Effect of the microstructure generated by repetitive corrugation and straightening (RCS) process on the mechanical properties and stress corrosion cracking of Al-7075 alloy

This study discussed the effect of the heterogeneous microstructure generated through the Repetitive Corrugation and Straightening (RCS) process on the mechanical and stress corrosion cracking behavior of the AA7075. As a result of the RCS process, significant grain refinement was obtained. The average grain size ranged from 126 to 59 µm, for the initial condition and 4 RCS passes, respectively. The yield strength and hardness increased 170% and 15% from the initial pass, remaining almost constant afterward. The evaluation of stress corrosion cracking showed a decrement in the number of cracks of 21.6% and 23.5% between the initial condition and fourth RCS passes. The cracking and pitting corrosion were the dominant mechanisms in the tested samples. The mechanical and corrosion results were also discussed in terms of the microstructural features.Peer ReviewedPostprint (published version

Mechanical, stress corrosion cracking and crystallographic study on flat components processed by two combined severe plastic deformation techniques

Although the current field of application of Al–alloy 7075 (AA7075) is vast, it is still limited due to some drawbacks, especially due to its susceptibility to stress corrosion cracking (SCC). This work aims to evaluate the microstructural, mechanical, and stress corrosion cracking (SCC) behaviors on an AA7075 in flat format deformed by a combination of repetitive corrugation and straightening (RCS) and accumulative roll bonding (ARB) techniques. Four different deformation routes were applied, namely: ARB (A), RCS (R), RCS + ARB (RA) and ARB + RCS (AR). As expected, the efficiency for grain refinement depends on the applied route, in terms of average grain size regarding the initial condition IC): AR > A > RA > R. All conditions resulted in unimodal and widened grain size distributions of micro-, submicro- and nano-metric dimensions. The study of crystallographic orientations showed that route R did not generate any new texture, whereas different preferred orientations were obtained for routes A, RA, and AR. The hardness and three-point bending tests showed an improvement of mechanical strength in the following order: AR > RA > A > R. The cracks per cm2 obtained in the corrosion study indicated that the best SCC resistance was R > A > AR > RA. Based on the above, the best combination of microstructural, mechanical, and SCC properties until one deformation pass was obtained by the single route of the ARB process.Peer ReviewedPostprint (published version

Repetitive corrugation and straightening effect on the microstructure, crystallographic texture and electrochemical behavior for the Al-7075 alloy

Anti-corrosion susceptibility is one of the top criteria for selecting metallic materials for several industrial applications. This work studies the corrosion performance on an Al-7075 alloy obtained by Repetitive Corrugation and Straightening (RCS). This processing method generated a microstructure formed by randomly distributed micro-, submicro-, and nano- metric grain sizes. The samples exhibited a drop in corrosion resistance for a longer duration in the electrolyte and higher deformation. However, the samples processed by RCS showed better electrochemical stability in comparison with the non-deformed condition. The improvement of electrochemical stability could be associated with the particular microstructure generated during the RCS process.Postprint (published version

Repetitive corrugation and straightening effect on the microstructure, crystallographic texture and electrochemical behavior for the Al-7075 alloy

Anti-corrosion susceptibility is one of the top criteria for selecting metallic materials for several industrial applications. This work studies the corrosion performance of an Al-7075 alloy obtained by repetitive corrugation and straightening (RCS). This processing method generated a microstructure formed by randomly distributed micro-, submicro-, and nano- metric grain sizes. The samples exhibited a drop in corrosion resistance for a longer duration in the electrolyte and higher deformation. However, the samples processed by RCS showed better electrochemical stability than the non-deformed condition. The improved electrochemical stability could be associated with the particular microstructure generated during the RCS process

Effect of the microstructure generated by Repetitive Corrugation and Straightening (RCS) process on the mechanical properties and stress corrosion cracking of Al-7075 alloy

This study discussed the effect of the heterogeneous microstructure generated through the Repetitive Corrugation and Straightening (RCS) process on the mechanical and stress corrosion cracking behavior of the AA7075. As a result of the RCS process, significant grain refinement was obtained. The average grain size ranged from 126 to 59 μm, for the initial condition and 4 RCS passes, respectively. The yield strength and hardness increased 170% and 15% from the initial pass, remaining almost constant afterward. The evaluation of stress corrosion cracking showed a decrement in the number of cracks of 21.6% and 23.5% between the initial condition and fourth RCS passes. The cracking and pitting corrosion were the dominant mechanisms in the tested samples. The mechanical and corrosion results were also discussed in terms of the microstructural features

Robust estimation of bacterial cell count from optical density

Optical density (OD) is widely used to estimate the density of cells in liquid culture, but cannot be compared between instruments without a standardized calibration protocol and is challenging to relate to actual cell count. We address this with an interlaboratory study comparing three simple, low-cost, and highly accessible OD calibration protocols across 244 laboratories, applied to eight strains of constitutive GFP-expressing E. coli. Based on our results, we recommend calibrating OD to estimated cell count using serial dilution of silica microspheres, which produces highly precise calibration (95.5% of residuals <1.2-fold), is easily assessed for quality control, also assesses instrument effective linear range, and can be combined with fluorescence calibration to obtain units of Molecules of Equivalent Fluorescein (MEFL) per cell, allowing direct comparison and data fusion with flow cytometry measurements: in our study, fluorescence per cell measurements showed only a 1.07-fold mean difference between plate reader and flow cytometry data

Residual stresses and microstructural study of ECAPed AA2017

The mechanical behavior and microstructural evolution of an AA2017 aluminum alloy processed by ECAP with an equivalent simple shear deformation of ~6 at 200¿°C were studied. Samples were characterized by means of scanning electron microscopy (SEM-EDS- EBSD), image-assisted by focus ion beam (FIB), Vickers microhardness and X-ray diffraction (XRD) techniques. During the deformation process, the Al2Cu precipitates did not get fragmented or re-absorbed in the Al matrix. After the first ECAP pass, at least 50% of grains displayed an ultrafine size. The EBSD analysis showed an increment of the misorientation angle immediately after the first ECAP pass. The macrotexture evolution was explained in terms of the formation of f1: A1¿*, A¿, A¿, A2¿*, f2: C¿, ¿, B¿, A¿, A¿, A1¿* and f3: C¿, B¿, ¿, A¿, A¿, A2¿* fibers. The macro-residual stress measurements of the highly deformed samples showed linear sin2¿ profiles. The micro and macro-residual stresses were compatible with dislocation rearrangement, in which the annihilation and formation were in quasi-equilibrium. It was found that the highest microhardness value (1176¿MPa) and grain refinement (at least 20% of grains showed a size smaller than 100¿µm2) appeared after the first extrusion pass. The decrease in hardness, after the second pass and the residual stress stability, could be associated to a dynamic recovery phenomenon.Peer ReviewedPostprint (published version

Residual stresses and microstructural study of ECAPed AA2017

The mechanical behavior and microstructural evolution of an AA2017 aluminum alloy processed by ECAP with an equivalent simple shear deformation of ~6 at 200¿°C were studied. Samples were characterized by means of scanning electron microscopy (SEM-EDS- EBSD), image-assisted by focus ion beam (FIB), Vickers microhardness and X-ray diffraction (XRD) techniques. During the deformation process, the Al2Cu precipitates did not get fragmented or re-absorbed in the Al matrix. After the first ECAP pass, at least 50% of grains displayed an ultrafine size. The EBSD analysis showed an increment of the misorientation angle immediately after the first ECAP pass. The macrotexture evolution was explained in terms of the formation of f1: A1¿*, A¿, A¿, A2¿*, f2: C¿, ¿, B¿, A¿, A¿, A1¿* and f3: C¿, B¿, ¿, A¿, A¿, A2¿* fibers. The macro-residual stress measurements of the highly deformed samples showed linear sin2¿ profiles. The micro and macro-residual stresses were compatible with dislocation rearrangement, in which the annihilation and formation were in quasi-equilibrium. It was found that the highest microhardness value (1176¿MPa) and grain refinement (at least 20% of grains showed a size smaller than 100¿µm2) appeared after the first extrusion pass. The decrease in hardness, after the second pass and the residual stress stability, could be associated to a dynamic recovery phenomenon.Peer Reviewe

Ciencia Odontológica

Es para los integrantes de la Red de Investigación en Estomatología (RIE) una enorme alegría presentar el primero de una serie de 5 libros sobre casos clínicos, revisiones de la literatura e investigaciones. La RIE está integrada por cuerpos académicos de la Universidad Autónoma del Estado de Hidalgo, Universidad Autónoma del Estado de México, Universidad Autónoma de Campeche y Universidad de Guadalajara