Remote Nanoimaging on Mars - Results of the Atomic Force Microscope Onboard NASA's Phoenix Mission

Extended abstract of a paper presented at Microscopy and Microanalysis 2011 in Nashville, Tennessee, USA, August 7-August 11, 201

Habitability of the Phoenix landing site

Peer Reviewedhttp://deepblue.lib.umich.edu/bitstream/2027.42/95488/1/jgre2706.pd

AFM investigation of Martian soil simulants on micromachined Si substrates

The micro and nanostructures of Martian soil simulants with particles in the micrometre-size range have been studied using a combination of optical and atomic force microscopy (AFM) in preparation for the 2007 NASA Phoenix Mars Lander mission. The operation of an atomic force microscope on samples of micrometre-sized soil particles is a poorly investigated area where the unwanted interaction between the scanning tip and loose particles results in poor image quality and tip contamination by the sample. In order to mitigate these effects, etched silicon substrates with a variety of features have been used to facilitate the sorting and gripping of particles. From these experiments, a number of patterns were identified that were particularly good at isolating and immobilizing particles for AFM imaging. This data was used to guide the design of micromachined substrates for the Phoenix AFM. Both individual particles as well as aggregates were successfully imaged, and information on sizes, shapes and surface morphologies were obtained. This study highlights both the strengths and weaknesses of AFM for the potential in situ investigation of Martian soil and dust. Also presented are more general findings of the limiting operational constraints that exist when attempting the AFM of high aspect ratio particles with current technology. The performance of the final designs of the substrates incorporated on Phoenix will be described in a later paper. © 2007 The Authors

Microscopy capabilities of the Microscopy, Electrochemistry, and Conductivity Analyzer

The Phoenix microscopy station, designed for the study of Martian dust and soil, consists of a sample delivery system, an optical microscope, and an atomic force microscope. The combination of microscopies facilitates the study of features from the millimeter to nanometer scale. Light-emitting diode illumination allows for full color optical imaging of the samples as well as imaging of ultraviolet-induced visible fluorescence. The atomic force microscope uses an array of silicon tips and can operate in both static and dynamic mode. Copyright 2008 by the American Geophysical Union

Microscopy analysis of soils at the Phoenix landing site, Mars: Classification of soil particles and description of their optical and magnetic properties

The optical microscope onboard the Phoenix spacecraft has returned color images (4 ?m pixel?1) of soils that were delivered to and held on various substrates. A preliminary taxonomy of Phoenix soil particles, based on color, size, and shape, identifies the following particle types [generic names in brackets]: (1) reddish fines, mostly unresolved, that are spectrally similar to (though slightly darker than) global airborne dust [red fines], (2) silt? to sand?sized brownish grains [brown sand], (3) silt? to sand?sized black grains [black sand], and (4) small amounts of whitish fines, possibly salts [white fines]. Most particles have a saturation magnetization in the range 0.5?2 Am2 kg?1 as inferred from their interaction with magnetic substrates. The particle size distribution has two distinct peaks below 10 ?m (fines) and in the range 20–100 ?m (grains), respectively, and is different from that of ripple soils in Gusev crater. In particular medium to large sand grains appear to be absent in Phoenix soils. Most sand grains have subrounded shape with variable texture. A fractured grain (observed on sol 112) reveals evidence of micrometer?sized crystal facets. The brown sand category displays a large diversity in color including shiny, almost colorless particles. Potential source regions for these grains may be the Tharsis volcanoes or Heimdal crater (20 km east of the landing site). The black grains are suggested to belong to a more widespread population of particles with mafic mineralogy. The absence of black/brown composite grains is consistent with different formation pathways and source regions for each grain type.Precision and Microsystems EngineeringMechanical, Maritime and Materials Engineerin