Laboratory observations of permeability enhancement by fluid pressure oscillation of in situ fractured rock

We report on laboratory experiments designed to investigate the influence of pore pressure oscillations on the effective permeability of fractured rock. Berea sandstone samples were fractured in situ under triaxial stresses of tens of megapascals, and deionized water was forced through the incipient fracture under conditions of steady and oscillating pore pressure. We find that short-term pore pressure oscillations induce long-term transient increases in effective permeability of the fractured samples. The magnitude of the effective permeability enhancements scales with the amplitude of pore pressure oscillations, and changes persist well after the stress perturbation. The maximum value of effective permeability enhancement is 5 × 10^(−16) m^2 with a background permeability of 1 × 10^(−15) m^2; that is, the maximum enhanced permeability is 1.5 × 10^(−15) m^2. We evaluate poroelastic effects and show that hydraulic storage release does not explain our observations. Effective permeability recovery following dynamic oscillations occurs as the inverse square root of time. The recovery indicates that a reversible mechanism, such as clogging/unclogging of fractures, as opposed to an irreversible one, like microfracturing, is responsible for the transient effective permeability increase. Our work suggests the feasibility of dynamically controlling the effective permeability of fractured systems. The result has consequences for models of earthquake triggering and permeability enhancement in fault zones due to dynamic shaking from near and distant earthquakes

Downscaling of fracture energy during brittle creep experiments

We present mode 1 brittle creep fracture experiments along fracture surfaces that contain strength heterogeneities. Our observations provide a link between smooth macroscopic time-dependent failure and intermittent microscopic stress-dependent processes. We find the large-scale response of slow-propagating subcritical cracks to be well described by an Arrhenius law that relates the fracture speed to the energy release rate. At the microscopic scale, high-resolution optical imaging of the transparent material used (PMMA) allows detailed description of the fracture front. This reveals a local competition between subcritical and critical propagation (pseudo stick-slip front advances) independently of loading rates. Moreover, we show that the local geometry of the crack front is self-affine and the local crack front velocity is power law distributed. We estimate the local fracture energy distribution by combining high-resolution measurements of the crack front geometry and an elastic line fracture model. We show that the average local fracture energy is significantly larger than the value derived from a macroscopic energy balance. This suggests that homogenization of the fracture energy is not straightforward and should be taken cautiously. Finally, we discuss the implications of our results in the context of fault mechanics

Interplay of seismic and aseismic deformations during earthquake swarms: An experimental approach

Observations of earthquake swarms and slow propagating ruptures on related faults suggest a close relation between the two phenomena. Earthquakes are the signature of fast unstable ruptures initiated on localized asperities while slow aseismic deformations are experienced on large stable segments of the fault plane. The spatial proximity and the temporal coincidence of both fault mechanical responses highlight the variability of fault rheology. However, the mechanism relating earthquakes and aseismic processes is still elusive due to the difficulty of imaging these phenomena of large spatiotemporal variability at depth. Here we present laboratory experiments that explore, in great detail, the deformation processes of heterogeneous interfaces in the brittle-creep regime. We track the evolution of an interfacial crack over 7 orders of magnitude in time and 5 orders of magnitude in space using optical and acoustic sensors. We explore the response of the system to slow transient loads and show that slow deformation episodes are systematically accompanied by acoustic emissions due to local fracture energy disorder. Features of acoustic emission activities and deformation rate distributions of our experimental system are similar to those in natural faults. On the basis of an activation energy model, we link our results to the Rate and State friction model and suggest an active role of local creep deformation in driving the seismic activity of earthquake swarms

Average crack-front velocity during subcritical fracture propagation in a heterogeneous medium

We study the average velocity of crack fronts during stable interfacial fracture experiments in a heterogeneous quasibrittle material under constant loading rates and during long relaxation tests. The transparency of the material (polymethylmethacrylate) allows continuous tracking of the front position and relation of its evolution to the energy release rate. Despite significant velocity fluctuations at local scales, we show that a model of independent thermally activated sites successfully reproduces the large-scale behavior of the crack front for several loading conditions

Development of novel chitosan / guar gum inks for extrusion-based 3D bioprinting: process, printability and properties

The major limitation of 3D bioprinting is the availability of inks. In order to develop new ink formulations, both their rheological behavior to obtain the best printability and the target bio-printed objects conformities must be studied. In this paper, for the first time in our knowledge, the preparation and the characterization of novel ink formulations based on two natural biocompatible polysaccharides, chitosan (CH) and guar gum (GG), are presented. Five ink formulations containing different proportions of CH and GG were prepared and characterized in terms of rheological properties and solvent evaporation. Their printability was assessed (by varying the nozzle diameter, pressure and speed) using an extrusion-based 3D bioprinting process performed directly in air at 37 °C. Results showed that the incorporation of GG improved both the printability of the pure chitosan ink by increasing the viscosity of the solution and the shape fidelity by accelerating the solvent evaporation. We showed that the ink containing 15% (w/w) of GG and 85% (w/w) of CH had the best printability. This formulation was therefore used for the preparation of membranes that were characterized by infrared spectroscopy (FTIR) and X-Ray Diffraction (XRD) before and after gelation as well as for their mechanical properties (Young modulus, strength and strain at break). The optimal process printing parameters were determined to be: 27 G micronozzle, extrusion pressure below 2 bars and robot head speed between 20 and 25 mm/s. This novel ink formulation is a guideline for developing 2D scaffolds (such as auto-supported membranes) or 3D scaffolds for biomedical applications.publishe

Downscaling of fracture energy during brittle creep experiments

We present mode 1 brittle creep fracture experiments along fracture surfaces that contain strength heterogeneities. Our observations provide a link between smooth macroscopic time-dependent failure and intermittent microscopic stress-dependent processes. We find the large-scale response of slow-propagating subcritical cracks to be well described by an Arrhenius law that relates the fracture speed to the energy release rate. At the microscopic scale, high-resolution optical imaging of the transparent material used (PMMA) allows detailed description of the fracture front. This reveals a local competition between subcritical and critical propagation (pseudo stick-slip front advances) independently of loading rates. Moreover, we show that the local geometry of the crack front is self-affine and the local crack front velocity is power law distributed. We estimate the local fracture energy distribution by combining high-resolution measurements of the crack front geometry and an elastic line fracture model. We show that the average local fracture energy is significantly larger than the value derived from a macroscopic energy balance. This suggests that homogenization of the fracture energy is not straightforward and should be taken cautiously. Finally, we discuss the implications of our results in the context of fault mechanics. Copyright © 2011 by the American Geophysical Union

Average crack-front velocity during subcritical fracture propagation in a heterogeneous medium.

We study the average velocity of crack fronts during stable interfacial fracture experiments in a heterogeneous quasibrittle material under constant loading rates and during long relaxation tests. The transparency of the material (polymethylmethacrylate) allows continuous tracking of the front position and relation of its evolution to the energy release rate. Despite significant velocity fluctuations at local scales, we show that a model of independent thermally activated sites successfully reproduces the large-scale behavior of the crack front for several loading conditions