93 research outputs found

    THE PHOSGENIZATION OF 2,4- AND 2,6-DIAMINOTOLUENE HYDROCHLORIDE

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    Effect of animal fats on the physical properties of palm fat

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    Palm fat is one of the most commonly used fats in food industry. The main role of palm fat is to develop the desired texture of food products. Fat blends were developed to find the most appropriate mixture fitting the technological needs. In our work palm mid fraction (PMF) was mixed with anhydrous milk fat (AMF), goose fat (G), and lard (L) in a 1:1 ratio. Anhydrous milk fat represents fat consisting of a wide range of fatty acids. Goose fat is a soft, easily melting fat, and lard is characterized as animal fat with wide melting temperature interval. The measurements aimed to establish the miscibility of the fats and the effect of animal fats on the melting-solidification profile of palm mid fraction. SFC vs temperature curves, Differential Scanning Calorimetry (DSC) melting thermograms describe the melting profile of the samples. Isotherm crystallization by SFC vs time curves and DSC cooling thermograms were measured to characterize the solidification of pure fats and the blends. Since the SFC curves did not show crosspoints we concluded that fats blended in a 1:1 ratio were miscible. Anhydrous milk fat strongly modified the properties of palm mid fraction, the blend became similar to anhydrous milk fat. Goose fat had no strong modification effect on palm mid fraction and could be considered as a softening agent. The effect of lard was complex: melting and solidification behaviour of the blend differed from the characteristics of both parent fats

    INVESTIGATION OF THE REACTION CONDITIONS OF PHOSGENE PRODUCTION

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    Signal-integrity measurements on VME320 backplane

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    Presentation made at the 4th Workshop on Electronics for LHC Experiments, INFN Rome, 21-25 September 1998.Using high-speed buses in data-acquisition systems is very much widespread. The bus topology and performance is one of the key factor in the overallperformance of the whole system. The limitation of the speed which can be achieved on a backplane-like bus is determined by the signal-integritybehavior of the bus and the driver and receiver of the daughter cards. This paper deals with the evaluation of one of the latest VME-like backplanes.Measurement results are presented for the impedance profile, frequency-domain response, skew, eye-diagram and BER of the transactions

    Application of electronic tongue to discriminate white wines originated from different regions of Hungary

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    In this work, the application of an electronic tongue (ET) based on a specific ion-selective sensor array for discrimination of different white wine types is presented. The electronic tongue equipped with specific sensor array containing seven IFSET sensors was used to analyze wine samples. The obtained ET responses were evaluated using different pattern recognition methods. Principal component analysis (PCA) provides the possibility to identify some initial patterns. Linear discriminant analysis (LDA) was used to build models to separate white wine samples based on wine regions and grape cultivars. The results showed that every group was distinguished from each other with no misclassification error. Furthermore, the sequence of the wine sample groups was similar to the increasing total acidity content. Partial least square (PLS) regression was used to build models for the prediction of the main chemical compositions of the wine samples based on the electronic tongue results. The closest correlation (R2=0.93) was found in case of ‘total acidity’, and the prediction error (RMSEP) was 6.9%. The pH of the wine samples was predicted with good correlation (R2=0.89) but higher prediction error (RMSEP=10.71%) from the electronic tongue results. The ET combining these statistical methods can be applied to determine the origin and variety of the wine samples in easy and quick way

    Global Maps of Science based on the new Web-of-Science Categories

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    In August 2011, Thomson Reuters launched version 5 of the Science and Social Science Citation Index in the Web of Science (WoS). Among other things, the 222 ISI Subject Categories (SCs) for these two databases in version 4 of WoS were renamed and extended to 225 WoS Categories (WCs). A new set of 151 Subject Categories (SCs) was added, but at a higher level of aggregation. Since we previously used the ISI SCs as the baseline for a global map in Pajek (Rafols et al., 2010) and brought this facility online (at http://www.leydesdorff.net/overlaytoolkit), we recalibrated this map for the new WC categories using the Journal Citation Reports 2010. In the new installation, the base maps can also be made using VOSviewer (Van Eck & Waltman, 2010).Comment: Scientometrics, in pres

    Obsessive and harmonious passion in physically active Spanish and Hungarian men and women: a brief report on cultural and gender differences

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    Increased research on passion in physical activity calls for direct examination of possible mediating variables that could influence the research outcome. The present study using a two by-two (nation by gender) between-participants design, examined whether gender and/or cultural differences in obsessive- and harmonious passion were present in Spanish and Hungarian physically active individuals. Participants (n=1,002) completed the Passion Scale, reported their gender, age, and weekly hours of physical activity. Multivariate analysis of covariance revealed that the experiencing of physical activity-related obsessive- and harmonious passion differed between the two countries and Hungarian women scored significantly higher on harmonious and obsessive passion than Spanish women. However, Hungarian men only scored significantly higher on obsessive passion, but not harmonious passion compared to Spanish men. These results suggest that the moderating role of gender and cultural differences should be addressed more carefully in conducting and interpreting results of research concerned with passion in physical activity

    Authentication of Tokaj Wine (Hungaricum) with the Electronic Tongue and Near Infrared Spectroscopy

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    Tokaj wines (Hungaricum) are botrytized wines acknowledged for the unique organoleptic properties bestowed by botrytized grape berries during production. Excluding these berries during wine production or manipulating the sugar content of low-grade wines to imitate high-grade wines are some recent suspicious activities that threaten the wine quality. Advanced methods such as spectroscopy and sensor-based devices have been lauded for rapid, reliable, and cost-effective analysis, but there has been no report of their application to monitor grape must concentrate adulteration in botrytized wines. The study aimed to develop models to rapidly discriminate lower grade Tokaj wines, "Forditas I" and "Forditas II," that were artificially adulterated with grape must concentrate to match the sugar content of high-grade Tokaj wines using an electronic tongue (e-tongue) and two near infrared spectrometers (NIRS). Data were evaluated with the following chemometrics: principal component analysis (PCA), discriminant analysis (LDA), partial least square regression (PLSR), and aquaphotomics (a novel approach). There was a noticeable pattern of separation in PCA for all three instruments and 100% classification of adulterated and nonadulterated wines in LDA using the e-tongue. Aquagrams from the aquaphotomics approach showed important water absorption bands capable of being markers of Tokaj wine quality. PLSR models showed coefficient of determination ((RCV)-C-2) of 0.98 (e-tongue), 0.97 (benchtop NIRS), 0.87 (handheld NIRS), and low root mean squared errors of cross-validation. All three instruments could discriminate, classify, and predict grape must concentrate adulteration in Tokaj with a high accuracy and low error. The methods can be applied for routine quality checks of botrytized wines. Practical Application Tokaj wines (Hungaricum) are botrytized wines acknowledged for the unique organoleptic properties bestowed by botrytized grape berries during production. Excluding these berries during wine production or manipulating the sugar content of low-grade wines to imitate high-grade wines are some recent suspicious activities that threaten the wine quality. Using advanced instruments, the electronic tongue, benchtop near infrared spectroscopy, and a handheld near infrared spectroscopy, we could discriminate, classify, and predict grape must concentrate adulteration in Tokaj with a high accuracy and low error. The models in our study can be applied for routine quality checks of botrytized wines
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