Water and Air Redistribution within a Dual Permeability Porous System Investigated Using Neutron Imaging

AbstractA ponded infiltration experiment was conducted under simultaneous imaging to investigate variations in quasi-saturated hydraulic conductivity a process frequently observed in infiltration experiments in soils with wide grain -size distribution. An artificially prepared heterogeneous sample composed of coarse quartz sand (representing pathways of preferential flow) and fine porous ceramic (representing soil matrix) was investigated. The sample was 34.5mm high and 29.0mm in diameter. Sequences of neutron radiography images (RI) of pixel size 0.045 × 0.045mm were taken at one angle during particular transient phases of the flow process. During quasi-steady state flow stages of the experiment radiography images were acquired in range of angles 0-180° in 0.9° step and. 3D neutron tomograms (TI) were then developed. Using the data a quantitative evaluation of the spatial and temporal distribution of water content within the sample was conducted. For every RI and TI the amount of water in particular pixels and voxels, respectively, was calculated by subtracting the image of dry sample. The accuracy of the water content estimates derived from the images was checked by comparing them to the corresponding gravimetrically determined water content data. Heavy water with equilibrium air saturation was introduced into the sample during two recurrent infiltrations. Thirty five hours later, during second infiltration, the inflow was switched to degassed heavy water in order to remove residual air present in the sample. During the first twelve hours of first infiltration run flow rate through the sample decreased from 3.7cm/hour to 1.0cm/hour at the end of the “steady state flow” stage. The flow rate in second run decreased from 3.6cm/hour to 1.6cm/hour. Comparison of the tomogram of the sample at the beginning and one taken at the end of the steady state flow stage in each run shows an increase of water content in the porous ceramic, while the water content in the coarse sand decreased. On the contrary, during the subsequent infiltration with degassed water the flow rate increased to its maximum value of 10.5cm/hour. The tomograms confirmed removal of the residual air during this stage. Increased water content in the coarse quartz sand was evident on a tomogram made at the end of the degassed water infiltration. The results show that the residual air saturation and its spatial distribution strongly affected the water flow in the quasi-saturated heterogeneous media representing natural soil

On-line monitoring of hygroscopicity and dimensional changes of wood during thermal modification by means of neutron imaging methods

European beech (Fagus sylvatica L.) and Norway spruce [Picea abies (L.) Karst.] have been thermally modified in a combined air-steam atmosphere between 70°C and 150°C and pressures up to 4 bar, and the changes of dimensions and moisture contents (MC) of the samples were studied in-situ by means of neutron imaging (NI). This non-invasive testing method offers unique opportunities. NI is highly sensitive for hydrogen and thus well suited for monitoring the MC changes, although some metals (e.g., Al), indispensable for sample environments under high temperature and pressure, are practically transparent to neutrons. The results show that the modification induced changes of MC and dimensions both in radial and tangential direction can well be determined by NI. Dimensional changes from water saturation to oven-dry state, the sorption isotherms, and the differential swelling were observed. Additionally, the sorption behaviour at 20°C was investigated after thermal modification and colour measurements were carried out before and after the thermal treatment

Geographical variation in orthopedic procedures in Norway: Cross-sectional population-based study

Background: Standardized surgery rates for common orthopedic procedures vary across geographical areas in Norway. We explored whether area-level factors related to demand and supply in publicly funded healthcare are associated with geographical variation in surgery rates for six common orthopedic procedures. Methods: The present study is a cross-sectional population-based study of hospital referral areas in Norway. We included adult admissions for arthroscopy for degenerative knee disease, arthroplasty for osteoarthritis of the knee and hip, surgical treatment for hip fracture, and decompression with/without fusion for lumbar disk herniation and lumbar spinal stenosis in 2012–2016. Variation in age and sex standardized rates was estimated using extremal quotients, coefficients of variation, and systematic components of variation (SCV). Associations between surgery rates and the socioeconomic factors urbanity, unemployment, low-income, high level of education, mortality, and number of surgeons and hospitals were explored with linear regression analyses. Results: Knee arthroscopy showed highest level of variation (SCV 10.3) and decreased in numbers. Variation was considerable for spine surgery (SCV 3.8–4.9), moderate to low for arthroplasty procedures (SCV 0.8–2.6), and small for hip fracture surgery (SCV 0.2). Higher rates of knee arthroscopy were associated with more orthopedic surgeons (adjusted coefficient 24.8, 95% confidence interval (CI): 2.7–47.0), and less urban population (adjusted coefficient −13.3, 95% CI: −25.4 to −1.2). Higher spine surgery rates were associated with more hospitals (adjusted coefficient 22.4, 95% CI: 4.6–40.2), more urban population (adjusted coefficient 2.1, 95% CI: 0.4–3.8), and lower mortality (adjusted coefficient −192.6, 95% CI: −384.2 to −1.1). Rates for arthroplasty and hip fracture surgery were not associated with supply/demand factors included. Conclusions: Arthroscopy for degenerative knee disease decreased in line with guidelines, but showed high variation of surgery rates. Socioeconomic factors included in this study did not explain geographical variation in orthopedic surgery.publishedVersio

New insights into early bronze age damascene technique north of the alps

Damascening, defined in this context as the inlay of one metal into a different metal base, is a rare decorative technique in the Early Bronze Age, known only from seven bronze artefacts found north of the Alps. This paper reports on the first thorough scientific examination of one such find, the axe from Thun-Renzenbühl grave no. 1. This interdisciplinary project involving several institutions in Germany and Switzerland investigated the axe by means of neutron radiographic imaging and X-ray microprobe methods, supported by microscopic examination. The result is an attempt to reconstruct the fabrication and decoration process and to reconsider the enigmatic question of the origins of the damascene technique north of the Alp

Durability of the Indian Kandla Grey sandstone under Western European climatic conditions

An increasing amount of imported natural building stones are being used in Western Europe, often as a replacement of more traditional, local building stones. Unlike for these traditional stones, which have been used under the prevailing climatic conditions in Western Europe, the durability of these imported stones is largely unknown. Therefore, it is essential to study their behaviour under these climatic conditions in order to predict their weathering resistance. The chemical and structural properties of these new building materials need to be determined and their behaviour under changing environmental conditions needs to be studied. When these materials are being used in Western Europe, they have to resist to significant mechanical stresses due to the imbibition of de-icing salt solutions. These de-icing salts are very frequently used during winter in Western Europe, while temperature fluctuates between freezing and thaw conditions. In this research, focus has been laid on the multi-disciplinary characterization of the compact Kandla Grey layered sandstone. This stone is recently frequently imported from India to Belgium. Besides traditional techniques, (according to European Standars for natural stone testing) highly advanced research techniques such as µ-XRF and HRXCT were used to characterize and monitor the changes under different external conditions such as freezing, thawing and salt crystallization. The results of this study demonstrate that the structural properties of the laminations inside Kandla Grey have an influence on the resistance of the stone to frost and salt weathering. Based on these results, it can be concluded that Kandla Grey can be vulnerable to these types of weathering under the current climatic conditions in Western Europe

Development of a Real-Time PCR for Identification of Brachyspira Species in Human Colonic Biopsies

Background: Brachyspira species are fastidious anaerobic microorganisms, that infect the colon of various animals. The genus contains both important pathogens of livestock as well as commensals. Two species are known to infect humans: B. aalborgi and B. pilosicoli. There is some evidence suggesting that the veterinary pathogenic B. pilosicoli is a potential zoonotic agent, however, since diagnosis in humans is based on histopathology of colon biopsies, species identification is not routinely performed in human materials. Methods: The study population comprised 57 patients with microscopic evidence of Brachyspira infection and 26 patients with no histopathological evidence of Brachyspira infection. Concomitant faecal samples were available from three infected patients. Based on publically available 16S rDNA gene sequences of all Brachyspira species, species-specific primer sets were designed. DNA was extracted and tested by real-time PCR and 16S rDNA was sequenced. Results: Sensitivity and specificity for identification of Brachyspira species in colon biopsies was 100% and 87.7% respectively. Sequencing revealed B. pilosicoli in 15.4% of patients, B. aalborgi in 76.9% and a third species, tentatively named ‘‘Brachyspira hominis’’, in 26.2%. Ten patients (12.3%) had a double and two (3.1%) a triple infection. The presence of Brachyspira pilosicoli was significantly associated with inflammatory changes in the colon-biopsy (p = 0.028). Conclusions: This newly designed PCR allows for sub-differentiation of Brachyspira species in patient material and thus allows large-scaled surveillance studies to elucidate the pathogenicity of human Brachyspira infections. One-third of affected patients appeared to be infected with a novel species

A QUANTITATIVE EVALUATION OF THE WATER DISTRIBUTION IN A SOIL SAMPLE USING NEUTRON IMAGING

This paper presents an empirical method by Kang et al. recently proposed for correcting two-dimensional neutron radiography for water quantification in soil. The method was tested on data from neutron imaging of the water infiltration in a soil sample. The raw data were affected by neutron scattering and by beam hardening artefacts. Two strategies for identifying the correction parameters are proposed in this paper. The method has been further developed for the case of three-dimensional neutron tomography. In a related experiment, neutron imaging is used to record ponded-infiltration experiments in two artificial soil samples. Radiograms, i.e., two-dimensional projections of the sample, were acquired during infiltration. A calculation was made of the amount of water and its distribution within the radiograms, in the form of two-dimensional water thickness maps. Tomograms were reconstructed from the corrected and uncorrected water thickness maps to obtain the 3D spatial distribution of the water content within the sample. Without the correction, the beam hardening and the scattering effects overestimated the water content values close to the perimeter of the sample, and at the same time underestimated the values close to the centre of the sample. The total water content of the entire sample was the same in both cases. The empirical correction method presented in this study is a relatively accurate, rapid and simple way to obtain the quantitatively determined water content from two-dimensional and three-dimensional neutron images. However, an independent method for measuring the total water volume in the sample is needed in order to identify the correction parameters

Neutron imaging and digital volume correlation to analyse the coupled hydro-mechanics of geomaterials

A new approach to characterise the evolution and coupling of deformation and fluid flow in geomaterials is presented. The method exploits some key features of neutrons, namely penetration of dense materials used for triaxial pressure cells, sensitivity to hydrogen and the possibility to distinguish hydrogen from its isotope deuterium (in normal water, H2O, and heavy water, D2O, respectively). Illustration of the approach is provided with results from a combined fluid flow/triaxial compression test on a cemented sand specimen performed in-situ (i.e., acquiring images during loading) at a neutron imaging station. Quantitative analysis of neutron tomography images acquired at different stages of deformation is made by Digital Volume Correlation to provide full 3D strain fields that highlight the evolution of localised deformation features. Spatio-temporal tracking of the effect of the evolution of the permeability in the sample was possible by neutron radiographies acquired during pressure driven flow of H2O into the sample saturated with D2O. By exploiting the H2O/D2O neutron transmission contrast and similarities of their flow behaviour, the tracking of the H2O/D2O front can be considered as an indicator of the permeability of the sample that is correlated to the measured evolution of the deformation

Neutron imaging of rock mechanics experiments

Understanding the mechanical behaviour of porous rocks and how this influences the fluid flow is key in a number of resource engineering challenges, in particular hydrocarbon production and CO2 sequestration. Deformation in these porous materials is, in general, not homogeneous, as deformation localises into narrow shear or compaction bands, which might then evolve into fractures. These local deformation features can act as barriers or conduits for fluid flow, depending on their evolution and resultant properties. This work focusses on achieving quantitative understanding of how localised deformation (shear or compaction bands and fractures) can change (local and global) permeability in porous rocks. In particular the aim is to overcome limitations of traditional methods for permeability measurement, which consider bulk sample measurements, and do not provide a good understanding of the permeability variations in the presence of material heterogeneity, e.g., localised deformations. Better understanding of the controlling factors on permeability evolution due to localised deformation requires mapping of the full permeability and strain fields through test specimens. Neutron tomography, in combination with 3D-volumetric Digital Image Correlation (3DDIC) is used to measure deformation and fast neutron radiography is used to visualise fluid-flow through the characterised deformed samples