97 research outputs found

    Quantitative determinations and imaging in different structures of buried human bones from the XVIII-XIXth centuries by energy dispersive X-ray fluorescence - Postmortem evaluation

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    In this work, a non-commercial triaxial geometry energy dispersive X-ray Fluorescence (EDXRF) setup and a benchtop mu-XRF system were used to identify postmortem contamination in buried bones. For two of the individuals, unusually high concentrations of Cu and Pb, but also Zn (in one individual) were observed. The pigments of the burial shroud coverings have been identified as the source of contamination.Accurate and precise quantitative results were obtained by nondestructive process using fundamental parameters method taking into account the matrix absorption effects.A total of 30 bones from 13 individuals, buried between the mid-XVlllth to early XIXth centuries, were analyzed to study the elemental composition and elemental distribution. The bones were collected from a church in Almada (Portugal), called Ermida do Espirito Santo, located near the Tagus River and at the sea neighbourhood.The triaxial geometry setup was used to quantify Ca, Fe, Cu, Zn, Br, Sr and Pb of powder pressed bone pellets (n=9 for each bone). Cluster analysis was performed considering the elemental concentrations for the different bones. There was a clear association between some bones regarding Fe, Cu, Zn, Br and Pb content but not a categorization between cortical and trabecular bones. The elemental distribution of Cu, Zn and Pb were assessed by the benchtop p.-analysis, the M4 Tornado, based on a polycapillary system which provides multi-elemental 2D maps. The results showed that contamination was mostly on the surface of the bone confirming that it was related to the burial shroud covering the individuals

    Combining ÎŒXANES and ÎŒXRD mapping to analyse the heterogeneity in calcium carbonate granules excreted by the earthworm Lumbricus terrestris

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    The use of fluorescence full spectral micro-X-ray absorption near-edge structure (ÎŒXANES) mapping is becoming more widespread in the hard energy regime. This experimental method using the Ca K-edge combined with micro-X-ray diffraction (ÎŒXRD) mapping of the same sample has been enabled on beamline I18 at Diamond Light Source. This combined approach has been used to probe both long- and short-range order in calcium carbonate granules produced by the earthworm Lumbricus terrestris. In granules produced by earthworms cultured in a control artificial soil, calcite and vaterite are observed in the granules. However, granules produced by earthworms cultivated in the same artificial soil amended with 500 p.p.m. Mg also contain an aragonite. The two techniques, ÎŒXRD and ÎŒXANES, probe different sample volumes but there is good agreement in the phase maps produced

    Public Communication in a Pandemic : Language in COVID‐19 public health advertising

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    This linguistic study in the field of pragmatics looked at the language used by public health authorities in Australia, the United Kingdom and the United States to inform citizens about COVID-19 in 2020 and 2021. It made a qualitative analysis of advertisements that were posted on Instagram by the Department of Health and Aged Care, the National Health Service and the Centers for Disease Control and Prevention in relation to COVID-19 during this time frame. Using Speech Act Theory and Gricean theory on the cooperative principle and conversational implicature, it shows how these linguistic features were operationalised in the advertisements to achieve a certain behaviour from its audience. The study also compared language use between the selected countries and over time. Some minor differences that can be attributed to national contexts, such as sporting events, specific holidays or differences caused by the strategies chosen to address the pandemic were found.Denna studie i det lingvistiska omrÄdet pragmatik studerar det sprÄk som anvÀndes av folkhÀlsomyndigheter i Australien, Storbritannien och USA för att informera medborgare om COVID-19 under Ären 2020 och 2021. Den gör en kvalitativ analys av COVID-19-relaterade annonser som publicerats pÄ Instagram av australiensiska Department of Health and Aged Care, brittiska National Health Service och amerikanska Centers for Disease control and Prevention under denna tidsperiod. Med hjÀlp av talaktsteori och Grices teorier om samarbetsprincipen och hans konversationsmaximer visar studien hur dessa sprÄkliga aspekter anvÀnds i annonserna för att uppnÄ ett önskat beteende frÄn sin tÀnkta publik. Studien jÀmförde Àven sprÄkanvÀndning mellan de utvalda lÀnderna och över tid. NÄgra mindre skillnader som kan hÀnföras till nationella sammanhang, som exempelvis idrottsevenemang, specifika helgdagar eller skillnader orsakade av de strategier som valts för att hantera pandemin noterades
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