Preparation and magnetoresistance of Ag 2+x Se thin films deposited via Pulsed Laser Deposition

The preparation of Ag 2+x Se thin films with thicknesses between 4 nm and 3000 nm by pulsed laser deposition on single crystalline NaCl and MgO substrates is reported. The films are perfectly dense and show a good lateral uniformity with a small number of defects. The microstructure of the films corresponds to a nanoparquet, being composed of two different phases of silver selenide. One phase is identified as the Naumannite low temperature phase of silver selenide, the structure of the other phase has not been reported in detail before and probably represents a metastable phase. Silver-rich films contain silver precipitates with typical sizes on the nanoscale. Their presence and their size appears to be responsible for the large and linear magnetoresistance effect of silver-rich silver selenide

Extraordinary Magnetoresistance in Hybrid Semiconductor-Metal Systems

We show that extraordinary magnetoresistance (EMR) arises in systems consisting of two components; a semiconducting ring with a metallic inclusion embedded. The im- portant aspect of this discovery is that the system must have a quasi-two-dimensional character. Using the same materials and geometries for the samples as in experiments by Solin et al.[1;2], we show that such systems indeed exhibit a huge magnetoresistance. The magnetoresistance arises due to the switching of electrical current paths passing through the metallic inclusion. Diagrams illustrating the flow of the current density within the samples are utilised in discussion of the mechanism responsible for the magnetoresistance effect. Extensions are then suggested which may be applicable to the silver chalcogenides. Our theory offers an excellent description and explanation of experiments where a huge magnetoresistance has been discovered[2;3].Comment: 12 Pages, 5 Figure

Nanoindentation of Bridgman YBCO samples

In this study, the mechanical properties of YBa2Cu3O7−x, obtained by the Bridgman technique, were examined using a Berkovich tip indenter on the basal plane (0 0 1). Intrinsic hardness was measured by nanoindentation tests and corrected using the Nix and Gao model for this material. Furthermore, Vickers hardness tests were performed, in order to determine the possible size effect on these measurements. The results showed an underestimation of the hardness value when the tests were performed with large loads. Moreover, the elastic modulus of the Bridgman samples was 128 ± 5 GPa. Different residual imprints were visualised by atomic force microscopy and a focused ion beam, in order to observe superficial and internal fracturing. Mechanical properties presented a considerable reduction at the interface. This effect could be attributed to internal stress generated during the texturing process. In order to corroborate this hypothesis, an observation using transmission electron microscopy was performed

Development of eddy current probes based on magnetoresistive sensors arrays

Conference of 40th Annual Review of Progress in Quantitative Nondestructive Evaluation, QNDE 2013, Incorporating the 10th International Conference on Barkhausen and Micro-Magnetics, ICBM 2013 ; Conference Date: 21 July 2013 Through 26 July 2013; Conference Code:105840International audienceEddy Current Technique is a powerful method for detection of surface notches and of buried flaws during inspection of metallic parts. Recent EC array probes have demonstrated a fast and efficient control of large surfaces. Nevertheless, when the size of flaws decreases or the defect is rather deep, traditional winding coil probes turn out to be useless. Magnetoresistive sensors present the advantages of flat frequency response and micron size. These sensors are hence very attractive for the detection of buried defects that require low frequencies because of skin depth effect. An optimization of the probe with magnetoresistive sensors as receivers has been made by simulations using CIVA software and finite elements methods with OPERA. EC probes for buried flaw detection have been designed. Experimental results have been compared with simulations

Evaluation of High Spatial Resolution Imaging of Magnetic Stray Fields for Early Damage Detection

Metal magnetic memory (MMM) technique with associated ISO 24497-1:3 [1] is gaining considerable interest in the magnetic NDT community. In contrast to traditional Magnetic Flux Leakage (MFL) testing, the inspection objects are not intentionally magnetized by an external magnetic field [1,2]. Due to the physical coupling between mechanical stress and magnetization of ferromagnetic materials [3], it is assumed that the distribution of the residual MFL correspond to the internal stress of the specimen [2,4], or in the most general sense, to a degradation of the material [1,2]. Usually, MMM measurements are performed by relatively bulky magnetic inspection sensors [2]. The evaluation of local magnetic field distribution is limited thereby. High precision GMR (Giant Magneto Resistance) measurements in the micrometer regime can provide a higher degree of information due to better spatial resolution [5]. We present a concise summary of studies on the correlation of magnetic structure and microstructure of steels. In particular, we compare residual stress measurements in S235JRC steel welds by means of neutron diffraction with high resolution magnetic field mappings. Results indicate a qualitative correlation between residual stresses and local stray field variation. In addition, stray field measurements of plastically deformed specimens for quasi- static and cyclic loading cases are discussed. The present study concludes that GMR sensors can detect inhomogeneous plastic deformations of S235JR steel in a very early stage, without specific signal processing according to the ISO 24497-1:3

Residual Stress Characterization of Steel TIG Welds by Neutron Diffraction and by Residual Magnetic Stray Field Mappings

The residual stress distribution of tungsten inert gas welded S235JRC C plates was determined by means of neutron diffraction. This investigation leads to the discovery of dominating longitudinal residual stresses with maxima around View the MathML source600MPa. With these results as reference, the evaluation of residual stress with high spatial resolution GMR giant magneto resistance sensors is discussed. The experiments performed indicate an interdependence of residual stress changes and the normal component of local residual magnetic stray fields. Spatial variations in the magnetic field strength perpendicular to the welds are in the order of the magnetic field of the eart

Influence of the Microstructure on Magnetic Stray Fields of Low Carbon Steel Welds

This study examines the relationship between the magnetic mesostructure with the microstructure of low carbon steel tungsten inert gas welds. Optical microscopy revealed variation in the microstructure of the parent material, in the heat affected and fusion zones, correlating with distinctive changes in the local magnetic stray fields measured with high spatial resolution giant magneto resistance sensors. In the vicinity of the heat affected zone high residual stresses were found using neutron diffraction. Notably, the gradients of von Mises stress and triaxial magnetic stray field modulus follow the same tendency transverse to the weld. In contrast, micro X ray fluorescence characterization indicated that local changes in element composition had no independent effect on magnetic stray field