NASA-UVA light aerospace alloy and structures technology program

The report on progress achieved in accomplishing of the NASA-UVA Light Aerospace Alloy and Structures Technology Program is presented. The objective is to conduct interdisciplinary graduate student research on the performance of next generation, light weight aerospace alloys and associated thermal gradient structures in close collaboration with researchers. The efforts will produce basic understanding of material behavior, new monolithic and composite alloys, processing methods, solid and fluid mechanics analyses, measurement advances, and a pool of educated graduate students. The presented accomplishments include: research on corrosion fatigue of Al-Li-Cu alloy 2090; research on the strengthening effect of small In additions to Al-Li-Cu alloys; research on localized corrosion of Al-Li alloys; research on stress corrosion cracking of Al-Li-Cu alloys; research on fiber-matrix reaction studies (Ti-1100 and Ti-15-3 matrices containing SCS-6, SCS-9, and SCS-10 fibers); and research on methods for quantifying non-random particle distribution in materials that has led to generation of a set of computer programs that can detect and characterize clusters in particles

On Extracting Mechanical Properties from Nanoindentation at Temperatures up to 1000∘^{\circ}C

Alloyed MCrAlY bond coats, where M is usually cobalt and/or nickel, are essential parts of modern turbine blades, imparting environmental resistance while mediating thermal expansivity differences. Nanoindentation allows the determination of their properties without the complexities of traditional mechanical tests, but was not previously possible near turbine operating temperatures. Here, we determine the hardness and modulus of CMSX-4 and an Amdry-386 bond coat by nanoindentation up to 1000$^{\circ}$C. Both materials exhibit a constant hardness until 400$^{\circ}$C followed by considerable softening, which in CMSX-4 is attributed to the multiple slip systems operating underneath a Berkovich indenter. The creep behaviour has been investigated via the nanoindentation hold segments. Above 700$^{\circ}$C, the observed creep exponents match the temperature-dependence of literature values in CMSX-4. In Amdry-386, nanoindentation produces creep exponents very close to literature data, implying high-temperature nanoindentation may be powerful in characterising these coatings and providing inputs for material, model and process optimisations

3D FEM model development from 3D optical measurement technique applied to corroded steel bars

Understanding the mechanical effects of the corrosion pits on the steel surface requires an accurate definition of their geometry and distribution along the rebar. 3D optical measurement technique is used to obtain the outer geometry of artificially corroded bars tested under cyclic or monotonic loads. 3D FEM model development from the 3D scanning results were carried out in order to investigate the failure process and local effects on the pits, which are responsible of the variation of the mechanical properties in corroded steel reinforcement. In addition, a validation of a simplified model, which allows the mechanical steel properties determination given an estimated corrosion level, is presented. 3D models were convenient to observe and measure the local effects on the pits.Peer ReviewedPostprint (author's final draft

Determination of stress concentration factors in offshore wind welded structures through a hybrid experimental and numerical approach

Offshore wind turbine (OWT) monopile support structures generally consist of steel cans connected together through circumferential welding joints. One critical factor to evaluate the localised increase in stresses is the stress concentration factor (SCF) which depends on the welding quality. The complex welding profiles in OWT monopiles makes the accurate calculation of SCF quite challenging. In this work, an innovative approach for the calculation of SCFs in offshore welded structures is proposed based on combined 3D (three-dimensional) laser scanning technology (LST) and 3D finite element analysis (FEA). The precise geometry of the welded specimens is captured using 3D LST, and then imported into a finite element software to perform 3D FEA modelling to accurately calculate SCFs. A 2D (two-dimensional) FEA model of a typical offshore welded structure with ideal geometry is also developed in this work. In addition to numerically calculate SCFs, the 2D FEA model is further combined with non-linear RSM (response surface method) to derive analytical equations, expressing SCFs of offshore welded structures in terms of key welding parameters. Both LST-FEA3D and RSM-FEA2D models are applied to calculate SCFs in large-scale S-N fatigue welded specimens. The results indicate that the LST-FEA3D approach is capable of capturing the variation of SCFs along the width of the welded specimens and identifying the critical points where fatigue crack is most likely to initiate; and the RSM-FEA2D is valuable and efficient in deriving analytical parametric equations for SCFs

Ground test program for a full-size solar dynamic heat receiver

Test hardware, facilities, and procedures were developed to conduct ground testing of a full size, solar dynamic heat receiver in a partially simulated, low Earth orbit environment. The heat receiver was designed to supply 102 kW of thermal energy to a helium and xenon gas mixture continuously over a 94 minute orbit, including up to 36 minutes of eclipse. The purpose of the test program was to quantify the receiver thermodynamic performance, its operating temperatures, and thermal response to changes in environmental and power module interface boundary conditions. The heat receiver was tested in a vacuum chamber using liquid nitrogen cold shrouds and an aperture cold plate. Special test equipment were designed to provide the required ranges in interface boundary conditions that typify those expected or required for operation as part of the solar dynamic power module on the Space Station Freedom. The support hardware includes an infrared quartz lamp heater with 30 independently controllable zones and a closed Brayton cycle engine simulator to circulate and condition the helium xenon gas mixture. The test article, test support hardware, facilities, and instrumentation developed to conduct the ground test program are all described

Combined Kelvin probe force microscopy and secondary ion mass spectrometry for hydrogen detection in corroded 2024 aluminium alloy

The capability of Kelvin probe force microscopy (KFM) to detect and locate hydrogen in corroded 2024 aluminium alloy was demonstrated. Hydrogen was introduced inside the 2024 alloy following a cyclic corrosion test consisting of cycles of immersion in 1 M NaCl solution followed by exposure to air at -20 °C. The combination of scanning electron microscopy, secondary ion mass spectrometry and KFM demonstrated that the grain and subgrain boundaries were preferential pathways for the short-circuit diffusion of hydrogen but also acted as a source of hydrogen diffusion in the lattice over distances of up to ten microns with non-negligible desorption when exposed to air at room temperature for 24 h