Successfully estimating tensile strength by small punch testing

The Small Punch (SP) test is a relatively simple test well suited for material ranking and material property estimation in situations where standard testing is not possible or considered too material consuming. The material tensile properties, e.g. the ultimate tensile strength (UTS) and the proof strength are usually linearly correlated to the force-deflection behaviour of a SP test. However, if the test samples and test set-up dimensions are not according to standardized dimensions or the material ductility does not allow the SP sample to deform to the pre-defined displacements used in these correlations, the standard formulations can naturally not be used. Also, in cases where no supporting UTS data is available the applied correlation factors cannot be verified. In this paper a formulation is proposed that enables the estimation of UTS without supporting uniaxial tensile strength data for a range of materials, both for standard type and for curved (tube section) samples. The proposed equation was originally developed for estimating the equivalent stress in small punch creep but is also found to robustly estimate the UTS of several ductile ferritic, ferritic/martensitic and austenitic steels. It is also shown that the methodology can be further applied on non-standard test samples and test set-ups and to estimate the properties of less ductile materials such as 46% cold worked 15-15Ti cladding steel tubes. In the case of curved samples the UTS estimates have to be corrected for curvature to match the corresponding flat specimen behaviour. The geometrical correction factors are dependent on tube diameters and wall thicknesses and were determined by finite element simulations. The outcome of the testing and simulation work shows that the UTS can be robustly estimated both for flat samples as well as for thin walled tube samples. The usability of the SP testing and assessment method for estimating tensile strength of engineering steels in general and for nuclear claddings in specific has been verified

Multiscale modelling for fusion and fission materials: the M4F project

The M4F project brings together the fusion and fission materials communities working on the prediction of radiation damage production and evolution and its effects on the mechanical behaviour of irradiated ferritic/martensitic (F/M) steels. It is a multidisciplinary project in which several different experimental and computational materials science tools are integrated to understand and model the complex phenomena associated with the formation and evolution of irradiation induced defects and their effects on the macroscopic behaviour of the target materials. In particular the project focuses on two specific aspects: (1) To develop physical understanding and predictive models of the origin and consequences of localised deformation under irradiation in F/M steels; (2) To develop good practices and possibly advance towards the definition of protocols for the use of ion irradiation as a tool to evaluate radiation effects on materials. Nineteen modelling codes across different scales are being used and developed and an experimental validation programme based on the examination of materials irradiated with neutrons and ions is being carried out. The project enters now its 4th year and is close to delivering high-quality results. This paper overviews the work performed so far within the project, highlighting its impact for fission and fusion materials science.This work has received funding from the Euratom research and training programme 2014-2018 under grant agreement No. 755039 (M4F project)

Towards modelling intergranular stress-corrosion cracks using experimentally obtained grain topologies

Predicting the effects of material aging in view of development of intergranular damage is of particular importance in a number of nuclear installations and especially in structural integrity assessments of critical components in energy generating power plants. Since the damage is initialized on small length scales, detailed multiscale models should be employed to tackle the problem. However, the complexity of such models is high due to the need of incorporating micro structural features. In line of this the research group from Jožef Stefan Institute and The University of Manchester joined forces and knowledge in development of such detailed multiscale models. The basic idea was to pair the knowledge of advanced experimental techniques of The University of Manchester group with the knowledge of advanced microstructure modelling techniques of the group at Jožef Stefan Institute. The presented paper proposes a novel approach for intergranular crack modelling whereby a state-of-the-art X-ray diffraction contrast tomography technique is used to obtain 3D topologies and crystallographic orientations of individual grains in a stainless steel wire and intergranular stress corrosion cracks. As measured topologies and orientations of individual grains are then reconstructed within a finite element model and coupled with advanced constitutive material behaviour: anisotropic elasticity and crystal plasticity. Due to the extreme complexity of grain topologies, transferring this information into the finite element model presents a challenging task. The feasibility of the proposed approach is presented. Difficulties in building a finite element model are discussed. Preliminary results of the analyses are also given. Copyright © 2009 by ASME

Offline commissioning of a new gas cell for the MARA Low-Energy Branch

Results of offline commissioning tests for a new dedicated gas cell for the Mass Analysing Recoil Apparatus (MARA) Low-Energy Branch are reported. Evacuation time, ion survival and transport efficiency in helium buffer gas were characterized with a radioactive 223Raα-recoil source. Suppression of the ion signal, originating from non-neutralized species in the gas cell, was explored with 219Rn ions, the daughter recoil of 223Ra, as a function of voltage applied to one of the ion-collector electrodes. Two-step laser resonance ionization of stable tin isotopes produced inside the gas cell from a heated bronze filament was demonstrated, and broadening of the atomic resonances in argon buffer gas was studied. These tests indicate the suitability of the new gas cell for future in-gas laser spectroscopy studies of exotic nuclei at the Accelerator Laboratory of the University of Jyväskylä