Evaluation of a simple hyphenated system for flow injection solid-phase pre-concentration and capillary electrophoresis

In this work, the development and evaluation of a hyphenated flow injection-capillary electrophoresis system with on-line pre-concentration is described. Preliminary tests were performed to investigate the influence of flow rates over the analytical signals. Results revealed losses in terms of sensitivity of the FIA-CE system when compared to the conventional CE system. To overcome signal decrease and to make the system more efficient, a lower flow rate was set and an anionic resin column was added to the flow manifold in order to pre-concentrate the analyte. The pre-concentration FIA-CE system presented a sensitivity improvement of about 660% and there was only a small increase of 8% in total peak dispersion. These results have confirmed the great potential of the proposed system for many analytical tasks especially for low concentration samples.Nesse trabalho apresentamos um sistema hifenizado envolvendo as duas técnicas analíticas: eletroforese capilar (CE) e análises por injeção em fluxo (FIA), denominado de FIA-CE. Parâmetros como a influência do fluxo e a natureza do eluente frente ao sistema CE foram avaliados. O sistema demonstrou-se promissor quanto à possibilidade de aplicações em diferentes áreas da química analítica. O aumento da sensibilidade foi da ordem de 660% devido ao emprego de colunas de troca iônica no sistema FIA. Esse resultado comprova o grande potencial do sistema FIA-CE.Coordenacao de Aperfeicoamento de Pessoal de Nivel Superior (CAPES)CNPqFAPES

Emission-Line Galaxy Surveys as Probes of the Spatial Distribution of Dwarf Galaxies. I. The University of Michigan Survey

Objective-prism surveys which select galaxies on the basis of line-emission are extremely effective at detecting low-luminosity galaxies and constitute some of the deepest available samples of dwarfs. In this study, we confirm that emission-line galaxies (ELGs) in the University of Michigan (UM) objective-prism survey (MacAlpine et al. 1977-1981) are reliable tracers of large-scale structure, and utilize the depth of the samples to examine the spatial distribution of low-luminosity (M$_{B} >$ -18.0) dwarfs relative to higher luminosity giant galaxies (M$_{B} \leq$ -18.0) in the Updated Zwicky Catalogue (Falco et al. 1999). New spectroscopic data are presented for 26 UM survey objects. We analyze the relative clustering properties of the overall starbursting ELG and normal galaxy populations, using nearest neighbor and correlation function statistics. This allows us to determine whether the activity in ELGs is primarily caused by gravitational interactions. We conclude that galaxy-galaxy encounters are not the sole cause of activity in ELGs since ELGs tend to be more isolated and are more often found in the voids when compared to their normal galaxy counterparts. Furthermore, statistical analyses performed on low-luminosity dwarf ELGs show that the dwarfs are less clustered when compared to their non-active giant neighbors. The UM dwarf samples have greater percentages of nearest neighbor separations at large values and lower correlation function amplitudes relative to the UZC giant galaxy samples. These results are consistent with the expectations of galaxy biasing.Comment: 17 pages, 4 tables, 10 figures. Accepted for publication in the Ap

Double Bars, Inner Disks, and Nuclear Rings in Early-Type Disk Galaxies

We present results from an imaging survey of an unbiased sample of thirty-eight early-type (S0--Sa), low-inclination, optically barred galaxies in the field. Our goal was to find and characterize central stellar and gaseous structures: secondary bars, inner disks, and nuclear rings. Bars inside bars are surprisingly common: at least one quarter of the sample galaxies (possibly as many as 40%) are double-barred, with no preference for Hubble type or the strength of the primary bar. A typical secondary bar is ~12% of the size of its primary bar and 240--750 pc in radius. We see no significant effect of secondary bars on nuclear activity. We also find kiloparsec-scale inner disks in at least 20% of our sample, almost exclusively in S0 galaxies. These disks are on average 20% the size of their host bar, and show a wider range of relative sizes than do secondary bars. Nuclear rings are present in about a third of our sample. Most are dusty, sites of current or recent star formation, or both; such rings are preferentially found in Sa galaxies. Three S0 galaxies (15% of the S0's) appear to have purely stellar nuclear rings, with no evidence for dust or recent star formation. The fact that these central stellar structures are so common indicates that the inner regions of early-type barred galaxies typically contain dynamically cool and disklike structures. This is especially true for S0 galaxies, where secondary bars, inner disks, and/or stellar nuclear rings are present at least two thirds of the time. (abridged)Comment: LaTeX, 15 pages, 7 EPS figures; to appear in The Astronomical Journal (July 2002

Longitudinal Ion Acceleration from High-Intensity Laser Interactions with Underdense Plasma

Longitudinal ion acceleration from high-intensity (I ~ 10^20 Wcm^-2) laser interactions with helium gas jet targets (n_e ~ 0.04 n_c) have been observed. The ion beam has a maximum energy for He^2+ of approximately 40 MeV and was directional along the laser propagation path, with the highest energy ions being collimated to a cone of less than 10 degrees. 2D particle-in-cell simulations have been used to investigate the acceleration mechanism. The time varying magnetic field associated with the fast electron current provides a contribution to the accelerating electric field as well as providing a collimating field for the ions. A strong correlation between the plasma density and the ion acceleration was found. A short plasma scale-length at the vacuum interface was observed to be beneficial for the maximum ion energies, but the collimation appears to be improved with longer scale-lengths due to enhanced magnetic fields in the ramp acceleration region.Comment: 18 pages, 6 figure

Ab initio alpha-alpha scattering

Processes involving alpha particles and alpha-like nuclei comprise a major part of stellar nucleosynthesis and hypothesized mechanisms for thermonuclear supernovae. In an effort towards understanding alpha processes from first principles, we describe in this letter the first ab initio calculation of alpha-alpha scattering. We use lattice effective field theory to describe the low-energy interactions of nucleons and apply a technique called the adiabatic projection method to reduce the eight-body system to an effective two-cluster system. We find good agreement between lattice results and experimental phase shifts for S-wave and D-wave scattering. The computational scaling with particle number suggests that alpha processes involving heavier nuclei are also within reach in the near future.Comment: 6 pages, 6 figure

Normal Globular Cluster Systems in Massive Low Surface Brightness Galaxies

We present the results of a study of the globular cluster systems of 6 massive spiral galaxies, originally cataloged as low surface brightness galaxies but here shown to span a wide range of central surface brightness values, including two intermediate to low surface brightness galaxies. We used the Advanced Camera for Surveys on board HST to obtain photometry in the F475W and F775W bands and select sources with photometric and morphological properties consistent with those of globular clusters. A total of 206 candidates were identified in our target galaxies. From a direct comparison with the Galactic globular cluster system we derive specific frequency values for each galaxy that are in the expected range for late-type galaxies. We show that the globular cluster candidates in all galaxies have properties consistent with globular cluster systems of previously studied galaxies in terms of luminosity, sizes and color. We establish the presence of globular clusters in the two intermediate to low surface brightness galaxies in our sample and show that their properties do not have any significant deviation from the behavior observed in the other sample galaxies. Our results are broadly consistent with a scenario in which low surface brightness galaxies follow roughly the same evolutionary history as normal (i.e. high surface) brightness galaxies except at a much lower rate, but require the presence of an initial period of star formation intense enough to allow the formation of massive star clusters.Comment: 14 pages, 6 figures. AJ accepte

Ionization disequilibrium in K- and L-shell ions

Producción CientíficaTime-gated Sc K-shell and Ge L-shell spectra are presented from a range of characterized thermodynamic states spanning ion densities of 1e19-1e20cm-3 and plasma temperatures around 2000eV. For the higher densities studied and temperatures from 1000 to 3000 eV, the Sc and Ge x-ray emission spectra are consistent with steady-state calculations from the modern atomic kinetics model SCRAM. At the lower ion densities achieved through plasma expansion, however, the model calculations require a higher plasma temperature to reproduce the observed Ge spectrum. We attribute this to ionization disequilibrium of the Sc because the ionization time scales exceed the hydrodynamic timescale when the inferred temperatures diverge.This work has been supported by the Research Grant No. PID2019-108764RB-I00 from the Spanish Ministry of Science and Innovation

Desfolhamento artificial durante o estádio de antese do girassol

In order to study the effects of various leaf removal treatments during anthesis stage on sunflower (Helianthus annuus L.) grain yield and other agronomic traits, an experiment was carried out at the Estação Experimental Agronômica da Universidade Federal do Rio Grande do Sul, in Guaíba, RS, Brazil, during the 1981/82 growing season. The leaf removal treatments were: an undefoliated check, leaves of the plant upper third removed, leaves of medium third removed, leaves of lower third removed, leaves of upper third plus lower third removed, leaves of upper plus medium thirds removed, leaves of medium plus lower thirds removed and all leaves removed. These eight leaf removal treatments were applied in two times: at the beginning and at the end of anthesis of ‘Conti-GH 8121’ sunflower cultivar. When compared with the undefoliated check, grain yield decreased from 9 to 80% with the defoliation treatments, except for two: removal of leaves of upper third of the plant and removal of the leaves of lower third of the plant. The yield component grain number in heads was affected only by leaf defoliation levels whereas the other component, grain weight, was affected by date as well as by levels of defoliation. The diameter of sunflower heads and the harvest index were also affected by defoliation date and level. Grain yield was positively associated with all other traits studied.Para avaliar os efeitos de diversos níveis de remoção de folhas durante o estádio de antese sobre o rendimento de grãos e outras características agronómicas do girassol (Helianthus annuus L.), foi conduzido este ensaio na Estação Experimental Agronômica da Universidade Federal do Rio Grande do Sul, em Guaíba, RS, no ano agrícola de 1981/82. Os níveis de desfolhamento utilizados foram: testemunha, sem remoção de folhas; remoção das folhas do terço superior das plantas, do terço médio, do terço inferior, do terço superior mais terço inferior, do terço superior mais terço médio, do terço médio mais terço inferior e remoção de todas as folhas. Estes oito níveis de remoção de folhas foram aplicados em duas épocas de desfolhamento, início e final da antese da cultivar Conti-GH 8121. Comparado com a testemunha, o rendimento de grãos decresceu entre 9 e 80% com a aplicação dos níveis de desfolhamento, exceto para dois tratamentos, remoção das folhas do terço superior e remoção das folhas do terço inferior das plantas. O componente do rendimento número de grãos por capítulo foi afetado apenas pelos níveis de desfolhamento enquanto o componente peso de grãos foi afetado pelas épocas e pelos níveis de desfolhamento. O diâmetro de capítulos e índice de colheita também foram afetados pelos tratamentos níveis e épocas de desfolhamento. O rendimento de grãos associou-se positivamente com todas as características estudadas

Radio and optical intra-day variability observations of five blazars

We carried out a pilot campaign of radio and optical band intra-day variability (IDV) observations of five blazars (3C66A, S5 0716+714, OJ287, B0925+504, and BL Lacertae) on December 18--21, 2015 by using the radio telescope in Effelsberg (Germany) and several optical telescopes in Asia, Europe, and America. After calibration, the light curves from both 5 GHz radio band and the optical R band were obtained, although the data were not smoothly sampled over the sampling period of about four days. We tentatively analyse the amplitudes and time scales of the variabilities, and any possible periodicity. The blazars vary significantly in the radio (except 3C66A and BL Lacertae with only marginal variations) and optical bands on intra- and inter-day time scales, and the source B0925+504 exhibits a strong quasi-periodic radio variability. No significant correlation between the radio- and optical-band variability appears in the five sources, which we attribute to the radio IDV being dominated by interstellar scintillation whereas the optical variability comes from the source itself. However, the radio- and optical-band variations appear to be weakly correlated in some sources and should be investigated based on well-sampled data from future observations.Comment: 6 pages, 6 figures, accepted by MNRA

An Imaging Survey of Early-Type Barred Galaxies

This paper presents the results of a high-resolution imaging survey, using both ground-based and Hubble Space Telescope images, of a complete sample of nearby barred S0--Sa galaxies in the field, with a particular emphasis on identifying and measuring central structures within the bars: secondary bars, inner disks, nuclear rings and spirals, and off-plane dust. A discussion of the frequency and statistical properties of the various types of inner structures has already been published. Here, we present the data for the individual galaxies and measurements of their bars and inner structures. We set out the methods we use to find and measure these structures, and how we discriminate between them. In particular, we discuss some of the deficiencies of ellipse fitting of the isophotes, which by itself cannot always distinguish between bars, rings, spirals, and dust, and which can produce erroneous measurements of bar sizes and orientations.Comment: LaTeX, 66 pages (including 42 figures, 36 in color). To appear in The Astrophysical Journal Supplement. Full-resolution and text-only versions available at http://www.iac.es/galeria/erwin/research