Polymer optical fiber gratings for microwave photonics and communications application

Tesis por compendio[ES] Con el continuo desarrollo de materiales y tecnologías de fabricación durante las últimas tres décadas, la atenuación de la transmisión de las fibras ópticas de polímero (POF) se ha reducido considerablemente. Las POF son ventajosas para las redes domésticas, así como para las interconexiones de almacenamiento, y tienen ventajas significativas para muchas aplicaciones de detección, que incluye el límite alto de tensión elástica, alta resistencia a la fractura, alta flexibilidad en la flexión, alta sensibilidad a la tensión y coeficientes termoópticos negativos. Esta tesis consigue mejorar la tecnología de irradiación con láser para POF e investiga dispositivos especiales basados en redes de difracción en POF para comunicaciones ópticas, microondas, fotónica y detección. En particular, desarrollamos la tecnología de fabricación rápida de FBGs en POF con un estudio detallado y la optimización de los parámetros de fabricación de redes de difracción de Bragg en fibra (FBG). Los resultados más destacados incluyen un FBG uniforme de 8 dB con un solo pulso láser Nd: YAG (26 nsm) (8 ns) basado en fibra dopada con BDK, que es el tiempo más corto presentado hasta ahora para la fabricación de FBGs en POF. La irradiación de fibras ópticas de polímero utilizando diferentes materiales basado en el láser KrF a 248 nm permitió demostrar un mejor rendimiento en comparación con el sistema que emplea el láser He-Cd a 325 nm. Además, se fabricaron FBGs uniformes en POFs de índice escalón dopadas con TS en menos de 1 segundo mediante la repetición de pulsos con baja energía. Finalmente, el estudio de la irradiación UV con pulsos de baja energía para la fabricación de redes de difracción estables permitió ahorrar energía en el proceso de fabricación de FBGs en POF, como uno de los principales requisitos para la producción en masa. Basándonos en la tecnología de fabricación mejorada, nos centramos en la fabricación de redes de difracción con diferentes estructuras: se fabricó un FBG con desplazamiento de fase utilizando dos pulsos de 15 ns a 248 nm KrF superpuestos por el método de Moiré; el primer FBG con chirp sintonizable se logró utilizando un solo pulso corto del láser, que abrió nuevas perspectivas a las aplicaciones basadas en redes de difracción con chirp en POF; también se propuso un nuevo método basado en gradientes térmicos para obtener FBG con chirp en POF basadas en FBG uniformes, y se demostró como la forma más conveniente publicada hasta la fecha para lograr este tipo de FBGs no uniformes en POF; y, finalmente, también se han fabricado redes de difracción de largo período utilizando un proceso de fabricación de corto tiempo, especialmente en comparación con investigaciones anteriores. En la última parte de la tesis, y en base a los dispositivos basados en redes de difracción obtenidos a lo largo de este trabajo, se han propuesto varias aplicaciones . De manera similar a los FBG en fibra de sílice, los FBGs con chirp en POF tienen muchas aplicaciones futuras en las áreas de comunicaciones ópticas y de los sensores. Este documento describe la aplicación de detección de tensión basada en una FBG con chirp sintonizable en POF, su aplicación para detección térmica en sistemas biomédicos; e ilustra el potencial de los dispositivos de dispersión sintonizables en el campo de las comunicaciones ópticas, bien como compensación de dispersión o en fotónica de microondas.[CA] Amb el continu desenvolupament de materials i tecnologies de fabricació durant les últimes tres dècades, l'atenuació de la transmissió de les fibres òptiques de polímer (POF) s'ha reduït considerablement. Els POF són avantatjosos per a les xarxes domèstiques, així com per a les interconnexions d'emmagatzematge, i tenen avantatges significatius per a moltes aplicacions de detecció, inclosos els límits de tensió elàstica alta, alta resistència a la fractura, alta flexibilitat en la flexió, alta sensibilitat a la tensió i potencials coeficients termoópticos negatius. Aquesta tesi va millorar la tecnologia d'irradiació amb làser per a POF i va investigar dispositius basats en xarxes difracció de Bragg (FBG) especials en POF per a comunicació òptica, microones, fotònica i detecció. En particular, desenvolupem la tecnologia de fabricació ràpida de FBG en POF amb un estudi detallat i l'optimització dels paràmetres per a la seua fabricació. Els punts destacats dels resultats inclouen un FBG uniforme de 8 dB amb un sol pols del làser Nd: YAG (266 nm) (8 ns) basat en fibra dopada amb BDK, que és el temps més curt reportat per a la fabricació de POF FBG. La irradiació de fibres òptiques de polímer utilitzant diferents materials sota el sistema de làser KrF a 248 nm va permetre demostrar un millor rendiment en comparació amb el sistema de làser Kimmon de 325 nm. A més, els FBG uniformes en el POF dopat amb TS d'índex escalonat es van aconseguir amb menys d'1 segon mitjançant la repetició de polsos de control i l'energia baixa de pols. Finalment, l'estudi de la irradiació d'energia de pols per a la fabricació de FBGs estables va permetre estalviar energia en el procés de fabricació de FBGs en POF, com un dels principals objectius de la producció en massa. Basant-nos en la tecnologia de fabricació millorada, ens centrem en la fabricació de diferents estructures de xarxes de difracció: es va fabricar un FBG amb desplaçament de fase utilitzant dos polsos de 15 ns a 248 nm KrF superposats pel mètode de Moiré; el primer FBG amb chirp sintonitzable es va aconseguir utilitzant un sol pols curt de làser, que va obrir les aplicacions basades en FBG amb chirp en POF; també es va proposar un nou mètode amb gradients tèrmics per a obtindre FBG en POF basat en FBG uniformes, i es va demostrar com la forma més convenient publicada fins hui per a aconseguir FBG POF estimulada; i, finalment, també s'han aconseguit xarxes de llarg període utilitzant un procés de fabricació de curt temps, especialment en comparació amb investigacions anteriors. Finalment, sobre la base dels dispositius de xarxes de difracció obtinguts al llarg d'aquest treball, s'han proposat diverses aplicacions potencials en aquesta tesi. De manera similar que per als FBG amb silici, el FBG amb chirp en POF té moltes aplicacions potencials en comunicacions òptiques i a l¿àrea de sensors. Aquest document descriu l'aplicació de detecció de tensió basada en FBG amb chirp sintonitzable en POF; a més, l'aplicació de detecció tèrmica en sistemes biomèdics; i el potencial dels dispositius de dispersió sintonitzables en les comunicacions òptiques, com per eixample a la compensació de dispersió o a la fotònica de microones.[EN] With the continuing development of material and fabrication technologies over the last three decades, the transmission attenuation of polymer optical fibers (POF) has been greatly decreased. POFs are advantageous for home networks as well as storage interconnections and have significant advantages for many sensing applications, including high elastic strain limits, high fracture toughness, high flexibility in bending, high sensitivity to strain and potential negative thermo-optic coefficients. This thesis improved the laser irradiation technology for POF and investigated special grating devices in POF for optical communication, microware photonics and sensing. In particular, we developed fast POF grating fabrication technology with a detailed study and optimization of the polymer optical fiber Bragg grating (POFBG) fabrication parameters. Highlights of the results include an 8 dB uniform POFBG with one single Nd:YAG (266nm) laser pulse (8 ns) based on BDK doped fiber, which is the shortest time ever reported for POFBG fabrication. The irradiation of polymer optical fibers using different materials under 248 nm KrF laser system allowed to demonstrate a better performance compared with 325 nm Kimmon laser system. Furthermore, uniform FBGs in step-index TS doped POF were achieved with less than 1 second by means of controlling pulse repetition and low pulse energy. Finally, the study of low UV pulse power irradiation for fabricating stable gratings allowed to save energy in the POF grating fabrication process, as one of the main goals for mass production. Based on the improved fabrication technology, we focused on the fabrication of different grating structures: a phase-shifted FBG was fabricated by using two 15 ns 248 nm KrF pulses overlapped by Moiré method; the first tunable chirped FBG was achieved by using a single laser short pulse, which opened the applications based on chirped POF BGs; also a novel thermal annealing method was proposed to obtain chirped POFBGs based on uniform FBGs, and proved as the ever published most convenient way to achieve chirped POFBG; and finally, long period gratings have been also achieved by using a short time fabrication process, specially when compared with previous research. Finally, based on the grating devices obtained throughout this work, several potential applications have been proposed in this thesis. Similarly, to silica chirped FBG, chirped FBG in POF have many potential applications in optical communications and sensing area. This document described the potential strain sensing application based on tunable chirped POFBG; also, the thermal detection application in bio-medical systems; and the potential of tunable dispersion devices in optical communications, i.e., dispersion compensation or microwave photonics.Min, R. (2019). Polymer optical fiber gratings for microwave photonics and communications application [Tesis doctoral no publicada]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/125473TESISCompendi

Fast and stable gratings inscription in POFs made of different materials with pulsed 248 nm KrF laser

"© 2018 Optical Society of America. One print or electronic copy may be made for personal use only. Systematic reproduction and distribution, duplication of any material in this paper for a fee or for commercial purposes, or modifications of the content of this paper are prohibited"[EN] This paper presents fiber Bragg grating (FBG) inscription with a pulsed 248 nm UV KrF laser in polymer optical fibers (POFs) made of different polymers, namely polymethyl methacrylate (PMMA), cyclic-olefin polymer and co-polymer, and Polycarbonate. The inscribed gratings and the corresponding inscription parameters are compared with grating inscribed in POFs made of the aforementioned materials but with the hitherto most used laser for inscription, which is a continuous wave 325 nm UV HeCd laser. Results show a reduction of the inscription time of at least 16 times. The maximum time reduction is more than 130 times. In addition, a reflectivity and a bandwidth close to or higher than the ones with the 325 nm laser were obtained. The polymer optical fiber Bragg gratings (POFBGs) inscribed with the 248 nm laser setup present high stability with small variations in their central wavelength, bandwidth, and reflectivity after 40 days. (c) 2018 Optical Society of America under the terms of the OSA Open Access Publishing Agreement.Fundacao para Ciencia e a Tecnologia (FCT) (SFRH/BPD/109458/2015, UID/EEA/50008/2013).Marques, C.; Min, R.; Leal-Junior, A.; Antunes, P.; Fasano, A.; Woyessa, G.; Nielsen, K.... (2018). Fast and stable gratings inscription in POFs made of different materials with pulsed 248 nm KrF laser. Optics Express. 26(2):2013-2022. https://doi.org/10.1364/OE.26.002013S20132022262Webb, D. J. (2015). Fibre Bragg grating sensors in polymer optical fibres. Measurement Science and Technology, 26(9), 092004. doi:10.1088/0957-0233/26/9/092004Prado, A. R., Leal-Junior, A. G., Marques, C., Leite, S., de Sena, G. L., Machado, L. C., … Pontes, M. J. (2017). Polymethyl methacrylate (PMMA) recycling for the production of optical fiber sensor systems. Optics Express, 25(24), 30051. doi:10.1364/oe.25.030051Hu, X., Saez-Rodriguez, D., Marques, C., Bang, O., Webb, D. J., Mégret, P., & Caucheteur, C. (2015). Polarization effects in polymer FBGs: study and use for transverse force sensing. Optics Express, 23(4), 4581. doi:10.1364/oe.23.004581Pospori, A., Marques, C. A. F., Bang, O., Webb, D. J., & André, P. (2017). Polymer optical fiber Bragg grating inscription with a single UV laser pulse. Optics Express, 25(8), 9028. doi:10.1364/oe.25.009028Marques, C. A. F., Webb, D. J., & Andre, P. (2017). Polymer optical fiber sensors in human life safety. Optical Fiber Technology, 36, 144-154. doi:10.1016/j.yofte.2017.03.010Fasano, A., Woyessa, G., Janting, J., Rasmussen, H. K., & Bang, O. (2017). Solution-Mediated Annealing of Polymer Optical Fiber Bragg Gratings at Room Temperature. IEEE Photonics Technology Letters, 29(8), 687-690. doi:10.1109/lpt.2017.2678481Woyessa, G., Pedersen, J. K. M., Fasano, A., Nielsen, K., Markos, C., Rasmussen, H. K., & Bang, O. (2017). Zeonex-PMMA microstructured polymer optical FBGs for simultaneous humidity and temperature sensing. Optics Letters, 42(6), 1161. doi:10.1364/ol.42.001161Fasano, A., Woyessa, G., Stajanca, P., Markos, C., Stefani, A., Nielsen, K., … Bang, O. (2016). Fabrication and characterization of polycarbonate microstructured polymer optical fibers for high-temperature-resistant fiber Bragg grating strain sensors. Optical Materials Express, 6(2), 649. doi:10.1364/ome.6.000649Woyessa, G., Nielsen, K., Stefani, A., Markos, C., & Bang, O. (2016). Temperature insensitive hysteresis free highly sensitive polymer optical fiber Bragg grating humidity sensor. Optics Express, 24(2), 1206. doi:10.1364/oe.24.001206Leal-Junior, A. G., Frizera, A., & José Pontes, M. (2018). Sensitive zone parameters and curvature radius evaluation for polymer optical fiber curvature sensors. Optics & Laser Technology, 100, 272-281. doi:10.1016/j.optlastec.2017.10.006Stefani, A., Andresen, S., Yuan, W., Herholdt-Rasmussen, N., & Bang, O. (2012). High Sensitivity Polymer Optical Fiber-Bragg-Grating-Based Accelerometer. IEEE Photonics Technology Letters, 24(9), 763-765. doi:10.1109/lpt.2012.2188024Marques, C. A. F., Peng, G.-D., & Webb, D. J. (2015). Highly sensitive liquid level monitoring system utilizing polymer fiber Bragg gratings. Optics Express, 23(5), 6058. doi:10.1364/oe.23.006058Jensen, J. B., Hoiby, P. E., Emiliyanov, G., Bang, O., Pedersen, L. H., & Bjarklev, A. (2005). Selective detection of antibodies in microstructured polymer optical fibers. Optics Express, 13(15), 5883. doi:10.1364/opex.13.005883Emiliyanov, G., Høiby, P., Pedersen, L., & Bang, O. (2013). Selective Serial Multi-Antibody Biosensing with TOPAS Microstructured Polymer Optical Fibers. Sensors, 13(3), 3242-3251. doi:10.3390/s130303242Hassan, H. U., Janting, J., Aasmul, S., & Bang, O. (2016). Polymer Optical Fiber Compound Parabolic Concentrator fiber tip based glucose sensor: in-Vitro Testing. IEEE Sensors Journal, 1-1. doi:10.1109/jsen.2016.2606580Yuan, W., Khan, L., Webb, D. J., Kalli, K., Rasmussen, H. K., Stefani, A., & Bang, O. (2011). Humidity insensitive TOPAS polymer fiber Bragg grating sensor. Optics Express, 19(20), 19731. doi:10.1364/oe.19.019731Johnson, I. P., Yuan, W., Stefani, A., Nielsen, K., Rasmussen, H. K., Khan, L., … Bang, O. (2011). Optical fibre Bragg grating recorded in TOPAS cyclic olefin copolymer. Electronics Letters, 47(4), 271. doi:10.1049/el.2010.7347Markos, C., Stefani, A., Nielsen, K., Rasmussen, H. K., Yuan, W., & Bang, O. (2013). High-T_g TOPAS microstructured polymer optical fiber for fiber Bragg grating strain sensing at 110 degrees. Optics Express, 21(4), 4758. doi:10.1364/oe.21.004758Woyessa, G., Fasano, A., Stefani, A., Markos, C., Nielsen, K., Rasmussen, H. K., & Bang, O. (2016). Single mode step-index polymer optical fiber for humidity insensitive high temperature fiber Bragg grating sensors. Optics Express, 24(2), 1253. doi:10.1364/oe.24.001253Woyessa, G., Fasano, A., Markos, C., Stefani, A., Rasmussen, H. K., & Bang, O. (2016). Zeonex microstructured polymer optical fiber: fabrication friendly fibers for high temperature and humidity insensitive Bragg grating sensing. Optical Materials Express, 7(1), 286. doi:10.1364/ome.7.000286Stefani, A., Nielsen, K., Rasmussen, H. K., & Bang, O. (2012). Cleaving of TOPAS and PMMA microstructured polymer optical fibers: Core-shift and statistical quality optimization. Optics Communications, 285(7), 1825-1833. doi:10.1016/j.optcom.2011.12.033Nielsen, K., Rasmussen, H. K., Adam, A. J., Planken, P. C., Bang, O., & Jepsen, P. U. (2009). Bendable, low-loss Topas fibers for the terahertz frequency range. Optics Express, 17(10), 8592. doi:10.1364/oe.17.008592Nielsen, K., Rasmussen, H. K., Jepsen, P. U., & Bang, O. (2010). Broadband terahertz fiber directional coupler. Optics Letters, 35(17), 2879. doi:10.1364/ol.35.002879Anthony, J., Leonhardt, R., Argyros, A., & Large, M. C. J. (2011). Characterization of a microstructured Zeonex terahertz fiber. Journal of the Optical Society of America B, 28(5), 1013. doi:10.1364/josab.28.001013Woyessa, G., Fasano, A., Markos, C., Rasmussen, H. K., & Bang, O. (2017). Low Loss Polycarbonate Polymer Optical Fiber for High Temperature FBG Humidity Sensing. IEEE Photonics Technology Letters, 29(7), 575-578. doi:10.1109/lpt.2017.2668524Johnson, I. P., Kalli, K., & Webb, D. J. (2010). 827 nm Bragg grating sensor in multimode microstructured polymer optical fibre. Electronics Letters, 46(17), 1217. doi:10.1049/el.2010.1595Stefani, A., Wu Yuan, Markos, C., & Bang, O. (2011). Narrow Bandwidth 850-nm Fiber Bragg Gratings in Few-Mode Polymer Optical Fibers. IEEE Photonics Technology Letters, 23(10), 660-662. doi:10.1109/lpt.2011.2125786Hu, X., Pun, C.-F. J., Tam, H.-Y., Mégret, P., & Caucheteur, C. (2014). Highly reflective Bragg gratings in slightly etched step-index polymer optical fiber. Optics Express, 22(15), 18807. doi:10.1364/oe.22.018807Hu, X., Pun, C.-F. J., Tam, H.-Y., Mégret, P., & Caucheteur, C. (2014). Tilted Bragg gratings in step-index polymer optical fiber. Optics Letters, 39(24), 6835. doi:10.1364/ol.39.006835Sáez-Rodríguez, D., Nielsen, K., Rasmussen, H. K., Bang, O., & Webb, D. J. (2013). Highly photosensitive polymethyl methacrylate microstructured polymer optical fiber with doped core. Optics Letters, 38(19), 3769. doi:10.1364/ol.38.003769Hu, X., Woyessa, G., Kinet, D., Janting, J., Nielsen, K., Bang, O., & Caucheteur, C. (2017). BDK-doped core microstructured PMMA optical fiber for effective Bragg grating photo-inscription. Optics Letters, 42(11), 2209. doi:10.1364/ol.42.002209Statkiewicz-Barabach, G., Kowal, D., Mergo, P., & Urbanczyk, W. (2015). Comparison of growth dynamics and temporal stability of Bragg gratings written in polymer fibers of different types. Journal of Optics, 17(8), 085606. doi:10.1088/2040-8978/17/8/085606Marques, C., Pospori, A., Demirci, G., Çetinkaya, O., Gawdzik, B., Antunes, P., … Webb, D. (2017). Fast Bragg Grating Inscription in PMMA Polymer Optical Fibres: Impact of Thermal Pre-Treatment of Preforms. Sensors, 17(4), 891. doi:10.3390/s17040891Bundalo, I.-L., Nielsen, K., Markos, C., & Bang, O. (2014). Bragg grating writing in PMMA microstructured polymer optical fibers in less than 7 minutes. Optics Express, 22(5), 5270. doi:10.1364/oe.22.005270Oliveira, R., Bilro, L., & Nogueira, R. (2015). Bragg gratings in a few mode microstructured polymer optical fiber in less than 30 seconds. Optics Express, 23(8), 10181. doi:10.1364/oe.23.010181Lacraz, A., Polis, M., Theodosiou, A., Koutsides, C., & Kalli, K. (2015). Femtosecond Laser Inscribed Bragg Gratings in Low Loss CYTOP Polymer Optical Fiber. IEEE Photonics Technology Letters, 27(7), 693-696. doi:10.1109/lpt.2014.2386692Theodosiou, A., Lacraz, A., Stassis, A., Koutsides, C., Komodromos, M., & Kalli, K. (2017). Plane-by-Plane Femtosecond Laser Inscription Method for Single-Peak Bragg Gratings in Multimode CYTOP Polymer Optical Fiber. Journal of Lightwave Technology, 35(24), 5404-5410. doi:10.1109/jlt.2017.2776862Yuan, W., Stefani, A., Bache, M., Jacobsen, T., Rose, B., Herholdt-Rasmussen, N., … Bang, O. (2011). Improved thermal and strain performance of annealed polymer optical fiber Bragg gratings. Optics Communications, 284(1), 176-182. doi:10.1016/j.optcom.2010.08.069Bundalo, I.-L., Nielsen, K., Woyessa, G., & Bang, O. (2017). Long-term strain response of polymer optical fiber FBG sensors. Optical Materials Express, 7(3), 967. doi:10.1364/ome.7.00096

3-D Multifunctional Sensors Fabricated on Fiber Tips Using a Two-Photon Polymerization Process

This thesis conducts research involving designing, fabricating, and testing optical fiber tip refractive index sensors. The fabrication process used for these sensors is a two-photon polymerization process utilizing a photo sensitive polymer. Unlike planar lithography, this fabrication process allows the creation of arbitrary shapes with a great degree of freedom. Three different fiber tip sensors were fabricated and tested. The first is a flat surfaced single cavity Fabry-Pérot interferometer (FPI) device, the second is a flat surfaced double cavity FPI device, and the final is a confocal surfaced double cavity FPI device. These sensors are tested for thermal radiation and volatile organic compounds (VOC) sensing. Thermal radiation sensing involves exposing the fiber tip device to temperatures ranging from room temperature up to 120oC. As the temperature increases, the fiber tip structure expands which changes its reflection spectrum. For VOC sensing each device was also exposed to isopropanol in gaseous form which results in a refractive index change. This change is also observed in the reflection spectrum. Lastly, research was conducted on thin dielectric reflective coatings for the purpose of increasing the reflectivity of the device surfaces resulting in a higher quality factor

Fiber-Optic Temperature Sensor Using a Thin-Film Fabry-Perot Interferometer

A fiber-optic temperature sensor was developed that is rugged, compact, stable, and can be inexpensively fabricated. This thin-film interferometric temperature sensor was shown to be capable of providing a +/- 2 C accuracy over the range of -55 to 275 C, throughout a 5000 hr operating life. A temperature-sensitive thin-film Fabry-Perot interferometer can be deposited directly onto the end of a multimode optical fiber. This batch-fabricatable sensor can be manufactured at a much lower cost than can a presently available sensor, which requires the mechanical attachment of a Fabry-Perot interferometer to a fiber. The principal disadvantage of the thin-film sensor is its inherent instability, due to the low processing temperatures that must be used to prevent degradation of the optical fiber's buffer coating. The design of the stable thin-film temperature sensor considered the potential sources of both short and long term drifts. The temperature- sensitive Fabry-Perot interferometer was a silicon film with a thickness of approx. 2 microns. A laser-annealing process was developed which crystallized the silicon film without damaging the optical fiber. The silicon film was encapsulated with a thin layer of Si3N4 over coated with aluminum. Crystallization of the silicon and its encapsulation with a highly stable, impermeable thin-film structure were essential steps in producing a sensor with the required long-term stability

Novos dispositivos e técnicas para tecnologias de comunicações e sensores

Doutoramento em Engenharia FísicaHoje em dia, a tecnologia de fibra óptica está a ser amplamente usada nas áreas de telecomunicações e sensores. Historicamente, as qualidades das fibras ópticas poliméricas (POFs) têm sido menosprezadas devido à popularidade das fibras óticas de vidro. Tal facto advém maioritariamente da sua elevada atenuação. No entanto, os materiais que compõem as POFs têm vindo a melhorar significativamente nestes últimos anos. Nesse sentido, a emergência de novas técnicas e dispositivos têm vindo a ser demonstradas/os. Considerando o campo das telecomunicações, as POFs estão a crescer rapidamente em aplicações de redes de acesso. Além disso, o advento da operação monomodo e das redes de Bragg em POF estão a ser amplamente explorados em aplicações de sensores e portanto, este tipo de tecnologia tenderá a ser uma realidade num futuro próximo. Devido à necessidade de criar uma conexão de baixa perda entre fibra óptica de vidro e polimérica, será demonstrada uma nova técnica capaz de produzir terminais de POF de alta qualidade, num processo rápido, fácil e semiautomático. A conectorização destes tipos de fibras será também analisada nesta dissertação. No seguimento desta tese serão desenvolvidos dois sistemas de gravação de redes de Bragg em POF. Num dos sistemas será usado o tradicional laser de HeCd com operação nos 325 nm, sendo que noutro será usado o laser de KrF com operação nos 248 nm. Os resultados mostrarão a capacidade de gravar redes de Bragg em POF em apenas alguns segundos, contrariamente às várias dezenas de minutos necessários com o laser de 325 nm. Com base no sucesso dos resultados, o sistema de gravação que opera nos 248 nm será usado para fabricar redes de Bragg noutros tipos de fibras, incluindo as de índice em degrau, micro-estruturadas e sem bainha. A gravação de redes de Bragg de excelente qualidade em POFs de elevada birrefringência também será apresentada. A separação entre picos de ressonância irá ser usada para estimar a birrefringência de fase, que será então comparada com a obtida por simulações numéricas e com recurso ao método de varredura de comprimento de onda. As redes de Bragg produzidas pelos métodos anteriores serão então caracterizadas à deformação, temperatura, pressão, humidade e índice de refracção. Os resultados serão comparados com a literatura e com aqueles encontrados teoricamente. Um dispositivo de interferência multimodal feito pela conexão de duas fibras ópticas monomodo de vidro a uma fibra óptica multimodo de polímero, será usado para demonstrar a medição de deformação e temperatura. As capacidades de absorção de água, oferecidas pelo material à base de polimetilmetacrilato serão usadas para medir humidade. No final desta dissertação, um sensor híbrido composto por um dispositivo de interferência multimodal, baseado em POF e contendo uma rede de Bragg, demonstrará a capacidade de medir deformação, temperatura e índice de refracção. A propriedades de baixa absorção de água por parte do material que compõe a fibra polimérica será usada para demonstrar insensibilidade à humidade por parte do sensor.Nowadays, fiber optic technology is being widely employed in communication and sensing areas. Historically, the qualities of polymer optical fibers (POFs) have been overwhelmed by the popularity of the silica optical fibers. This has been mainly due to the POFs higher transmission loss. However, in last years, POF materials are improving their performance. Therefore, the emergence of new devices and techniques have been demonstrated. Considering the communications field, POFs are growing rapidly in fiber to the home applications. Additionally, the advent of single mode operation and fiber Bragg gratings in POFs are being widely explored in several sensing applications. Consequently, this technology will tend to be a reality in a near future. Due to the need of a low loss connection between silica and polymer optical fibers, it will be demonstrated a new technique capable to produce POF terminals of high quality in an easy, fast and semi-automated process. The connectorization of these types of fibers will be then analysed in this dissertation. The development of two Bragg grating inscription systems for POFs will also be explored in this thesis. One of the systems will employ the traditional HeCd laser operating at 325 nm, while the other will use the KrF laser operating at 248 nm. Results will show the capability to write Bragg gratings in a POF in few seconds, contrary to the several tens of minutes reported for the 325 nm radiation. Based on the success of the results, the 248 nm inscription setup will be used to inscribe Bragg gratings in other types of POFs, including step-index, microstructured, and unclad POFs. The inscription of a high quality Bragg grating in a high-birefringence POF will also be presented and the phase birefringence arising from the Bragg peak separation will be compared with the numerical simulations togheter with the wavelength scanning method. The fiber Bragg gratings produced through the previous methods will be characterized to strain temperature, pressure, humidity and refractive index. Results will be compared with literature and with the ones found theoretically. A multimode interference device made by sandwiching a multimode POF between two single mode silica fibers will be used to demonstrate the ability to measure strain and temperature. The water absorption capabilities offered by the polymethylmethacrylate material will be used to measure humidity. At the end of this dissertation, a hybrid sensor composed of a POF based multimode interference device, comprising a fiber Bragg grating, will demonstrate the capability to measure strain, temperature and refractive index. The low water absorption properties of the material that composes the POF will be used to demonstrate a POF sensor with humidity insensitiveness

A review of single-mode fiber optofluidics

We review the field we describe as “single-mode fiber optofluidics” which combines the technologies of microfluidics with single-mode fiber optics for delivering new implementations of well-known single-mode optical fiber devices. The ability of a fluid to be easily shaped to different geometries plus the ability to have its optical properties easily changed via concentration changes or an applied electrical or magnetic field offers potential benefits such as no mechanical moving parts, miniaturization, increased sensitivity and lower costs. However, device fabrication and operation can be more complex than in established single-mode fiber optic devices

Refractometer based on fiber Bragg grating Fabry-Pérot cavity embedded with a narrow microchannel

We report on inscription of microchannels of different widths in optical fiber using femtosecond (fs) laser inscription assisted chemical etching and the narrowest channel has been created with a width down to only 1.2µm. Microchannels with 5µm and 35µm widths were fabricated together with Fabry-Pérot (FP) cavities formed by UV laser written fiber Bragg gratings (FBGs), creating high function and linear response refractometers. The device with a 5µm microchannel has exhibited a refractive index (RI) detection range up to 1.7, significantly higher than all fiber grating RI sensors. In addition, the microchannel FBG FP structures have been theoretically simulated showing excellent agreement with experimental measured characteristics