3,912 research outputs found
Complementary use of TEM and APT for the investigation of steels nanostructured by severe plastic deformation
The properties of bulk nanostructured materials are often controlled by
atomic scale features like segregation along defects or composition gradients.
Here we discuss about the complimentary use of TEM and APT to obtain a full
description of nanostructures. The advantages and limitations of both
techniques are highlighted on the basis of experimental data collected in
severely deformed steels with a special emphasis on carbon spatial
distribution
Decomposition process in a FeAuPd alloy nanostructured by severe plastic deformation
The decomposition process mechanisms have been investigated in a Fe50Au25Pd25
(at.%) alloy processed by severe plastic deformation. Phases were characterized
by X-ray diffraction and microstructures were observed using transmission
electron microscopy. In the coarse grain alloy homogenized and aged at , the bcc \alpha-Fe and fcc AuPd phases nucleate in the fcc
supersaturated solid solution and grow by a discontinuous precipitation process
resulting in a typical lamellar structure. The grain size of the homogenized
FeAuPd alloy was reduced in a range of 50 to 100nm by high pressure torsion.
Aging at this nanostructure leads to the decomposition
of the solid solution into an equi-axed microstructure. The grain growth is
very limited during aging and the grain size remains under 100nm. The
combination of two phases with different crystallographic structures (bcc
\alpha-Fe and fcc AuPd) and of the nanoscaled grain size gives rise to a
significant hardening of the allo
Mott transition in Cr-doped V2O3 studied by ultrafast reflectivity: electron correlation effects on the transient response
The ultrafast response of the prototype Mott-Hubbard system (V1-xCrx)2O3 was
systematically studied with fs pump-probe reflectivity, allowing us to clearly
identify the effects of the metal-insulator transition on the transient
response. The isostructural nature of the phase transition in this material
made it possible to follow across the phase diagram the behaviour of the
detected coherent acoustic wave, whose average value and lifetime depend on the
thermodynamic phase and on the correlated electron density of states. It is
also shown how coherent lattice oscillations can play an important role in some
changes affecting the ultrafast electronic peak relaxation at the phase
transition, changes which should not be mistakenly attributed to genuine
electronic effects. These results clearly show that a thorough understanding of
the ultrafast response of the material over several tenths of ps is necessary
to correctly interpret its sub-ps excitation and relaxation regime, and appear
to be of general interest also for other strongly correlated materials.Comment: 6 pages, 3 figures. Europhysics Letters (in press
A standardised method for measuring in situ denitrification in shallow aquifers: numerical validation and measurements in riparian wetlands
A tracer test to examine in situ denitrification in shallow groundwater by a piezometer with a packer system used bromide as a tracer of dilution and acetylene (10%) to block the denitrification process at the nitrous oxide stage. During the test, dissolved oxygen, nitrate (NO3-), bromide (Br-), nitrous oxide (N2O) and dissolved organic carbon (DOC) were measured. To calibrate the experimental method, comparison with numerical simulations of the groundwater transfer were carried out, taking into account the environmental characteristics. The method was tested by measurements undertaken in different environmental conditions (geology, land use and hydrology) in two riparian wetlands. Denitrification rates measured by this method ranged from 5.7 10-6 g N-NO3-L-1 h-1 to 1.97 10-3 g N-NO3-L-1 h-1 The method is applicable in shallow aquifers with a permeability from 10-2 to 10-4m s-1
Dissecting the spiral galaxy M83: mid-infrared emission and comparison with other tracers of star formation
We present a detailed mid-infrared study of the nearby, face-on spiral galaxy
M83 based on ISOCAM data. M83 is a unique case study, since a wide variety of
MIR broad-band filters as well as spectra, covering the wavelength range of 4
to 18\mu m, were observed and are presented here. Emission maxima trace the
nuclear and bulge area, star-formation regions at the end of the bar, as well
as the inner spiral arms. The fainter outer spiral arms and interarm regions
are also evident in the MIR map. Spectral imaging of the central 3'x3' (4 kpc x
4 kpc) field allows us to investigate five regions of different environments.
The various MIR components (very small grains, polycyclic aromatic hydrocarbon
(PAH) molecules, ionic lines) are analyzed for different regions throughout the
galaxy. In the total 4\mu m to 18\mu m wavelength range, the PAHs dominate the
luminosity, contributing between 60% in the nuclear and bulge regions and 90%
in the less active, interarm regions. Throughout the galaxy, the underlying
continuum emission from the small grains is always a smaller contribution in
the total MIR wavelength regime, peaking in the nuclear and bulge components.
The implications of using broad-band filters only to characterize the
mid-infrared emission of galaxies, a commonly used ISOCAM observation mode, are
discussed. We present the first quantitative analysis of new H-alpha and 6cm
VLA+Effelsberg radio continuum maps of M83. The distribution of the MIR
emission is compared with that of the CO, HI, R band, H-alpha and 6cm radio. A
striking correlation is found between the intensities in the two mid-infrared
filter bands and the 6cm radio continuum. To explain the tight
mid-infrared-radio correlation we propose the anchoring of magnetic field lines
in the photoionized shells of gas clouds.Comment: 22 pages, 15 figures. Accepted for publication in A&
Mid-infrared observations of the ultraluminous galaxies IRAS14348-1447, IRAS19254-7245, and IRAS23128-5919
We present a study of the three ultraluminous infrared galaxies
IRAS14348-1447, IRAS19254-7245, and IRAS23128-5919, based on mid-infrared (MIR)
spectro-imaging (5-18microns) observations performed with ISOCAM. We find that
the MIR emission from each system, which consists of a pair of interacting late
type galaxies, is principally confined to the nuclear regions with diameters of
1-2kpc and can account for more than 95% of their IRAS 12micron flux. In each
interacting system, the galaxy hosting an active galactic nucleus (AGN)
dominates the total spectrum and shows stronger dust continuum (12-16microns)
relative to the Unidentified Infrared Band (UIB) emission (6-9microns),
suggestive of its enhanced radiation field. The MIR dominant galaxy also
exhibits elevated 15micron/Halpha and 15micron/K ratios which trace the high
extinction due to the large quantities of molecular gas and dust present in its
central regions. Using only diagnostics based on our mid-infrared spectra, we
can establish that the Seyfert galaxy IRAS19254-7245 exhibits MIR spectral
features of an AGN while the MIR spectrum of the Seyfert (or LINER) member of
IRAS23128-5919 is characteristic of dust emission principally heated by star
forming regions.Comment: Accepted for publication in Astronomy & Astrophysics, 13 pages, 9
figure
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