2,113 research outputs found

    Preparation and characterization of magnetite (Fe3O4) nanoparticles By Sol-Gel method

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    The magnetite (Fe3O4) nanoparticles were successfully synthesized and annealed under vacuum at different temperature. The Fe3O4 nanoparticles prepared via sol-gel assisted method and annealed at 200-400ºC were characterized by Fourier Transformation Infrared Spectroscopy (FTIR), X-ray Diffraction spectra (XRD), Field Emission Scanning Electron Microscope (FESEM) and Atomic Force Microscopy (AFM). The XRD result indicate the presence of Fe3O4 nanoparticles, and the Scherer`s Formula calculated the mean particles size in range of 2-25 nm. The FESEM result shows that the morphologies of the particles annealed at 400ºC are more spherical and partially agglomerated, while the EDS result indicates the presence of Fe3O4 by showing Fe-O group of elements. AFM analyzed the 3D and roughness of the sample; the Fe3O4 nanoparticles have a minimum diameter of 79.04 nm, which is in agreement with FESEM result. In many cases, the synthesis of Fe3O4 nanoparticles using FeCl3 and FeCl2 has not been achieved, according to some literatures, but this research was able to obtained Fe3O4 nanoparticles base on the characterization results

    Preparation of high performance conductive Polyaniline Magnetite (PANI/Fe3O4) nanocomposites by sol-gel method

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    The conductivities of polyaniline magnetite (PANI/Fe3O4) nanocomposites prepared by sol-gel method were measured by standard van der Pauw DC 4-point probe method. PANI/Fe3O4 conductivity was measured as a function of wt % (5, 10, 15, 20 and 25 wt %) of Fe3O4 nanoparticles. It was observed that the conductivity of polyaniline containing certain percentage of Fe3O4 nanoparticles is slightly lower than the bulk PANI nanotubes and drastically decreases with increase of wt % Fe3O4 nanoparticles. The high conductivities of PANI/ Fe3O4 nanocomposites was observed due to high concentration of dopant (oxidants) used in the polymerization process and the optimization of these composites allows this being use as a parameter for the production of nanofibers. Fourier transform infrared spectra, field emission scanning electron microscope, X-ray diffraction and ultraviolet-visible absorption spectra are used to characterize the phase structure, morphologies and functional group of the PANI/Fe3O4 composites samples. Fourier transform infrared analysis indicates the presence of PANI containing Fe3O4 nanoparticles and the field emission scanning electron microscope (FESEM) results has proven that the formation of nanofibers in the PANI/Fe3O4 nanocomposites. The crystalline phase of PANI/Fe3O4 nanocomposites studied by X-ray diffraction indicated that the Fe3O4 nanoparticles was present in the PANI matrices

    Peranan Hukum Adat dalam Menjaga Kelestarian Hutan Larangan Adat Kenegerian Rumbio Kecamatan Kampar Kabupaten Kampar

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    One example of common law in Indonesia is common law in Kenegerian Rumbio, Kampar District, Kampar Regency, Riau Province. Kenegerian Rumbio has banned indigenous forest still maintained continuity. The forest area is listed on the Forest department is approximately 530 ha. This is research used a snowball sampling technique, subjects were selected based on recommendations person to person according to research to be interviewed. Data collection methods used in this study were in-depth interviews, observation, and study documents. The data analysis was conducted in three phases. The first phase, researchers conducted an analysis that linked the answers intrasubjek subjects with theory and concepts related to the research. The second phase, conducted antarsubjek analysis comparing data from each subject. At this stage, researchers performed the interpretation of the data so as to achieve the purpose of research. The third phase, the data collected were then analyzed using descriptive analysis. Kenegerian Rumbio customary law has two forms of customary rules in the forest preserve customary prohibition, namely: the rules of the ban and the rules of thing is allowed. The rules of prohibition are: cutting down trees without permission from the ninik mamak, burn the forest, enable divert forest land, wildlife hunting, arrogant when entering the forest, and speaking dirty in the woods. While the form of the permitted rules are: take firewood (wood that is already dead), took the fruit has matured, and conduct scientific research. If there is a breach in the case, the perpetrator will be prosecuted according to the customary laws in Kenegerian Rumbio. The perpetrator will be given sanction in accordance with the agreement of the ninik mamak in the deliberations conducted in the customary hall

    A Consistency Check of Concrete Compressive Strength using Pearson’s Correlation Coefficient

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    The efficiency of the concrete ready mix service provider is undoubtedly and has become a widespread trend among contractors in which facilitates and eliminated a large budget surplus in maintenance, operating costs and is preferred as it reflects more efficient asset utilization. However, the quality assurance of concrete supplied is always raised associated with the inconsistencies of concrete compressive strength at the age of 28 days. The objective(s) of this study are to determine the correlations between the compressive strength of ready mix concrete, to evaluate the consistencies of the results and to identify the irregular sources that lead to the inconsistencies. Based on the compressive strength values obtained from the existing experimental data using different concrete mixes from the batching plant, a statistical analysis was conducted. A total of 90 concrete cubes specimens were attained from 15 concrete batches. A correlation analysis was conducted using the Pearson Correlation calculation to check the consistency of concrete compressive strength. The calculation showed the Pearson correlation coefficient of this study is +0.990. This indicated that there are significant linear relationship exists between the concrete compressive strength and the density of concrete batches which is positively high. In conclusion, the analysis reveals that the design of ready mix concrete compressive strength is in high consistencies and acceptable in practices for the proposed mix design to the contractor. Doi: 10.28991/cej-2021-03091672 Full Text: PD

    Quality-of-life and beliefs about medication in relation to a therapy adherence intervention in resistant hypertension:the Resistant HYpertension: MEasure to ReaCh Targets trial

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    Objective: To assess the impact of personalized feedback on therapy adherence testing results on quality of life and beliefs about medication in patients with resistant hypertension, as well as to identify patient-oriented predictors of therapy adherence. Methods: This study was a prespecified post hoc analysis of the multicenter randomized controlled trial Resistant Hypertension: Measure to Reach Targets (RHYME-RCT). Patients were randomized to a personalized feedback conversation on measured antihypertensive drug levels additional to standard-of-care, or standard-of-care only. The primary outcomes consisted of EuroQol EQ-5D-5L and Beliefs about Medicine Questionnaire (BMQ) scores at 12 months. Results: A total of 56 patients with median age 61.5 [25th-75th percentile: 55.8-69.3] years (21.4% women) were included. Mean blood pressure ±SD was 149.8/84.1 ± 14.9/13.8 mmHg while being on a median of 5.6 [4.8-7.3] defined daily dosages (DDD) of antihypertensive drugs. At 12 months, no differences were observed in EQ-5D-5L index (0.81 [0.69-0.89] vs. 0.89 [0.73-1.00]; P = 0.18) and visual analogue scale score on general patient-perceived health (70 [60-80] vs. 70 [60-82]; P = 0.53) between the intervention-arm and the standard-of-care only-arm. Likewise, individual EQ-5D-5L domain scores and BMQ scores did not differ between both arms. Irrespective of the intervention, independent positive predictors of the percentage adherence were patient age, EQ-5D-5L index score, BMQ-specific necessity score and concern score, whereas the total number of drugs prescribed was a negative predictor. Conclusion: Within this prespecified subanalysis of the randomized RHYME-RCT trial, implementation of a personalized feedback conversation targeting therapy adherence did not improve health-related quality-of-life and beliefs about medication in patients with resistant hypertension.</p

    Impacts of Dietary Lysine and Crude Protein on Performance, Hepatic and Renal Functions, Biochemical Parameters, and Histomorphology of Small Intestine, Liver, and Kidney in Broiler Chickens

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    The present study aimed to investigate the effects of increasing dietary lysine (Lys) levels with an adequate dietary crude protein (CP) content, as well as the effects of a reduction in dietary CP content with the recommended amino acid (AAs) level, on the performance, blood biochemical parameters, and histomorphology of the duodenum, liver, and kidney in broiler chickens. A total of 500 broiler chickens were randomly distributed into five dietary treatment groups, following a completely randomized design, where, at the beginning, the control group (C) was fed a diet containing the standard CP and Lys levels: 23% CP with 1.44% Lys during the starter period; 21.5% CP with 1.29% Lys during the growing period; and 19.5% CP with 1.16% Lys during the finishing period. The Lys content was increased by 10% above the recommended control basal requirements in the second group (Gr1) and by 20% in the third group (Gr2), while using the same recommended CP percentage as the C group. The fourth group (Gr3) had a 1% lower CP content and the fifth group had a 2% lower CP content than the C group, with the same recommended AA level as the C group. Increasing the Lys content in the Gr1 group improved the broilers’ weight gains (p \u3c 0.05) during the starter, growing, and finishing periods. Decreasing dietary CP with the standard AA levels (Gr3 and Gr4) did not significantly affect (p \u3e 0.05) the live weight gain, feed intake, or feed conversion ratio (FCR) of the broilers compared with those fed with the C diet. Blood total bilirubin, direct and indirect bilirubin, triglycerides, cholesterol, low-density lipoprotein (LDL), and very LDL were not different among the experimental groups. However, blood aspartate aminotransferase levels were increased (p \u3c 0.05) in the Gr1 and Gr3 groups compared with the other treatment groups. All dietary treatments decreased the serum creatinine levels (p \u3c 0.05) compared with the C group. The Gr2 broilers had greater serum total protein and globulin (p \u3c 0.05) than those receiving the other treatments. Increasing dietary Lys levels resulted in a significant improvement in duodenum villus height and width (p \u3c 0.05), while the low-CP diets resulted in shorter villi length and width, along with degenerated areas and lymphocytic infiltration. Low dietary CP content induced hepatocyte disorganization and moderate degeneration, along with vacuolated hepatic cells, excessive connective tissue, and lymphocytic infiltration. The cortical regions of the kidney exhibited obvious alterations in the Gr3 and Gr4 groups and large interstitial spaces were found between tubules. Renal tubules in the Gr3 and Gr4 groups were smaller in size and some of these tubules were atrophied. In conclusion, reducing dietary CP levels to 1% or 2% lower than the recommended level did not negatively affect growth performance, inducing minimal influence on the blood metabolic indicators of health status, and resulting in moderate alterations to the histomorphology of the duodenum, liver, and kidney. Furthermore, increasing the Lys content by 10% above the recommended level improved the growth performance, health status, and histomorphology of the duodenum, liver, and kidney in broiler chickens

    Симптоматические выражения с семантикой проявления радости в хинди и в русском языке

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    ВУЗЫВЫСШИЕ УЧЕБНЫЕ ЗАВЕДЕНИЯОБРАЗОВАНИЕ МЕДИЦИНСКОЕСТУДЕНТЫ МЕДИЦИНСКИХ УЧЕБНЫХ ЗАВЕДЕНИЙИНОСТРАННЫЕ СТУДЕНТЫРУССКИЙ ЯЗЫКСЕМАНТИКАСИМПТОМАТИЧЕСКИЕ ВЫРАЖЕНИЯХИНДИРАДОСТ

    A search for charged massive long-lived particles

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    We report on a search for charged massive long-lived particles (CMLLPs), based on 5.2 fb1^{-1} of integrated luminosity collected with the D0 detector at the Fermilab Tevatron ppˉp\bar{p} collider. We search for events in which one or more particles are reconstructed as muons but have speed and ionization energy loss (dE/dx)(dE/dx) inconsistent with muons produced in beam collisions. CMLLPs are predicted in several theories of physics beyond the standard model. We exclude pair-produced long-lived gaugino-like charginos below 267 GeV and higgsino-like charginos below 217 GeV at 95% C.L., as well as long-lived scalar top quarks with mass below 285 GeV.Comment: submitted to Phys. Rev. Letter
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