248 research outputs found
Artificial Neural Networks and Concentration Residual Augmented Classical Least Squares for the Simultaneous Determination of Diphenhydramine, Benzonatate, Guaifenesin and Phenylephrine in their Quaternary Mixture
- Publication venue
- 'African Journals Online (AJOL)'
- Publication date
- 13/01/2015
- Field of study
Purpose: To develop two multivariate calibration methods for the simultaneous spectrophotometric determination of a quaternary mixture composed of diphenhydramine HCl, benzonatate, guaifenesin and phenylephrine HCl in Bronchofree âą capsules in the ratio of 2.5 : 10 : 10 : 1, respectively.Methods: Novel artificial neural networks (ANNs) and concentration residual augmented classical least squares (CRACLS) methods were developed for the quantitative determination of the quaternary mixture. For proper analysis, a four-level, four-factor experimental design was established resulting in a training set of 16 mixtures containing different ratios of the four analytes. A validation set consisting of six mixtures was used to validate the prediction ability of the suggested models.Results: ANNs and CRACLS methods were successfully applied for the analysis of raw materials and capsules. For ANNs method, % recovery of diphenhydramine HCl, benzonatate, guaifenesin and phenylephrine HCl in the capsules was 102.21 ± 1.34, 100.30 ± 1.17, 99.31 ± 2.00 and 98.50 ± 1.27, respectively. On the other hand, % recovery of the four analytes by CRACLS was 99.84 ± 2.22, 100.07 ± 0.63, 98.37 ± 1.42 and 97.99 ± 0.96, respectively.Conclusion: The proposed methods can be applied for the quantitative determination of the four components without interference from excipients, thus obviating the need for preliminary extraction of analytes from the pharmaceutical formulation. The ability of the methods to deconvolute the highly overlapped UV spectra of the four componentsâ mixtures using low-cost and easy-to-handle instruments such as UV spectrophotometer is also an advantage.Keywords: Artificial neural networks, Concentration residual augmented classical least squares, Quaternary mixture, Simultaneous determinatio
Global behavior of the solutions of some difference equations
- Author
- aa Kulenovic MRS
- C Cinar
- C Cinar
- C Wang
- C Wang
- Elmetwally M Elabbasy
- Elsayed M Elsayed
- EM Elabbasy
- EM Elabbasy
- EM Elabbasy
- EM Elabbasy
- EM Elabbasy
- EM Elsayed
- EM Elsayed
- EM Elsayed
- EM Elsayed
- EME Zayed
- H El-Metwally
- H El-Metwally
- Hamdy A El-Metwally
- I Yalçinkaya
- I Yalçinkaya
- I Yalçinkaya
- I Yalçinkaya
- M Aloqeili
- MC Mackey
- R Agarwal
- RE Mickens
- RP Agarwal
- RP Agarwal
- VL Kocic
- X Yang
- Publication venue
- 'Springer Science and Business Media LLC'
- Publication date
- Field of study
Reproductive Outcomes Following Ectopic Pregnancy: Register-Based Retrospective Cohort Study
- Author
- A Bernoux
- A Ego
- AA Sobande
- Amanda J Lee
- C Allonier
- David J McLernon
- F Mol
- J Bouyer
- J Bouyer
- J Bouyer
- J Coste
- J Coste
- J Elson
- J Thorburn
- JE Buster
- JL Glock
- JN Lasker
- L Westrom
- M Egger
- M Metwally
- M Wolbers
- MA Hassan
- MC Sowter
- N Dalkalitsis
- N Job-Spira
- N Job-Spira
- Nicholas M Fisk
- S Bunyavejchevin
- S Helmy
- Siladitya Bhattacharya
- Sohinee Bhattacharya
- V Carstairs
- WM Ankum
- Publication venue
- Public Library of Science
- Publication date
- 19/06/2012
- Field of study
Using Scottish national registry data, Sohinee Bhattacharya and colleagues investigate pregnancy outcomes following ectopic pregnancy in comparison to livebirth, miscarriage, or termination in a first pregnancy
Validated spectrophotometric methods for determination of Alendronate sodium in tablets through nucleophilic aromatic substitution reactions
- Author
- A De-Haro-Moreno
- A Raza
- AA Gouda
- C Fernandes
- D Bexheti
- D Kottke
- DD Perrin
- E Ban
- E Kwong
- EA Taha
- EW Tsai
- EW Tsai
- EW Tsai
- FA Van der Horst
- FA Van der Horst
- H Miyano
- I Tarcomnicu
- J Kuljanin
- JC Miller
- JS Esteve-Romero
- K Imai
- KA Connor
- LS Goodman
- LS Zhu
- M Koba
- M Pesez
- M Podolska
- M Podolska
- Manal Eid
- MH Yun
- MI Walash
- MI Walash
- MI Walash
- Mohamed E-S Metwally
- Mohamed I Walash
- N El-Enany
- PD Tzanavaras
- Rania N El-Shaheny
- S Sweetman
- SF Belal
- SK Al Deeb
- SM Anis
- ST Ulu
- SW Su
- WF Kline
- XZ Qin
- YHR Han
- Publication venue
- BioMed Central
- Publication date
- 01/04/2012
- Field of study
<p>Abstract</p> <p>Background</p> <p>Alendronate (ALD) is a member of the bisphosphonate family which is used for the treatment of osteoporosis, bone metastasis, Paget's disease, hypocalcaemia associated with malignancy and other conditions that feature bone fragility. ALD is a non-chromophoric compound so its determination by conventional spectrophotometric methods is not possible. So two derivatization reactions were proposed for determination of ALD through the reaction with 4-chloro-7-nitrobenzo-2-oxa-1,3-diazole (NBD-Cl) and 2,4-dinitrofluorobenzene (DNFB) as chromogenic derivatizing reagents.</p> <p>Results</p> <p>Three simple and sensitive spectrophotometric methods are described for the determination of ALD. Method I is based on the reaction of ALD with NBD-Cl. Method II involved heat-catalyzed derivatization of ALD with DNFB, while, Method III is based on micellar-catalyzed reaction of the studied drug with DNFB at room temperature. The reactions products were measured at 472, 378 and 374 nm, for methods I, II and III, respectively. Beer's law was obeyed over the concentration ranges of 1.0-20.0, 4.0-40.0 and 1.5-30.0 Όg/mL with lower limits of detection of 0.09, 1.06 and 0.06 Όg/mL for Methods I, II and III, respectively. The proposed methods were applied for quantitation of the studied drug in its pure form with mean percentage recoveries of 100.47 ± 1.12, 100.17 ± 1.21 and 99.23 ± 1.26 for Methods I, II and III, respectively. Moreover the proposed methods were successfully applied for determination of ALD in different tablets. Proposals of the reactions pathways have been postulated.</p> <p>Conclusion</p> <p>The proposed spectrophotometric methods provided sensitive, specific and inexpensive analytical procedures for determination of the non-chromophoric drug alendronate either per se or in its tablet dosage forms without interference from common excipients.</p> <p>Graphical abstract</p> <p><display-formula><graphic file="1752-153X-6-25-i3.gif"/></display-formula></p
CCI-779 (Temsirolimus) exhibits increased anti-tumor activity in low EGFR expressing HNSCC cell lines and is effective in cells with acquired resistance to cisplatin or cetuximab
- Author
- A Cassell
- A Chawla
- A Herzog
- A Jimeno
- A Stenzinger
- AA Molinolo
- AC Pickhard
- Albrecht Stenzinger
- DM Parkin
- E Vilar
- F Kamangar
- F Nicolantonio Di
- F Schedel
- F Yang
- FJ Kuppeveld van
- Franziska Niehr
- H Populo
- Ingeborg Tinhofer
- J Gilbert
- JA Bonner
- JD Coppock
- JE Bauman
- MA Gadhikar
- MA Metwally
- MG Fury
- N Agrawal
- N Aissat
- N Stransky
- O Ekshyyan
- P Bossi
- PC Ng
- Q Li
- R Krumbach
- S Oiso
- S Satheesha
- SA Forbes
- T Lu
- TK Hoffmann
- V DâAmato
- V Endris
- V Ramensky
- VKU GrĂŒnwald
- Volker Budach
- VW Lui
- Wilko Weichert
- ZJ Sun
- Publication venue
- 'Springer Science and Business Media LLC'
- Publication date
- Field of study
Laparoscopy in management of appendicitis in high-, middle-, and low-income countries: a multicenter, prospective, cohort study.
- Author
- Abantanga F
- Abbas M
- Abbo O
- Abd El Galeel A
- Abd El Hameed OS
- Abd El Hamid N
- Abd El Salam Y
- Abd El Slam M
- Abd El-Salam F
- Abd Elrasoul Y
- Abd-Elrasoul Y
- Abdallah E
- Abdel-Wahab NYE
- AbdelFattah I
- Abdelgelil A
- Abdelghany S
- Abdelkader M
- Abdelkareem A
- Abdelraheim M
- Abdelshafy M
- Abdulgawad M
- Abdullah AAN
- Abdullah NAN
- Abebe NS
- Abebe NS
- Aber A
- Abington E
- Aboarab A
- Aboraya M
- Aboraya M
- Abouelnasr A
- Abouzahra A
- Abozaid M
- Abozeid K
- Abozyed MAF
- Abudeeb H
- Abuseif M
- Acharya P
- Adams R
- Adebanjo A
- Adekoya A
- Adel A
- Adel A
- Ademuyiwa A
- Ademuyiwa AO
- Adeniran J
- Adeniyi A
- Adesanya O
- Adesina A
- Adesuyi A
- Adeyeye A
- Adham W
- Afandy A
- Afifi AM
- Afzal M
- Agalianos C
- Agarwal A
- Agius M
- Aguilar-Jimenez J
- Aguilera M
- Aguilera O
- Ahlqvist S
- Ahmed A
- Ahmed EA
- Ahmed H
- Ahmed SM
- Aigrain Y
- Ajao AE
- Akeel N
- Akhtar M
- Al Awwad S
- Al-Aarag AA-R
- Al-Azraqi IAA
- Al-Faifi JJ
- Al-Hameedi HII
- Al-Hasani RKMJ
- Al-Mallah A
- Al-Mousa M
- Al-Nahrawi S
- Al-Obaedi O
- Al-shammari A
- Alahmady O
- Alakaloko F
- Alamoudi U
- Albeladi B
- Aldalaq A
- Aldhafeeri S
- Aledrisy M
- Alfarsi MA
- Alghamdi B
- Alghamdi M
- Algohary O
- Alhabli I
- Alhendy M
- Ali A
- Ali A
- Ali H
- Ali SS
- Alimi Q
- Aljiffry M
- Aljohani E
- Aljohani S
- Alkammash A
- Alkhabbaz D
- Alkhouri M
- Allam M
- Allegri A
- Allen JLY
- Allott R
- Almallah A
- Almoflihi A
- Almuallem S
- Almy J
- Alnawam E
- Alnuqaydan SA
- Alomar IN
- Alqahtani E
- Alrahawy M
- Alrajraji M
- Alrifaie A
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- Alsaggaf M
- Alsaggaf MU
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- Altoe F
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- Alvarez Barreda LM
- Alwafai MG
- Aly AK
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- Alzahrani M
- Alzayat T
- Amandito R
- Ambrozeviciute V
- Ameen M
- Amer MA
- Amin J
- Ammar M
- Ammar MS
- Amreia M
- Anandkumar D
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- Anwar AW
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- Arachchi PP
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- Aranzabal Durand SY
- Araujo R
- Ardley R
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- Arevalo Azmitia JR
- Arias Pacheco RD
- Arman S
- Arnaud AP
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- Publication venue
- 'Springer Science and Business Media LLC'
- Publication date
- 01/01/2018
- Field of study
BACKGROUND: Appendicitis is the most common abdominal surgical emergency worldwide. Differences between high- and low-income settings in the availability of laparoscopic appendectomy, alternative management choices, and outcomes are poorly described. The aim was to identify variation in surgical management and outcomes of appendicitis within low-, middle-, and high-Human Development Index (HDI) countries worldwide. METHODS: This is a multicenter, international prospective cohort study. Consecutive sampling of patients undergoing emergency appendectomy over 6Â months was conducted. Follow-up lasted 30Â days. RESULTS: 4546 patients from 52 countries underwent appendectomy (2499 high-, 1540 middle-, and 507 low-HDI groups). Surgical site infection (SSI) rates were higher in low-HDI (OR 2.57, 95% CI 1.33-4.99, pâ=â0.005) but not middle-HDI countries (OR 1.38, 95% CI 0.76-2.52, pâ=â0.291), compared with high-HDI countries after adjustment. A laparoscopic approach was common in high-HDI countries (1693/2499, 67.7%), but infrequent in low-HDI (41/507, 8.1%) and middle-HDI (132/1540, 8.6%) groups. After accounting for case-mix, laparoscopy was still associated with fewer overall complications (OR 0.55, 95% CI 0.42-0.71, pâ<â0.001) and SSIs (OR 0.22, 95% CI 0.14-0.33, pâ<â0.001). In propensity-score matched groups within low-/middle-HDI countries, laparoscopy was still associated with fewer overall complications (OR 0.23 95% CI 0.11-0.44) and SSI (OR 0.21 95% CI 0.09-0.45). CONCLUSION: A laparoscopic approach is associated with better outcomes and availability appears to differ by country HDI. Despite the profound clinical, operational, and financial barriers to its widespread introduction, laparoscopy could significantly improve outcomes for patients in low-resource environments. TRIAL REGISTRATION: NCT02179112
Pooled analysis of WHO Surgical Safety Checklist use and mortality after emergency laparotomy
- Author
- Aahlin EK
- Aamer A
- Aaniana K
- Ababneh A
- Abaliksta T
- Abantanga F
- Abantanga F
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- Abd El Hameed OS
- Abd El Hamid N
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- Abd El Slam M
- Abd El-Salam F
- Abd Elrasoul Y
- Abd-Elmawla M
- Abd-Elrasoul Y
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- Abdel-Hameed N
- Abdel-Kader SM
- Abdel-Wahab NYE
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- Abdelhamed R
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- Aranzabal Durand SY
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- El Shoura Y
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- Elhadad A
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- Elhalawany E
- Elhamouly S
- Elhelbawy MS
- Elhendawy A
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- Elhoseny G
- Elhusseiny AAE
- Elizabeth Lopez C
- Elkadsh I
- Elkady F
- Elkelany A
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- Elkhadrawi M
- Elkhalek EA
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- Elsherbiny AS
- Elsherif FA
- Elshobary M
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- Elsorogy DEAA
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- Elwy E
- Elzahed N
- Elzayat I
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- Elzowawi F
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- Eng C
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- Escalante Salas MDC
- Espin-Basany E
- Espinoza F
- Essam A
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- Farouk SAM
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- Farrugia A
- Farrugia A
- Faruq A
- Fathy AM
- Fattah AA
- Fatuga A
- Faturoti O
- Faturoti O
- Faure A
- Fautz T
- Favero A
- Fawzy A
- Feidantsis T
- Felipe CO
- Fergany A
- Fergusson SJ
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- Kalles V
- Kalles V
- Kalles V
- Kamarajah SK
- Kamarulzamil SNA
- Kamil R
- Kamya S
- Kanani A
- Kandil AM
- Kandil H
- Kang MK
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- Karabacak U
- Karabelias G
- Karabulut K
- Karahan SR
- Karakahya M
- Karandikar S
- Karandikar S
- Kariem N
- Karim A
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- Karjiker P
- Karkeet M
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- Karlo R
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- Karousos D
- Karumnas P
- Kaselis N
- Kaselis N
- Kasem E
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- Kasputyte S
- Kaul A
- Kazanavicius D
- Kedar A
- Kefalidi E
- Keke KR
- Kelany M
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- Kennedy ED
- Kennedy M
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- Kesinger M
- Khafagy T
- Khairy H
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- Khajanchi M
- Khaled H
- Khalifah E
- Khalili M
- Khalique A
- Khallaf S
- Khamajeet A
- Khan A
- Khan K
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- Khan R
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- Khan ZA
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- Khatri C
- Khatri C
- Khattab K
- Khedr AE-RH
- Khoja A
- Khoja A
- Khokha D
- Khokha V
- Khosla S
- Khouri Ferreira SA
- Khreishi R
- Khreishi R
- Khulu LB
- Khyrallh A
- Kiasat A
- Kidd T
- Kielty P
- Kim MY-H
- Kim S-H
- Kim SB
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- Kinandu K
- King R
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- Kiran RP
- Kirby A
- Kirishnan A
- Kirupagaran A
- Kiudelis M
- Kjellin A
- Klappenbach R
- Knight S
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- Koay KL
- Kobal BB
- Koh C
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- Kojo ATT
- Kojo ATT
- Kojo ATT
- Kolosov A
- Komolafe O
- Kondrotas P
- Kong C
- Kong SN
- Kong V
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- Konstantina K
- Kontos M
- Kordorwu HEK
- Korkolis D
- Kosai NR
- Kosai NR
- Kose E
- Koskenvuo L
- Kostov E
- Kotb AHE-B
- Kotecha D
- Koto MZ
- Kotobi H
- Koumpa F
- Kouraklis G
- Kourdouli A
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- Kretzmann H
- Krishna K
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- Kyriazanos I
- Kyrou G
- Kyziridis D
- L'Heveder A
- La Brocca A
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- Labib P
- Ladukas A
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- Lakhani SM
- Lakshmi HN
- Lam FY
- Lam JCY
- Lam WH
- Lamanna GL
- Lanau MIV
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- Landolfo G
- Landolfo G
- Lap G
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- Lasek A
- Lasheen A
- Lasheen KT
- Latif A
- Laugzemys E
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- Laurie K
- Lauzikas G
- Law JH
- Lawal A
- Lawal AO
- Lawal T
- Lawal TA
- Lawani I
- Lawther R
- Lazzari G
- Lazzari V
- Lazzarini Cury AD
- Le VTH
- Leal A
- Leal M
- Leanne Almanon C
- Lecompte J-F
- Lee C
- Lee EX
- Lee F
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- Leppaniemi A
- Leppaniemi A
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- Leusink A
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- Lilford R
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- Lim G
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- Limaye N
- Limoges B
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- lo Conte A
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- Macchitella Y
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- Macfarlane A
- Machaca M
- Machain Vega GM
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- Maciejec L
- Madiba T
- Madkor MH
- Madrid Barrientos LA
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- Manipal CE
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- Mirza A
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- Mistry A
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- Mohamed B
- Mohamed F
- Mohamed I
- Mohamed M
- Mohamed MA
- Mohamed MAEH
- Mohamed MM
- Mohamed O
- Mohamed SR
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- Mohammad A
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- Montes I
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- Montoya Botero JA
- Montrimaite M
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- Mosalum O
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- Nwabuoku E
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- Samaraweera DI
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- Publication venue
- Publication date
- 15/10/2018
- Field of study
Background The World Health Organization (WHO) Surgical Safety Checklist has fostered safe practice for 10 years, yet its place in emergency surgery has not been assessed on a global scale. The aim of this study was to evaluate reported checklist use in emergency settings and examine the relationship with perioperative mortality in patients who had emergency laparotomy. Methods In two multinational cohort studies, adults undergoing emergency laparotomy were compared with those having elective gastrointestinal surgery. Relationships between reported checklist use and mortality were determined using multivariable logistic regression and bootstrapped simulation. Results Of 12 296 patients included from 76 countries, 4843 underwent emergency laparotomy. After adjusting for patient and disease factors, checklist use before emergency laparotomy was more common in countries with a high Human Development Index (HDI) (2455 of 2741, 89.6 per cent) compared with that in countries with a middle (753 of 1242, 60.6 per cent; odds ratio (OR) 0.17, 95 per cent c.i. 0.14 to 0.21, P <0001) or low (363 of 860, 422 per cent; OR 008, 007 to 010, P <0.001) HDI. Checklist use was less common in elective surgery than for emergency laparotomy in high-HDI countries (risk difference -94 (95 per cent c.i. -11.9 to -6.9) per cent; P <0001), but the relationship was reversed in low-HDI countries (+121 (+7.0 to +173) per cent; P <0001). In multivariable models, checklist use was associated with a lower 30-day perioperative mortality (OR 0.60, 0.50 to 073; P <0.001). The greatest absolute benefit was seen for emergency surgery in low- and middle-HDI countries. Conclusion Checklist use in emergency laparotomy was associated with a significantly lower perioperative mortality rate. Checklist use in low-HDI countries was half that in high-HDI countries.Peer reviewe
Search for strongly interacting massive particles generating trackless jets in proton-proton collisions at s = 13 TeV
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- Ăzçelik Ă
- Ć irokĂœ J
- Publication venue
- 'Springer Science and Business Media LLC'
- Publication date
- 01/01/2022
- Field of study
A search for dark matter in the form of strongly interacting massive particles (SIMPs) using the CMS detector at the LHC is presented. The SIMPs would be produced in pairs that manifest themselves as pairs of jets without tracks. The energy fraction of jets carried by charged particles is used as a key discriminator to suppress efficiently the large multijet background, and the remaining background is estimated directly from data. The search is performed using proton-proton collision data corresponding to an integrated luminosity of 16.1 fb - 1 , collected with the CMS detector in 2016. No significant excess of events is observed above the expected background. For the simplified dark matter model under consideration, SIMPs with masses up to 100 GeV are excluded and further sensitivity is explored towards higher masses
Measurement of the inclusive and differential Higgs boson production cross sections in the decay mode to a pair of Ï Leptons in pp collisions at sqrt[s]=13ââTeV
- Author
- Aarrestad TK
- Aarup Petersen H
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- Ălvarez FernĂĄndez A
- Ăzçelik Ă
- Publication venue
- 'American Physical Society (APS)'
- Publication date
- 01/01/2022
- Field of study
Measurements of the inclusive and differential fiducial cross sections of the Higgs boson are presented, using the Ï lepton decay channel. The differential cross sections are measured as functions of the Higgs boson transverse momentum, jet multiplicity, and transverse momentum of the leading jet in the event, if any. The analysis is performed using proton-proton collision data collected with the CMS detector at the LHC at a center-of-mass energy of 13ââTeV and corresponding to an integrated luminosity of 138ââfb^{-1}. These are the first differential measurements of the Higgs boson cross section in the final state of two Ï leptons. In final states with a large jet multiplicity or with a Lorentz-boosted Higgs boson, these measurements constitute a significant improvement over measurements performed in other final states
Search for decays of the 125 GeV Higgs boson into a Z boson and a Ï or Ï meson
- Author
- Aarrestad T. K.
- Aarup Petersen H.
- Abbaneo D.
- Abbiendi G.
- Abbrescia M.
- Abdullin S.
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- Ăzçelik Ă.
- Publication venue
- Scuola Internazionale Superiore di Studi Avanzati
- Publication date
- 01/11/2020
- Field of study
Decays of the 125 GeV Higgs boson into a Z boson and a Ï^0(770) or Ï(1020) meson are searched for using proton-proton collision data collected by the CMS experiment at the LHC at âs = 13 TeV. The analysed data set corresponds to an integrated luminosity of 137 fbâ»Âč. Events are selected in which the Z boson decays into a pair of electrons or a pair of muons, and the Ï and Ï mesons decay into pairs of pions and kaons, respectively. No significant excess above the background model is observed. As different polarization states are possible for the decay products of the Z boson and Ï or Ï mesons, affecting the signal acceptance, scenarios in which the decays are longitudinally or transversely polarized are considered. Upper limits at the 95% confidence level on the Higgs boson branching fractions into ZÏ and ZÏ are determined to be 1.04â1.31% and 0.31â0.40%, respectively, where the ranges reflect the considered polarization scenarios; these values are 740â940 and 730â950 times larger than the respective standard model expectations. These results constitute the first experimental limits on the two decay channels
- âŠ