Correlative microscopy analysis of surface topography in machining Ti-6Al-7Nb

Titanium alloys, namely Ti-6Al-7Nb, are used in the biomedical industry. The study of surface topography is crucial for the development of medical components. The objective of this work is to propose the correlative microscopy technique developed for the analysis of surfaces machined by the turning process of Ti-6Al-7Nb alloy. This technique was based on the association of the 3D reconstruction by extended depth- of-field method from Optical Microscopy (OM) with the Scanning Electron Microscopy (SEM) and microanalysis modes. The correlative microscopy allows a correspondence between the cutting conditions and the material properties, through the analysis of the machined surface.in publicatio

Development of a device compatible with universal testing machine to perform hole expansion and Erichsen cupping tests

The material characterization regarding sheet metal formability is usually assessed by the forming limit curve (FLC). The FLC requires specialized and expensive equipment, several samples with different geometries, and can be a very time-consuming procedure for data treatment. Alternatively, the hole expansion test (HET) and the Erichsen Cupping Test (ECT) can be used for routine evaluations of sheet metal mechanical behavior. These formability tests require fewer quantities of material and easy specimen preparation with a fast analysis of results. The HET and ECT procedures provide a proper evaluation of sheet material stretch-flangeability, formability, strength, and ductility. In this work, we developed a low-cost mechanical device capable of performing the HET and ECT tests using a universal testing machine. The equipment is designed to meet the test parameters set by ISO 16630 (HET) and ISO 20482 (ECT) standards. In order to verify its functionality, tests were carried out with the dual-phase steels DP600 and DP780. The corresponding values determined for the hole expansion ratio and the Erichsen index provided reliable results in terms of the accuracy and repeatability of the proposed testing device.publishe

Characterisation of microbial attack on archaeological bone

As part of an EU funded project to investigate the factors influencing bone preservation in the archaeological record, more than 250 bones from 41 archaeological sites in five countries spanning four climatic regions were studied for diagenetic alteration. Sites were selected to cover a range of environmental conditions and archaeological contexts. Microscopic and physical (mercury intrusion porosimetry) analyses of these bones revealed that the majority (68%) had suffered microbial attack. Furthermore, significant differences were found between animal and human bone in both the state of preservation and the type of microbial attack present. These differences in preservation might result from differences in early taphonomy of the bones. © 2003 Elsevier Science Ltd. All rights reserved