5 research outputs found
Analysis of the carbide precipitation and microstructural evolution in HCCI as a function of the heating rate and destabilization temperature
Microstructural modifcation of high chromium cast irons (HCCI) through the precipitation of
secondary carbides (SC) during destabilization treatments is essential for improving their tribological
response. However, there is not a clear consensus about the frst stages of the SC precipitation
and how both the heating rate (HR) and destabilization temperature can afect the nucleation and
growth of SC. The present work shows the microstructural evolution, with a special focus on the SC
precipitation, in a HCCI (26 wt% Cr) during heating up to 800, 900, and 980 °C. It was seen that the HR
is the most dominant factor infuencing the SC precipitation as well as the matrix transformation in
the studied experimental conditions. Finally, this work reports for frst time in a systematic manner,
the precipitation of SC during heating of the HCCI, providing a further understanding on the early
stages of the SC precipitation and the associated microstructural modifcations
A Detailed Analysis of the Microstructural Changes in the Vicinity of a Crack-Initiating Defect in Additively Manufactured AISI 316L
The fatigue life of metals manufactured via laser-based powder bed fusion (L-PBF) highly
depends on process-induced defects. In this context, not only the size and geometry of the defect, but
also the properties and the microstructure of the surrounding material volume must be considered.
In the presented work, the microstructural changes in the vicinity of a crack-initiating defect in a
fatigue specimen produced via L-PBF and made of AISI 316L were analyzed in detail. Xenon plasma
focused ion beam (Xe-FIB) technique, scanning electron microscopy (SEM), and electron backscatter
diffraction (EBSD) were used to investigate the phase distribution, local misorientations, and grain
structure, including the crystallographic orientations. These analyses revealed a fine grain structure
in the vicinity of the defect, which is arranged in accordance with the melt pool geometry. Besides
pronounced cyclic plastic deformation, a deformation-induced transformation of the initial austenitic
phase into α’-martensite was observed. The plastic deformation as well as the phase transformation
were more pronounced near the border between the defect and the surrounding material volume.
However, the extent of the plastic deformation and the deformation-induced phase transformation
varies locally in this border region. Although a beneficial effect of certain grain orientations on the
phase transformation and plastic deformability was observed, the microstructural changes found
cannot solely be explained by the respective crystallographic orientation. These changes are assumed
to further depend on the inhomogeneous distribution of the multiaxial stresses beneath the defect as
well as the grain morphology
A Detailed Analysis of the Microstructural Changes in the Vicinity of a Crack-Initiating Defect in Additively Manufactured AISI 316L
The fatigue life of metals manufactured via laser-based powder bed fusion (L-PBF) highly depends on process-induced defects. In this context, not only the size and geometry of the defect, but also the properties and the microstructure of the surrounding material volume must be considered. In the presented work, the microstructural changes in the vicinity of a crack-initiating defect in a fatigue specimen produced via L-PBF and made of AISI 316L were analyzed in detail. Xenon plasma focused ion beam (Xe-FIB) technique, scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD) were used to investigate the phase distribution, local misorientations, and grain structure, including the crystallographic orientations. These analyses revealed a fine grain structure in the vicinity of the defect, which is arranged in accordance with the melt pool geometry. Besides pronounced cyclic plastic deformation, a deformation-induced transformation of the initial austenitic phase into α’-martensite was observed. The plastic deformation as well as the phase transformation were more pronounced near the border between the defect and the surrounding material volume. However, the extent of the plastic deformation and the deformation-induced phase transformation varies locally in this border region. Although a beneficial effect of certain grain orientations on the phase transformation and plastic deformability was observed, the microstructural changes found cannot solely be explained by the respective crystallographic orientation. These changes are assumed to further depend on the inhomogeneous distribution of the multiaxial stresses beneath the defect as well as the grain morphology