and heterogeneous preparation. For example, claims that exosomes are endowed with exquisite and specific activities remain difficult to support experimentally, given our still limited knowledge of their specific molecular machineries of biogenesis and release, as compared with other biophysically similar EVs. The MISEV2018 guidelines include tables and outlines of suggested protocols and steps to follow to document specific EV-associated functional activities. Finally, a checklist is provided with summaries of key points
A Simple and Efficient Synthesis of 2,3-Diarylnaphthofurans Using Sequential Hydroarylation/Heck Oxyarylation
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