7 research outputs found

    Colloidal Hydroxyapatite/Poly(Acrylic Acid) Hybrids Using Calcium Sucrate and Ammoniumdihydrogen Orthophosphate

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    This manuscript is concerned with a simple and novel method to synthesize hydroxyapatite-poly(acylic acid) hybrid materials for broad range of applications. In this method, hydroxyapatite nanoparticles are synthesized using calcium sucrate and ammoniumdihydrogen orthophosphate in the presence of poly(acrylic acid). Increase in poly(acrylic acid) concentration in the synthesis medium results in the increase in the hydrodynamic radius of particle size allowing increased hydration. Poly(acylic acid) tends to control both crystallite size and colloidal stability. Increase in poly(acrylic acid) concentration decreases the crystallite size of the products but considerably increases their shelf life as stable colloidal solutions. Thermo gravimetric analysis shows that there are no combustible or volatile impurities present in these samples. This is further supported by FT-IR studies, which show three types of interactions between hydroxyapatite nanoparticles and poly(acrylic acid)

    Data from: Akaganeite nanorices deposited muscovite mica surfaces as sunlight active green photocatalyst

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    Thin-films of akaganeite [FeO(OH)] nanorices deposited muscovite mica (ANPM) surfaces are produced using the facile urea assisted controlled self-assembly technique. The synthesized materials are characterized using scanning electron microscopy (SEM) with energy dispersive X-ray spectroscopy (EDS), atomic force microscopy, X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectroscopy and thermo gravimetric analysis (TGA). The prepared nanorices on mica surfaces show average particle length and width as 200 nm and 50 nm respectively. Synthesized material acts as an efficient photocatalyst under UV and sunlight conditions as demonstrated by the degradation of standard methylene blue solution. The methylene blue degradation efficiencies of the catalyst under exposure to 180 min sunlight and UV are 89% and 87.5% respectively which shows that the catalyst is highly active under sunlight than under UV light. Therefore, the synthesized material is a potential green photocatalyst in efficient treatment of industrial dye effluents under direct sunlight
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