preliminary study of glass production remains found in granada, spain, dated to the 16th and 17th centuries

UID/00729/2020 UID/Multi/04349/2013A set of 14 glass fragments and production remains dated to the 16th and 17th centuries was collected during rescue archaeological works conducted in Granada, Spain, and was characterised by µ-PIXE. This preliminary study constitutes the first analytical approach to glass manufacturing remains from a Spanish production dated to the early-modern period. µ-PIXE allowed for the quantification of major, minor and some trace elements of the glass fragments. It also allowed mapping the elemental distribution on the fragments that were identified as an interface of crucible/glass. This analysis constitutes an evaluation of the ionic exchange between glass and crucible. The glass colours vary from the natural green and blue hues to completely colourless samples. The results show that the majority of the glass samples are of soda-lime-silicate composition, and only one proved to be of a potassium-rich composition. From this, one can hypothesise that glass rich in sodium (following the Mediterranean tradition) and potassium-rich glass (following a central and north European tradition) were both locally produced. Since this location was known as la Calle Horno del Vidrio (Glass Furnace Street) and several production evidences were found, it is highly probable that an artisanal glass production existed in this area.publishersversionpublishe

An Overview of Germanic Grisailles through the Stained-Glass Collection at Pena Palace

The authors would like to thank António Nunes Pereira (Director) and all the team at Pena National Palace for in their efforts to make this and similar ongoing research possible through their collaboration and stimulus, as well as to Parques de Sintra—Monte da Lua for access to the collection studied. The authors also thank the anonymous reviewers for their valuable contribution to the improvement and enrichment of the manuscript. Publisher Copyright: © 2022 by the authors. Licensee MDPI, Basel, Switzerland.The lack of studies reporting the characterisation of Germanic grisaille is evident, despite the recent interest of researchers in this glass painting material. This work consists of the first assessment of Germanic grisaille’ chemical composition on a wide chronology (14th–19th centuries), that was only possible through the unique stained-glass collection of King Ferdinand II of Portugal. From the considerable amount of panels produced in Germanic territory and assembled by Ferdinand, twenty-two panels were characterised, and some trends of glass support typical composition and grisaille recipes were verified through this case study. A copper-based grisaille appears to have been the preference up to the 18th century. The 19th century shows higher diversity in composition, with new compounds (such as Co, Cr, Mn) appearing as colourising materials. However, with a limited number of analyses, and dispersed throughout time and different geographic locations, the results of this study are unprecedented, by being able to present the first overview on grisaille composition in Germanic stained glasses.publishersversionpublishe

Caracterização de uma conta de vidro proveniente do povoado fortificado calcolítico da Moita da Ladra (Vila Franca de Xira)

The full excavation of the fortified Chalcolithic settlement of Moita da Ladra by one of us (J.L.C.) has shown the existence of a single archaeological layer corresponding to the occupation of the site during the second half of the 3rd millennium BC. Among the archaeological remains collected during the field campaigns there is a bead, with a spheroid shape, longitudinally fractured, presenting a black matrix with numerous whitish spots. The fracture presents a vitreous greasy surface, and exposes a suspension cylindrical bore. Various techniques were used to identify the material that was used in the manufacture of the artifact, including CHN elemental analysis, EDXRF, μ-PIXE and XRD, conducted by the other authors. It was found that the material is not organic (carbon is absent), presenting significant amounts of the elements Si, K, Ca, Ti, Fe, Sr, Zr, and Sb. The X-ray diffraction spectra indicates that the material has an essentially vitreous nature, being the whitish particles dispersed in the vitreous mass identified as quartz. μ-PIXE results show a chemical composition that is consistent with an artificial glass, which implies a much more recent chronology for the bead than that of the Chalcolithic archaeological layer where it was recovered. Thus, although the bead was recorded from a Chalcolithic context, its provenance must be ascribed to the Late Bronze Age occupation recorded nearby and resulting from the early Phoenician trade.info:eu-repo/semantics/publishedVersio

a set of foreign stained glasses in Portugal

This work presents the first results of the iconographic study and analytical characterisation of a set of four stained-glass panels that are part of the collection of National Palace of Pena (Sintra, Portugal). These panels were collected by the King Ferdinand II in the mid-nineteenth century, for his main residence the Palace of Necessidades (Lisbon, Portugal), and only first presented to the general public in 2011. This study contributes with the knowledge of Technical Art History and Heritage Science to a better and deeper understanding of their history, materials and techniques used in the production, where an art-historical and a scientific approach are applied to attribute their origins. Based on the analysis of the formal and stylistic characteristic of the panels, it is proposed that the drawings used for the production of three of these panels may be based on the design and painting being carried out in the same workshop, and that the four panels have the same provenance (Germany). The composition of the glass and grisaille was determined and colourising elements were identified. Through this approach, conclusive correlation between the analysed glasses was possible: all are calcium rich or calcium–potassium rich types, and the results also suggest that the same source of silica was used for their production. A typical mixture of glass and lead oxide was found in the grisaille applied on the painted panels. However, less usual was the use of a copper oxide pigment for the black grisaille. All these findings support the proposals made regarding provenance and production period (fifteenth century).publishersversionpublishe

Um estudo analítico

UID/EAT/00729/2019 PD/BD/136673/2018Grisaille is one of the oldest and most widely used vitreous paint applied for the production of stained-glass panels and Debitus is one of the most renowned commercial brands whose grisailles are frequently used for the chromatic reintegration in stained-glass window restoration. This article presents the morphological, chemical and thermal analyses of five grisailles from Debitus, to evaluate their properties before and after firing with the objective of knowing their future stability. The characterisation was carried out by optical microscopy, scanning electron microscopy, particle induced X-ray emission, X-ray diffraction, and infrared thermography. This study showed a well-balanced ratio between the different components and a good interdiffusion into the glass, as well as a consistent thermal behaviour between them and with the glass, which indicates the good stability and durability of these materials.publishersversionpublishe

Leitura arqueométrica de artefactos do final da Idade do Bronze: depósitos metálicos de Santa Cruz e de S. Francisco da Serra (Santiago do Cacém)

No âmbito da preparação do Atlas do Património Cultural do Alentejo Litoral e Costa Vicentina, coordenado por uma das signatárias (J. S.), procedeu-se à análise química de três machados metálicos do Museu de Santiago do Cacém por µ-sonda de feixe externo, por forma a clarificar a biografia desses artefactos, e a ensaiar a recontextualização dos mesmos. As peças agora estudadas foram manufacturadas em ligas de bronze (Cu-Sn), com teores variáveis de estanho (8,2 a 15,8% Sn) e acrescentam informação sobre dois possíveis depósitos metálicos do final da Idade do Bronze: Sobral da Várzea/Santa Cruz e Senhora do Livramento.Concerning the development of the Atlas of Cultural Heritage of the Southwest Portuguese Coast, coordinated by one of the authors (J. S.), three metallic axes part of the Museu de Santiago do Cacém collection were analysed by µ-PIXE to determine the elemental composition in order to clarify their biography and reappraise the archaeological contextualization. The axes are composed of binary bronze alloys (Cu-Sn) with distinct tin contents (8,2 to 15,8% Sn) and low amount of iron shedding new light on two probable Late Bronze Age deposits: Sobral da Várzea/Santa Cruz and Senhora do Livramento.info:eu-repo/semantics/publishedVersio

Modernizando o ensino de Ciências com atividades gamificadas e jogos digitais / Modernizing Science teaching with gamified activities and digital games

Este artigo descreve os resultados parciais de um projeto em andamento realizado por alunos do IFSP (Campus São José dos Campos). Eles realizam pesquisas e atividades de programação de jogos lúdicos voltados para o ensino de Ciências e Química. Com a crescente popularização das tecnologias de informação e do consumo de jogos digitais, fica evidente a importância da realização de estudos que analisem o uso de jogos em contexto educacional. Assim, aplicando um formulário online para alunos do Ensino Fundamental II e Médio para obter suas preferências quanto aos estilos de jogos comercializados. O objetivo principal da pesquisa foi analisar os resultados para a futura produção de jogos educativos que sejam eficientes para a construção de um ambiente participativo de ensino e aprendizagem contextualizado para os alunos. O papel do educador na utilização dos jogos educativos está no planejamento metodológico, ou seja, na análise dos materiais necessários à produção, execução e feedback, exigindo conhecimentos básicos na área de tecnologia da informação.

An overview of migratory birds in Brazil

We reviewed the occurrences and distributional patterns of migratory species of birds in Brazil. A species was classified as migratory when at least part of its population performs cyclical, seasonal movements with high fidelity to its breeding grounds. Of the 1,919 species of birds recorded in Brazil, 198 (10.3%) are migratory. Of these, 127 (64%) were classified as Migratory and 71 (36%) as Partially Migratory. A few species (83; 4.3%) were classified as Vagrant and eight (0,4%) species could not be defined due to limited information available, or due to conflicting data.Fil: Somenzari, Marina. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Amaral, Priscilla Prudente do. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Cueto, Víctor. Consejo Nacional de Investigaciones Científicas y Técnicas. Centro Científico Tecnológico Conicet - Patagonia Norte. Centro de Investigación Esquel de Montaña y Estepa Patagóica. Universidad Nacional de la Patagonia "San Juan Bosco". Facultad de Ciencias Naturales - Sede Esquel. Centro de Investigación Esquel de Montaña y Estepa Patagónica; ArgentinaFil: Guaraldo, André de Camargo. Universidade Federal do Paraná; BrasilFil: Jahn, Alex. Universidade Estadual Paulista Julio de Mesquita Filho; BrasilFil: Lima, Diego Mendes. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Lima, Pedro Cerqueira. Fundação BioBrasil; BrasilFil: Lugarini, Camile. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Machado, Caio Graco. Universidade Estadual de Feira de Santana; BrasilFil: Martinez, Jaime. Universidade de Passo Fundo; BrasilFil: do Nascimento, João Luiz Xavier. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Pacheco, José Fernando. Comitê Brasileiro de Registros Ornitológicos; BrasilFil: Paludo, Danielle. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Prestes, Nêmora Pauletti. Universidade de Passo Fundo; BrasilFil: Serafini, Patrícia Pereira. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Silveira, Luís Fábio. Universidade de Sao Paulo; BrasilFil: de Sousa, Antônio Emanuel Barreto Alves. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: de Sousa, Nathália Alves. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: de Souza, Manuella Andrade. Centro Nacional de Pesquisa e Conservação de Aves Silvestres. Instituto Chico Mendes de Conservação da Biodiversidade; BrasilFil: Telino-Júnior, Wallace Rodrigues. Universidade Federal de Pernambuco; BrasilFil: Whitney, Bret Myers. State University of Louisiana; Estados Unido

Pervasive gaps in Amazonian ecological research

Biodiversity loss is one of the main challenges of our time,1,2 and attempts to address it require a clear un derstanding of how ecological communities respond to environmental change across time and space.3,4 While the increasing availability of global databases on ecological communities has advanced our knowledge of biodiversity sensitivity to environmental changes,5–7 vast areas of the tropics remain understudied.8–11 In the American tropics, Amazonia stands out as the world’s most diverse rainforest and the primary source of Neotropical biodiversity,12 but it remains among the least known forests in America and is often underrepre sented in biodiversity databases.13–15 To worsen this situation, human-induced modifications16,17 may elim inate pieces of the Amazon’s biodiversity puzzle before we can use them to understand how ecological com munities are responding. To increase generalization and applicability of biodiversity knowledge,18,19 it is thus crucial to reduce biases in ecological research, particularly in regions projected to face the most pronounced environmental changes. We integrate ecological community metadata of 7,694 sampling sites for multiple or ganism groups in a machine learning model framework to map the research probability across the Brazilian Amazonia, while identifying the region’s vulnerability to environmental change. 15%–18% of the most ne glected areas in ecological research are expected to experience severe climate or land use changes by 2050. This means that unless we take immediate action, we will not be able to establish their current status, much less monitor how it is changing and what is being lostinfo:eu-repo/semantics/publishedVersio