225 research outputs found
LZS/Al2O3 nanostructured composites obtained by colloidal processing and spark plasma sintering
[EN] Li2O-SiO2-ZrO2 (LZS) glass-ceramics have high mechanical strength, hardness, resistance to abrasion and chemical attack, but also a high coefficient of thermal expansion (CTE), which can be reduced adding alumina nanoparticles. The conventional glass-ceramic production is relatively complex and energy consuming, since it requires the melting of the raw materials to form a glass frit and a two-step milling process to obtain particle sizes adequate for compaction. This study describes the preparation of LZS glass-ceramics through a colloidal processing approach from mixtures of SiO2 and ZrO2 nanopowders and a Li precursor (lithium acetate obtained by reaction of the carbonate with acetic acid). Concentrated suspensions were freeze-dried to obtain homogeneous mixtures of powders that were pressed (100 MPa) and sintered conventionally and by spark plasma sintering. The effect of the alumina nanoparticles additions on suspensions rheology, sintering behavior and properties such as thermal expansion, thermal conductivity, hardness and Young's modulus were evaluated. (C) 2017 Elsevier Ltd. All rights reserved.This work has been supported by Ministerio de Economia y Competitividad (MINECO) and FEDER Funds under grant No MAT2016-67586-C3-R. Authors greatly acknowledge the financial Support of CAPES in the frame of the International Cooperation Program Science without Borders for Special Visiting Researcher PVE (MEC/MCTI/CAPES/CNPQ/FAPs/No 71/2013), Project no. A011/2013. A. Borrell acknowledges the MINECO for her Juan de la Cierva-Incorporacion contract (IJCI-2014-19839).Arcaro, S.; Novaes De Oliveira, A.; Gutierrez-Gonzalez, C.; Salvador Moya, MD.; Borrell TomĂĄs, MA.; Moreno, R. (2017). LZS/Al2O3 nanostructured composites obtained by colloidal processing and spark plasma sintering. Journal of the European Ceramic Society. 37(16):5139-5148. https://doi.org/10.1016/j.jeurceramsoc.2017.03.023S51395148371
Gel casting of silicon nitride foams using biopolymers as gelling agents
Abstract Si3N4-based foams were prepared by the gel casting route using egg-albumen, agar-agar, or methylcellulose as biopolymer gelling agents. Microstructural, permeability, and mechanical properties of the foams were determined. The use of a variety of environmentally friendly gelling agents produced Si3N4 foams with a wide range of porosity (79â89%), mean cell size (199â852 ÎŒm), and mean window size (51â152 ÎŒm). The pressureless sintering method was successfully applied and resulted in Si3N4 foams with compressive strengths ranging from 1.6 to 9.4 MPa when treated at 1600 °C and up to 33.5 MPa when sintered at 1700 °C, due to the formation of the ÎČâSi3N4 phase. Darcian (k1) and non-Darcian (k2) permeability coefficients were 4.41 Ă 10â12 to 1.61 Ă 10â10 m2 and 5.07 Ă 10â7 to 1.02 Ă 10â6 m, respectively, allowing the produced Si3N4 foams to be used in a wide variety of fluid flow and filtering applications
Properties of LZS/nanoAl2O3 glass-ceramic composites
[EN] The LZS glass-ceramic (19.58 Li2O center dot 11.10ZrO(2)center dot 69.32SiO(2)) have a high coefficient thermal expansion (CTE) which can be a limitation in some applications. The addition of alumina in a LZS glass-ceramic matrix is able to reduce the CTE significantly. This happens because of the alumina affinity with respect to lithium silicates to form beta-spodumene (LiAlSi2O6), a crystalline phase having a CTE nearly zero (0.9 x 10(-6) degrees C-1).In this work, (1-5 vol%) Al2O3 nanoparticles (13 nm) were added to a LZS (3.5 mu m) glass-ceramic matrix to prepare composites with the main goal of evaluation the influence of Al2O3 on their mechanical, thermal and electrical properties. Each composition was wet homogenized and then dried at 110 degrees C for 48 h for disaggregation. The composites, sintered at 900 degrees C for 30 min, with relative densities between 92% and 98%, showed zircon and beta-spodumene as main crystalline phases. The incorporation of increasing additions of nanosized alumina progressively decreases the final density. This makes the properties to slightly decrease, also. The Young's modulus significantly decreases from 111 to 78 GPa of hardness due to the exponential variation with porosity, but the changes of toughness and hardness are much lower. The electrical conductivity was maintained within +/- 10-7 S. cm(-1), and the dielectric constant ranged from 5 to 6 for all compositions. Thermal conductivity ranged around 4.2 to 3.5 W/mK. (C) 2017 Elsevier B.V. All rights reserved.This work has been supported by CAPES in the frame of the International Cooperation Program Science without Borders for Special Visiting Researcher PVE (MEC/MCTI/CAPES/CNPq/FAPs/ No 71/2013), Project No A011/2013 (Brazil) and CNPq (National Council for Scientific and Technological Development, Brazil). This work has been also supported by Ministerio de Economia y Cornpetitividad and FEDER Funds under grant No MAT2016-67586-C3-R and grant ENE2013-49111-C2-1-R. A. Borrell acknowledges the MINECO for her Juan de la Cierva-Incorporacion contract (IJCI-2014-19839).Arcaro, S.; Moreno, B.; Chinarro, E.; Salvador Moya, MD.; Borrell TomĂĄs, MA.; Nieto, M.; Moreno, R.... (2017). Properties of LZS/nanoAl2O3 glass-ceramic composites. Journal of Alloys and Compounds. 710:567-574. https://doi.org/10.1016/j.jallcom.2017.03.299S56757471
Search for Higgs bosons decaying to tautau pairs in ppbar collisions at sqrt(s) = 1.96 TeV
We present a search for the production of neutral Higgs bosons decaying into
tautau pairs in ppbar collisions at a center-of-mass energy of 1.96 TeV. The
data, corresponding to an integrated luminosity of 5.4 fb-1, were collected by
the D0 experiment at the Fermilab Tevatron Collider. We set upper limits at the
95% C.L. on the product of production cross section and branching ratio for a
scalar resonance decaying into tautau pairs, and we then interpret these limits
as limits on the production of Higgs bosons in the minimal supersymmetric
standard model (MSSM) and as constraints in the MSSM parameter space.Comment: 7 pages, 5 figures, submitted to PL
Measurement of three-jet differential cross sections d sigma-3jet / d M-3jet in p anti-p collisions at sqrt(s)=1.96 TeV
We present the first measurement of the inclusive three-jet differential
cross section as a function of the invariant mass of the three jets with the
largest transverse momenta in an event in p anti-p collisions at sqrt(s) = 1.96
TeV. The measurement is made in different rapidity regions and for different
jet transverse momentum requirements and is based on a data set corresponding
to an integrated luminosity of 0.7 fb^{-1} collected with the D0 detector at
the Fermilab Tevatron Collider. The results are used to test the three-jet
matrix elements in perturbative QCD calculations at next-to-leading order in
the strong coupling constant. The data allow discrimination between
parametrizations of the parton distribution functions of the proton.Comment: 10 pages, 4 figures, 2 tables, submitted to Phys. Lett. B, corrected
chi2 values for NNPD
Search for pair production of the scalar top quark in muon+tau final states
We present a search for the pair production of scalar top quarks
(), the lightest supersymmetric partners of the top quarks, in
collisions at a center-of-mass energy of 1.96 TeV, using data
corresponding to an integrated luminosity of {7.3 } collected with the
\dzero experiment at the Fermilab Tevatron Collider. Each scalar top quark is
assumed to decay into a quark, a charged lepton, and a scalar neutrino
(). We investigate final states arising from and
. With no significant excess of events observed above the
background expected from the standard model, we set exclusion limits on this
production process in the (,) plane.Comment: Submitted to Phys. Lett.
Measurements of inclusive W+jets production rates as a function of jet transverse momentum in ppbar collisions at sqrt{s}=1.96 TeV
This Letter describes measurements of inclusive W (--> e nu) + n jet cross
sections (n = 1-4), presented as total inclusive cross sections and
differentially in the nth jet transverse momentum. The measurements are made
using data corresponding to an integrated luminosity of 4.2 fb-1 collected by
the D0 detector at the Fermilab Tevatron Collider, and achieve considerably
smaller uncertainties on W +jets production cross sections than previous
measurements. The measurements are compared to next-to-leading order
perturbative QCD (pQCD) calculations in the n =1-3 jet multiplicity bins and to
leading order pQCD calculations in the 4-jet bin. The measurements are
generally in agreement with pQCD predictions, although certain regions of phase
space are identified where the calculations could be improved
Measurement of spin correlation in ttbar production using dilepton final states
We measure the correlation between the spin of the top quark and the spin of
the anti-top quark in (ttbar -> W+ W- b bbar -> l+ nu b l- nubar bbar) final
states produced in ppbar collisions at a center of mass energy sqrt(s)=1.96
TeV, where l is an electron or muon. The data correspond to an integrated
luminosity of 5.4 fb-1 and were collected with the D0 detector at the Fermilab
Tevatron collider. The correlation is extracted from the angles of the two
leptons in the t and tbar rest frames, yielding a correlation strength C=
0.10^{+0.45}_{-0.45}, in agreement with the NLO QCD prediction within two
standard deviations, but also in agreement with the no correlation hypothesis.Comment: 10 pages, 3 figures, submitted to PL
Measurement of the ttbar production cross section using dilepton events in ppbar collisions
We present a measurement of the ttbar production cross section sigma(ttbar)
in ppbar collisions at sqrt{s} = 1.96 TeV using 5.4 fb-1 of integrated
luminosity collected with the D0 detector. We consider final states with at
least two jets and two leptons (ee, emu, mumu), and events with one jet for the
the emu final state as well. The measured cross section is sigma(ttbar)= 7.36
+0.90-0.79 (stat + syst) pb. This result combined with the cross section
measurement in the lepton + jets final state yields sigma(ttbar)=7.56
+0.63-0.56 (stat + syst) pb, which agrees with the standard model expectation.
The relative precision of 8% of this measurement is comparable to the latest
theoretical calculations.Comment: 9 pages, published in Phys. Lett.
Search for single top quarks in the tau+jets channel using 4.8 fb of collision data
We present the first direct search for single top quark production using tau
leptons. The search is based on 4.8 fb of integrated luminosity
collected in collisions at =1.96 TeV with the D0 detector
at the Fermilab Tevatron Collider. We select events with a final state
including an isolated tau lepton, missing transverse energy, two or three jets,
one or two of them tagged. We use a multivariate technique to discriminate
signal from background. The number of events observed in data in this final
state is consistent with the signal plus background expectation. We set in the
tau+jets channel an upper limit on the single top quark cross section of
\TauLimObs pb at the 95% C.L. This measurement allows a gain of 4% in expected
sensitivity for the observation of single top production when combining it with
electron+jets and muon+jets channels already published by the D0 collaboration
with 2.3 fb of data. We measure a combined cross section of
\SuperCombineXSall pb, which is the most precise measurement to date.Comment: 12 pages, 5 figure
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