Normal soaking extraction (NSE) of rotenone from Derris elliptica

Derris elliptica or the tuba plant contains rotenone, bio-active compound known that has the potential to be used as bio-pesticide. Bio-pesticide is the best-known alternative bio-pesticide which has the potential to replace the use of conventional pesticides, as it is more environmentally friendly. The main objective of the paper is to obtain the best extraction solvent for optimizing the yield in rotenone extraction. Rotenone was extracted from Derris root using three different parts of roots and three types of solvent in Normal Soaking Extraction (NSE). The types of Derris roots are: (1) Fine root (2) Coarse root (3) Stem. The three types of solvent system are: (1) Acetone 95 % (v/v), (2) Chloroform 99.9 % (v/v) and (3) a mixture of ethanol: H2O (9:1) added with oxalic acid (1mg/ml). The liquid crude extracts were further cleaned up to remove the fine debris of roots. The presence of rotenone was confirmed using qualitative analysis Thin Layer Chromatography (TLC) and thereupon the determination of rotenone content was carried out using High Performance Liquid Chromatography (HPLC). From the results obtained, it was found that the Normal Soaking Extraction (NSE) using acetone 95 % (v/v) was the best method to extract the highest yield of rotenone; 1.14 % (w/w)

Ferromagnetic Ga₁ˍₓ Mnₓ As produced by ion implantation and pulsed-laser melting

We demonstrate the formation of ferromagneticGa₁ˍₓMnₓAsfilms by Mn ion implantation into GaAs followed by pulsed-laser melting. Irradiation with a single excimer laser pulse results in the epitaxial regrowth of the implanted layer with Mn substitutional fraction up to 80% and effective Curie temperature up to 29 K for samples with a maximum Mn concentration of x≈0.03. A remanent magnetization persisting above 85 K has been observed for samples with x≈0.10, in which 40% of the Mn resides on substitutional lattice sites. We find that the ferromagnetism in Ga₁ˍₓMnₓAs is rather robust to the presence of structural defects.The work at the Lawrence Berkeley National Laboratory was supported by the Director, Office of Science, Office of Basic Energy Sciences, Division of Materials Sciences and Engineering, of the U.S. Department of Energy under Contract No. DE-AC03-76SF00098. The work at Harvard was supported by NASA Grant No. NAG8-1680. One of the authors ~M.A.S.! acknowledges support from an NSF Graduate Research Fellowship

Scattering length for helium atom-diatom collision

We present results on the scattering lengths of ^4He--^4He_2 and ^3He--^4He_2 collisions. We also study the consequence of varying the coupling constant of the atom-atom interaction.Comment: Contribution to Proceedings of the International Workshop ``Critical Stability of Few-Body Quantum Systems'' (Dresden, October 17--22, 2005

Texture Measurement by Neutron Diffraction for A1 Nonstandard Steel Bars

Texture measurements are used to determine the orientation distribution of crystalline grains in a polycrystalline sample. A material is termed textured if the grains are aligned in a preferred orientation along certain lattice planes. The texture is usually introduced in the fabrication process (e.g. rolling of thin sheet metal, deposition, etc.) and affects the material properties by introducing structural anisotropy. The pole figure is the starting point of neutron texture analysis. Texture properties in an non-standard austenite Fe-Ni low carbon alloywere measured by the neutron diffraction method with the PD/Residual Stress Diffractometer DN3 apparatus in BATAN. In this paper, effects of hot rolling on the texture are studied using ODF plots generated by MAUD application code developed by Lutteroti. It was found that The ODF plots for the A1 as cast and 1200 °C hot rolled specimens show typical patterns for recrystallized and rolled cubic structure. The pole figures for this plate are consistent with Face Centered Cubic (FCC) rolling textures

Progress in Monte Carlo calculations of Fermi systems: normal liquid 3He

The application of the diffusion Monte Carlo method to a strongly interacting Fermi system as normal liquid $^3$He is explored. We show that the fixed-node method together with the released-node technique and a systematic method to analytically improve the nodal surface constitute an efficient strategy to improve the calculation up to a desired accuracy. This methodology shows unambiguously that backflow correlations, when properly optimized, are enough to generate an equation of state of liquid $^3$He in excellent agreement with experimental data from equilibrium up to freezing.Comment: 14 pages, 3 eps figure

The Phenomena of Spreading of Hydrotalcite Sol on A Porous Silica Surface Governed by Marangoni Effect

Wetting phenomena plays a crucial role in a wide range of technological applications. Spreading of liquids on solids involving phase change is encountered in many areas ranging from biological systems to industrial applications such as coatings, printing, painting and spraying. The fundamental study on wetting of membrane precursors namely hydrotalcite sols on a porous silica surface with different types of precursor material was successfully carried out. Relationship between the contact angle of a hydrotalcite droplet on silica surface and the Marangoni effect was also investigated. The presence of PVA in hydrotalcite sols was found to influence the rheological properties of the sols significantly, resulting in higher viscosity and ultimately leading to lower contact angle on solid surfaces. The degree of hydrotalcite's philicity on a substrate was improved by the addition of PVA solution. In this study, the spreading of a liquid droplet on a solid surface controlled by a surface tension gradient, due to Marangoni effect was found to drive better spreading of the liquid droplet. Marangoni Number, Ma was found to be proportionally related with the surface tension of the sols but inversely proportional to contact angles of the sols. Marangoni forces that decreased the contact angle, promoted spreading of hydrotalcite droplets on the selected glass substrates.Keywords: contact angle, hydrotalcite, marangoni effect, spreading, wetting evolutio

A slope-theory approach to electrical probe recording on phase-change media

Copyright © 2005 American Institute of Physics. This article may be downloaded for personal use only. Any other use requires prior permission of the author and the American Institute of Physics. The following article appeared in Journal of Applied Physics 97 (2005) and may be found at http://link.aip.org/link/?JAPIAU/97/103537/1notes: The first paper to address theoretically the issue of writing resolution in electrical probe recording on phase-change media. The theory combined the thermal, kinetic, and electronic properties of the storage medium in an analytical framework to predict the ultimate writing resolutions of this technology. The theory also provided directions in material selection and design to increase the resolution and hence storage density of this new technology. The work led to invited presentations at on probe-based storage at the IEEE/IoP Magnetics Society Wohlfarth Lecture Meeting, London, April 2005 and at the Seagate Research Conclave, June 2007 at Sprintown, Northern Ireland.A theoretical approach to predicting the spatial extent of the amorphous to crystalline transition region during the probe recording process on phase-change storage media is presented. The extent of this transition region determines the ultimate achievable linear density for data storage using phase-change materials. The approach has parallels with the slope theory used to find magnetic transition lengths in magnetic recording, and shows that the amorphous to crystalline transition length can be minimized by reducing the thickness of the phase-change layer, by minimizing lateral heat flow, and by maximizing the ratio of the activation energy for crystallization to the transition temperature Ec/Tt

High-quality variational wave functions for small 4He clusters

We report a variational calculation of ground state energies and radii for 4He_N droplets (3 \leq N \leq 40), using the atom-atom interaction HFD-B(HE). The trial wave function has a simple structure, combining two- and three-body correlation functions coming from a translationally invariant configuration-interaction description, and Jastrow-type short-range correlations. The calculated ground state energies differ by around 2% from the diffusion Monte Carlo results.Comment: 5 pages, 1 ps figure, REVTeX, submitted to Phys. Rev.

A comprehensive overview of electric vehicle charging using renewable energy

The integration of PV with the electric vehicle (EV) charging system has been on the rise due to several factors, namely continuous reduction in the price of PV modules, rapid growth in EV and concern over the effects of greenhouse gases. Over the years, numerous papers have been published on EV charging using the standard utility (grid) electrical supply; however, there seems to be an absence of a comprehensive overview using PV as one of the components for the charger. With the growing interest in this topic, it is timely to review, summarize and update all the related works on PV charging, and to present it as a single reference. For the benefit of a wider audience, the paper also includes the bries description on EV charging stations, background of EV, as well as a brief description of PV systems. Some of the main features of battery management system (BMS) for EV battery are also presented. It is envisaged that the information gathered in this paper will be a valuable one–stop source of information for researchers working in this topic