124 research outputs found

    Magnetic remanent states in antiferromagnetically coupled multilayers

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    In antiferromagnetically coupled multilayers with perpendicular anisotropy unusual multidomain textures can be stabilized due to a close competition between long-range demagnetization fields and short-range interlayer exchange coupling. In particular, the formation and evolution of specific topologically stable planar defects within the antiferromagnetic ground state, i.e. wall-like structures with a ferromagnetic configuration extended over a finite width, explain configurational hysteresis phenomena recently observed in [Co/Pt(Pd)]/Ru and [Co/Pt]/NiO multilayers. Within a phenomenological theory, we have analytically derived the equilibrium sizes of these "ferroband" defects as functions of the antiferromagnetic exchange, a bias magnetic field, and geometrical parameters of the multilayers. In the magnetic phase diagram, the existence region of the ferrobands mediates between the regions of patterns with sharp antiferromagnetic domain walls and regular arrays of ferromagnetic stripes. The theoretical results are supported by magnetic force microscopy images of the remanent states observed in [Co/Pt]/Ru.Comment: Paper submitted by the Joint European Magnetics Symposia 2008, Dublin (4 pages, 3 figures

    Synteza i badanie właściwości fizykochemicznych związków makrocyklicznych zawierających atomy siarki oraz tlenu lub azotu

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    Macrocyclic compounds from the family of crown ethers are subject of an enduring interest due to their interesting properties and numerous applications. The most characteristic feature of chemical compounds belonging to this class is their ability to form complexes with metal cations from I and II group, and the dependence of stability of these complexes on the matching of a cation diameter and the size of the cavity in a macrocyclic ring. The changing of part or all oxygen atoms in the crown ether ring by other heteroatoms (for example sulfur or nitrogen atoms) allows the obtaining of macrocyclic compounds with differentiated complexing properties. During the research, a number of new macrocyclic compounds containing sulfur and oxygen or nitrogen atoms were synthesized. Each of the synthesized macrocyclic compounds also possesses an aromatic moiety in its structure. Complexes of the part of obtained macrocycles with chosen transition metal cations were also synthesized. Obtained compounds were characterized by means of instrumental analytical methods such as NMR, FTIR, UV-Vis spectrometry. Single crystals obtained during research were used to determine crystal structures of large part of obtained compounds by means of the XRD method. Conducted research aims in broadening of fundamental knowledge in the field of described group of macrocyclic compounds, with emphasis on their crystal structures and crystal structures of their complexes with transition metal cations

    Crystal structure of sparteinium tetrachlorocuprate monohydrate‑packing polymorph

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    A new polymorph of sparteinium tetrachlorocuprate monohydrate [(C15H28N2)CuCl4·H2O] is reported. The structure of the analyzed crystal was solved in the orthorhombic P212121 space group with the following unit cell parameters at 295 K: a = 9.7722(2) Å; b = 13.4582(3) Å; c = 15.1582(3) Å. The various types of hydrogen bonding interactions existing in the crystal structure of this salt were compared with the data of the previously reported polymorph. XRPD measurement proved that our salt consists of a pure phase of the new polymorph. Cooling down the salt to ca. 230 K caused its color to change from orange-brown to yellow. DSC experiments revealed that during the cooling an endothermic process takes place corresponding to the mentioned color change of the salt

    Crystal structures and other properties of ephedrone (methcathinone) hydrochloride, N‑acetylephedrine and N‑acetylephedrone

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    Purpose Three compounds obtained from ephedrine were identified and characterized by various instrumental analytical methods. Ephedrone (methcathinone) hydrochloride and its fundamental derivatives N-acetylephedrine and N-acetylephedrone were analyzed as precursors of a cathinone derivative. Methods The obtained samples were analyzed by gas chromatography coupled with mass spectrometry, nuclear magnetic resonance spectroscopy, infrared and Raman spectroscopy, and X-ray crystallography. Results The three compounds were confirmed as: N-methyl-2-amino-1-phenylpropan-1-one (methcathinone) hydrochloride, N-acetyl-N-methyl-2-amino-1-phenylpropan-1-one (cathinone derivative), and N-acetyl-N-methyl-2-amino-1-phenylpropan- 1-ol (acetyl derivative of ephedrine). Conclusions X-ray crystallography is especially useful for identifying the new designer drugs and their different precursor forms

    Topological defects in antiferromagnetically coupled multilayers with perpendicular anisotropy

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    A rich variety of specific multidomain textures recently observed in antiferromagnetically coupled multilayers with perpendicular anisotropy include regular (equilibrium) multidomain states as well as different types of topological magnetic defects. Within a phenomenological theory we have classified and analyzed the possible magnetic defects in the antiferromagnetic ground state and determine their structures. We have derived the optimal sizes of the defects as functions of the antiferromagnetic exchange, the applied magnetic field, and geometrical parameters of the multilayer. The calculated magnetic phase diagrams show the existence regions for all types of magnetic defects. Experimental investigations of the remanent states (observed after different magnetic pre-history) in [Co/Pt]/Ru multilayers with wedged Co layers reveal a corresponding succession of different magnetic defect domain types.Comment: 3 pages, 4 figure

    Muon Track Reconstruction and Data Selection Techniques in AMANDA

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    The Antarctic Muon And Neutrino Detector Array (AMANDA) is a high-energy neutrino telescope operating at the geographic South Pole. It is a lattice of photo-multiplier tubes buried deep in the polar ice between 1500m and 2000m. The primary goal of this detector is to discover astrophysical sources of high energy neutrinos. A high-energy muon neutrino coming through the earth from the Northern Hemisphere can be identified by the secondary muon moving upward through the detector. The muon tracks are reconstructed with a maximum likelihood method. It models the arrival times and amplitudes of Cherenkov photons registered by the photo-multipliers. This paper describes the different methods of reconstruction, which have been successfully implemented within AMANDA. Strategies for optimizing the reconstruction performance and rejecting background are presented. For a typical analysis procedure the direction of tracks are reconstructed with about 2 degree accuracy.Comment: 40 pages, 16 Postscript figures, uses elsart.st

    Sensitivity of the IceCube Detector to Astrophysical Sources of High Energy Muon Neutrinos

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    We present the results of a Monte-Carlo study of the sensitivity of the planned IceCube detector to predicted fluxes of muon neutrinos at TeV to PeV energies. A complete simulation of the detector and data analysis is used to study the detector's capability to search for muon neutrinos from sources such as active galaxies and gamma-ray bursts. We study the effective area and the angular resolution of the detector as a function of muon energy and angle of incidence. We present detailed calculations of the sensitivity of the detector to both diffuse and pointlike neutrino emissions, including an assessment of the sensitivity to neutrinos detected in coincidence with gamma-ray burst observations. After three years of datataking, IceCube will have been able to detect a point source flux of E^2*dN/dE = 7*10^-9 cm^-2s^-1GeV at a 5-sigma significance, or, in the absence of a signal, place a 90% c.l. limit at a level E^2*dN/dE = 2*10^-9 cm^-2s^-1GeV. A diffuse E-2 flux would be detectable at a minimum strength of E^2*dN/dE = 1*10^-8 cm^-2s^-1sr^-1GeV. A gamma-ray burst model following the formulation of Waxman and Bahcall would result in a 5-sigma effect after the observation of 200 bursts in coincidence with satellite observations of the gamma-rays.Comment: 33 pages, 13 figures, 6 table

    On the selection of AGN neutrino source candidates for a source stacking analysis with neutrino telescopes

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    The sensitivity of a search for sources of TeV neutrinos can be improved by grouping potential sources together into generic classes in a procedure that is known as source stacking. In this paper, we define catalogs of Active Galactic Nuclei (AGN) and use them to perform a source stacking analysis. The grouping of AGN into classes is done in two steps: first, AGN classes are defined, then, sources to be stacked are selected assuming that a potential neutrino flux is linearly correlated with the photon luminosity in a certain energy band (radio, IR, optical, keV, GeV, TeV). Lacking any secure detailed knowledge on neutrino production in AGN, this correlation is motivated by hadronic AGN models, as briefly reviewed in this paper. The source stacking search for neutrinos from generic AGN classes is illustrated using the data collected by the AMANDA-II high energy neutrino detector during the year 2000. No significant excess for any of the suggested groups was found.Comment: 43 pages, 12 figures, accepted by Astroparticle Physic

    Limits on the high-energy gamma and neutrino fluxes from the SGR 1806-20 giant flare of December 27th, 2004 with the AMANDA-II detector

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    On December 27th 2004, a giant gamma flare from the Soft Gamma-ray Repeater 1806-20 saturated many satellite gamma-ray detectors. This event was by more than two orders of magnitude the brightest cosmic transient ever observed. If the gamma emission extends up to TeV energies with a hard power law energy spectrum, photo-produced muons could be observed in surface and underground arrays. Moreover, high-energy neutrinos could have been produced during the SGR giant flare if there were substantial baryonic outflow from the magnetar. These high-energy neutrinos would have also produced muons in an underground array. AMANDA-II was used to search for downgoing muons indicative of high-energy gammas and/or neutrinos. The data revealed no significant signal. The upper limit on the gamma flux at 90% CL is dN/dE < 0.05 (0.5) TeV^-1 m^-2 s^-1 for gamma=-1.47 (-2). Similarly, we set limits on the normalization constant of the high-energy neutrino emission of 0.4 (6.1) TeV^-1 m^-2 s^-1 for gamma=-1.47 (-2).Comment: 14 pages, 3 figure

    Detection of Atmospheric Muon Neutrinos with the IceCube 9-String Detector

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    The IceCube neutrino detector is a cubic kilometer TeV to PeV neutrino detector under construction at the geographic South Pole. The dominant population of neutrinos detected in IceCube is due to meson decay in cosmic-ray air showers. These atmospheric neutrinos are relatively well-understood and serve as a calibration and verification tool for the new detector. In 2006, the detector was approximately 10% completed, and we report on data acquired from the detector in this configuration. We observe an atmospheric neutrino signal consistent with expectations, demonstrating that the IceCube detector is capable of identifying neutrino events. In the first 137.4 days of livetime, 234 neutrino candidates were selected with an expectation of 211 +/- 76.1(syst.) +/- 14.5(stat.) events from atmospheric neutrinos
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