NASA Tech Briefs, September 2011

Topics covered include: Fused Reality for Enhanced Flight Test Capabilities; Thermography to Inspect Insulation of Large Cryogenic Tanks; Crush Test Abuse Stand; Test Generator for MATLAB Simulations; Dynamic Monitoring of Cleanroom Fallout Using an Air Particle Counter; Enhancement to Non-Contacting Stress Measurement of Blade Vibration Frequency; Positively Verifying Mating of Previously Unverifiable Flight Connectors; Radiation-Tolerant Intelligent Memory Stack - RTIMS; Ultra-Low-Dropout Linear Regulator; Excitation of a Parallel Plate Waveguide by an Array of Rectangular Waveguides; FPGA for Power Control of MSL Avionics; UAVSAR Active Electronically Scanned Array; Lockout/Tagout (LOTO) Simulator; Silicon Carbide Mounts for Fabry-Perot Interferometers; Measuring the In-Process Figure, Final Prescription, and System Alignment of Large; Optics and Segmented Mirrors Using Lidar Metrology; Fiber-Reinforced Reactive Nano-Epoxy Composites; Polymerization Initiated at the Sidewalls of Carbon Nanotubes; Metal-Matrix/Hollow-Ceramic-Sphere Composites; Piezoelectrically Enhanced Photocathodes; Iridium-Doped Ruthenium Oxide Catalyst for Oxygen Evolution; Improved Mo-Re VPS Alloys for High-Temperature Uses; Data Service Provider Cost Estimation Tool; Hybrid Power Management-Based Vehicle Architecture; Force Limit System; Levitated Duct Fan (LDF) Aircraft Auxiliary Generator; Compact, Two-Sided Structural Cold Plate Configuration; AN Fitting Reconditioning Tool; Active Response Gravity Offload System; Method and Apparatus for Forming Nanodroplets; Rapid Detection of the Varicella Zoster Virus in Saliva; Improved Devices for Collecting Sweat for Chemical Analysis; Phase-Controlled Magnetic Mirror for Wavefront Correction; and Frame-Transfer Gating Raman Spectroscopy for Time-Resolved Multiscalar Combustion Diagnostics

Modeling and Experimental Techniques to Demonstrate Nanomanipulation With Optical Tweezers

The development of truly three-dimensional nanodevices is currently impeded by the absence of effective prototyping tools at the nanoscale. Optical trapping is well established for flexible three-dimensional manipulation of components at the microscale. However, it has so far not been demonstrated to confine nanoparticles, for long enough time to be useful in nanoassembly applications. Therefore, as part of this work we demonstrate new techniques that successfully extend optical trapping to nanoscale manipulation. In order to extend optical trapping to the nanoscale, we must overcome certain challenges. For the same incident beam power, the optical binding forces acting on a nanoparticle within an optical trap are very weak, in comparison with forces acting on microscale particles. Consequently, due to Brownian motion, the nanoparticle often exits the trap in a very short period of time. We improve the performance of optical traps at the nanoscale by using closed-loop control. Furthermore, we show through laboratory experiments that we are able to localize nanoparticles to the trap using control systems, for sufficient time to be useful in nanoassembly applications, conditions under which a static trap set to the same power as the controller is unable to confine a same-sized particle. Before controlled optical trapping can be demonstrated in the laboratory, key tools must first be developed. We implement Langevin dynamics simulations to model the interaction of nanoparticles with an optical trap. Physically accurate simulations provide a robust platform to test new methods to characterize and improve the performance of optical tweezers at the nanoscale, but depend on accurate trapping force models. Therefore, we have also developed two new laboratory-based force measurement techniques that overcome the drawbacks of conventional force measurements, which do not accurately account for the weak interaction of nanoparticles in an optical trap. Finally, we use numerical simulations to develop new control algorithms that demonstrate significantly enhanced trapping of nanoparticles and implement these techniques in the laboratory. The algorithms and characterization tools developed as part of this work will allow the development of optical trapping instruments that can confine nanoparticles for longer periods of time than is currently possible, for a given beam power. Furthermore, the low average power achieved by the controller makes this technique especially suitable to manipulate biological specimens, but is also generally beneficial to nanoscale prototyping applications. Therefore, capabilities developed as part of this work, and the technology that results from it may enable the prototyping of three-dimensional nanodevices, critically required in many applications

Polyelectrolyte nanostructures formed in the moving contact line: fabrication, characterization and application: Polyelectrolyte nanostructures formed in the moving contact line: fabrication, characterization and application

Having conducted the research described in this thesis I found that there exists a possibility to produce polyelectrolyte nanostructures on hydrophobic surfaces by application of the moving contact line approach. It was demonstrated that the morphology of nanostructures displays a range of structure variations from root-like to a single wire structure with a high anisotropy and aspect ratio (providing diameters of several nanometers and the length limited by the sample surface dimensions). Such nanostructures can be produced exactly on the spot of interest or can be transferred from the surface where they were produced to any other surfaces by the contact printing technique. A model describing the polymer deposition during the moving contact line processes on hydrophobic surfaces has been proposed. The application of this model provides the ground for an explanation of all the obtained experimental data. Utilizing moving contact line approach aligned one-dimensional polycation structures were fabricated and these structures were used as templates for assembling amphiphile molecules. Quasiperiodic aligned and oriented nanostructures of polyelectrolyte molecules formed in moving droplets were utilized for fabrication of electrically conductive one-dimensional nanowires

USE OF HIGH SURFACE NANOFIBROUS MATERIALS IN MEDICINE

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DEVELOPMENT OF FUNCTIONAL NANOCOMPOSITE MATERIALS TOWARDS BIODEGRADABLE SOFT ROBOTICS AND FLEXIBLE ELECTRONICS

World population is continuously growing, as well as the influence we have on the ecosystem\u2019s natural equilibrium. Moreover, such growth is not homogeneous and it results in an overall increase of older people. Humanity\u2019s activity, growth and aging leads to many challenging issues to address: among them, there are the spread of suddenly and/or chronic diseases, malnutrition, resource pressure and environmental pollution. Research in the novel field of biodegradable soft robotics and electronics can help dealing with these issues. In fact, to face the aging of the population, it is necessary an improvement in rehabilitation technologies, physiological and continuous monitoring, as well as personalized care and therapy. Also in the agricultural sector, an accurate and efficient direct measure of the plants health conditions would be of help especially in the less-developed countries. But since living beings, such as humans and plants, are constituted by soft tissues that continuously change their size and shapes, today\u2019s traditional technologies, based on rigid materials, may not be able to provide an efficient interaction necessary to satisfy these needs: the mechanical mismatch is too prohibitive. Instead, soft robotic systems and devices can be designed to combine active functionalities with soft mechanical properties that can allow them to efficiently and safely interact with soft living tissues. Soft implantable biomedical devices, smart rehabilitation devices and compliant sensors for plants are all applications that can be achieved with soft technologies. The development of sophisticated autonomous soft systems needs the integration on a unique soft body or platform of many functionalities (such as mechanical actuation, energy harvesting, storage and delivery, sensing capabilities). A great research interest is recently arising on this topic, but yet not so many groups are focusing their efforts in the use of natural-derived and biodegradable raw materials. In fact, resource pressure and environmental pollution are becoming more and more critical problems. It should be completely avoided the use of in exhaustion, pollutant, toxic and non-degradable resources, such as lithium, petroleum derivatives, halogenated compounds and organic solvents. So-obtained biodegradable soft systems and devices could then be manufactured in high number and deployed in the environment to fulfil their duties without the need to recover them, since they can safely degrade in the environment. The aim of the current Ph.D. project is the use of natural-derived and biodegradable polymers and substances as building blocks for the development of smart composite materials that could operate as functional elements in a soft robotic system or device. Soft mechanical properties and electronic/ionic conductive properties are here combined together within smart nanocomposite materials. The use of supersonic cluster beam deposition (SCBD) technique enabled the fabrication of cluster-assembled Au electrodes that can partially penetrate into the surface of soft materials, providing an efficient solution to the challenge of coupling conductive metallic layers and soft deformable polymeric substrates. In this work, cellulose derivatives and poly(3-hydroxybutyrate) bioplastic are used as building blocks for the development of both underwater and in-air soft electromechanical actuators that are characterized and tested. A cellulosic matrix is blended with natural-derived ionic liquids to design and manufacture completely biodegradable supercapacitors, extremely interesting energy storage devices. Lastly, ultrathin Au electrodes are here deposited on biodegradable cellulose acetate sheets, in order to develop transparent flexible electronics as well as bidirectional resistive-type strain sensors. The results obtained in this work can be regarded as a preliminary study towards the realization of full natural-derived and biodegradable soft robotic and electronic systems and devices

Dielectrophoresis Control of Semiconductor Nanowires for Sensing Technology

Semiconductor nanowires (NWs) synthesis successes have given keys to unprecedented nano-scale sensitivity opening up new opportunities in device applications. NWs’ potential relies upon the possibility of engineering and modifying properties such as sensitivity and carrier transport, by tailoring the NWs’ morphology and conductivity. New challenges have taken place with the downscaling of electronics for NWs integration and assembly techniques. Amongst a large variety of integration techniques, dielectrophoresis (DEP) is a powerful tool for the precise manipulation of NWs of different compositions and sizes. However, experimental implementation and analysis with DEP often lack depth regarding the optimisation of the technique and the effects of the parameters on the performances of the final devices, which is crucial for the understanding of NWs’ electric transport properties and technology improvement. Consequently, this thesis presents a comprehensive study of the experimental implementation of DEP which is of paramount importance to obtaining optimum conditions for NWs alignment. With this aim in mind, the presented work demonstrates a detailed investigation of the electrical and optical properties of germanium (Ge) and gallium-arsenide-bismuth (GaAsBi) NWs-based devices by DEP as a function of the collection frequency. The Ge and GaAsBi NWs were obtained by MOVPE and MBE respectively as a collaborative work with the Institute of Material for Electronic and Magnet (Italy) for the Ge NWs, and with the research team of Dr Robert Richard at the University of Sheffield (Department of Electrical Engineering and Electronics) for the GaAsBi NWs. Firstly, to maximise NWs alignment precision, optimum DEP parameters are for the first time thoroughly extracted by testing the effects of different mediums (chemical inertia, volatility and contact angle) and electrode designs (gradients and electric field). Secondly, fabricated with a DEP frequency range of 500 kHz to 10 MHz the devices were electrically characterised using voltage-current response. An asymmetric diode-like behaviour was found to be originating from heterostructured Ge NWs specifically orientated by electrophoresis combined with DEP. This result is particularly promising for orientation control demonstrated for the first time, tuning and altering current response from chemically heterostructured nanowires. A particular focus was given to the effect of increasing frequency on the device performances such as carrier transport. Despite a decrease of aligned NWs corroborating theoretical analysis, increasing frequency collected higher conductivity Ge NWs with carrier mobility improving from 2θ at 500 kHz to 4.38θ at 10 MHz demonstrated using Mott-Gurney, and GaAsBi NWs with carrier mobility increasing from 5.29 ± 0.027 to 100 ± 0.70 cm2 V−1.s−1 at 500 kHz and 10 MHz demonstrated using the Fermi-velocity law. Such selectivity is of great potential to improve sensing technology transduction. Using optimum parameters previously found, a low-cost and simple voltage divider system joined to DEP is demonstrated for the first time to improve the alignment technique of a single Ge nanowire. The resulting spectral response was consistent with optical characterisations found in the literature for a single Ge nanowire and demonstrated high sensitivity near-infrared and communication wavelength as confirmed with a high responsivity of 6.2 x 105 A/W at 1550 nm. Such high resistivity is amongst the highest ever obtained for NWs. Furthermore, a NWs-based biosensor for the spike protein of the SARS-CoV-2 was fabricated by multilayered surface functionalisation evidenced by Raman spectroscopy. Upon exposure to increasing concentration of the protein, the biosensors transduced increasing current response with a working range of at least 1 aM to 100 fM. Selectivity to the spike protein was testified using bovine serum albumin as a negative control reference. The GaAsBi NWs were for the first time fully characterised and implemented as devices by DEP. The NWs surface roughness showcased the importance of surface properties that influenced DEP collection and carrier transport. Spectral responses from the devices brought to light the different bismuth content at the origin of reduced band-gap energy shown by the cut-off energies of the spectrum. With a Bi content increase of roughly 1% in GaAs the photodetectors presented high responsivity from 1.3 x 104 A/W to 5.6 x 104 A/W. Effective NWs-based biosensors and photodetectors were proof of concept devices that corroborate NWs and dielectrophoresis functionality paving the way to future nanotechnology improvement

Nanogenerators in Korea

Fossil fuels leaded the 21st century industrial revolution but caused some critical problems such as exhaustion of resources and global warming. Also, current power plants require too much high cost and long time for establishment and facilities to provide electricity. Thus, developing new power production systems with environmental friendliness and low-cost is critical global needs. There are some emerging energy harvesting technologies such as thermoelectric, piezoelectric, and triboelectric nanogenerators, which have great advantages on eco-friendly low-cost materials, simple fabrication, and various operating sources. Since the introduction of various energy harvesting technologies, many novel designs and applications as power suppliers and physical sensors in the world have been demonstrated based on their unique advantages. In this Special Issue, we would like to address and share basic approaches, new designs, and industrial applications related to thermoelectric, piezoelectric, and triboelectric devices which are on-going in Korea. With this Special Issue, we aim to promote fundamental understanding and to find novel ways to achieve industrial product manufacturing for energy harvesters

Engineering for a changing world: 60th Ilmenau Scientific Colloquium, Technische Universität Ilmenau, September 04-08, 2023 : programme

In 2023, the Ilmenau Scientific Colloquium is once more organised by the Department of Mechanical Engineering. The title of this year’s conference “Engineering for a Changing World” refers to limited natural resources of our planet, to massive changes in cooperation between continents, countries, institutions and people – enabled by the increased implementation of information technology as the probably most dominant driver in many fields. The Colloquium, supplemented by workshops, is characterised but not limited to the following topics: – Precision engineering and measurement technology Nanofabrication – Industry 4.0 and digitalisation in mechanical engineering – Mechatronics, biomechatronics and mechanism technology – Systems engineering – Productive teaming - Human-machine collaboration in the production environment The topics are oriented on key strategic aspects of research and teaching in Mechanical Engineering at our university

Embedded Energy Landscapes In Soft Matter For Micro-Robotics And Reconfigurable Structures

The ability to manipulate microscale objects with precision to form complex structures is central to the field of micro-robotics and to the realization of reconfigurable systems. Understanding and exploiting the forces that dominate at the microscale in complex environments pose major challenges and open untapped opportunities. This is particularly the case for micro-particles in soft milieu like fluid interfaces or nematic liquid crystalline fluids, which deform or reorganize around dispersed colloids or near bounding surfaces. These energetically costly deformations can be designed as embedded energy landscapes, a form of physical intelligence, to dictate emergent colloidal interactions. The fluid nature of these soft milieu allows colloids to move to minimize the free energy and externally forced robotic structures to re-write the embedded energy landscapes in the domain. Such physically intelligent systems are of great interest at the intersection of materials science and micro-robotics. Micro-particles on fluid interfaces deform the interface shape, migrate, and assemble to minimize the capillary energy. In the first part of my thesis, I design and fabricate a magnetic micro-robot as a mobile curvature source to interact with passive colloids on the water/oil interface. An analytical expression that includes both capillary and hydrodynamic interactions is derived and captures the main feature of experimental observations. I further demonstrate multiple micro-robotic tasks including directed assembly, cargo carrying, desired release and cargo delivery on the interface. Micro-particles in confined nematic liquid crystals (NLCs) distort the nematic director field, generating interactions. These interactions depend strongly on the colloids shape and surface chemistry, geometric frustration of director field and behavior of dynamic topological defects. To probe far-from-equilibrium dynamics, I fabricate a magnetic disk with hybrid anchoring. Upon controlled rotation, the disk’s companion defect undergoes periodic rearrangement, executing a complex swim stroke that propels disk translation. I study this new swimming modality in both high and low Ericksen number regimes. At high rotation rates, the defect elongates significantly adjacent to the disk, generating broken symmetries that allow steering of the disk. This ability is exploited in path planning. Thereafter, I design a four-armed micro-robot as a mobile distortion source to promote passive colloids assembly at particular sites via emergent interactions in NLCs whose strengths are characterized and found to be several orders of magnitude larger than thermal energies. While the strength of theses interactions allows colloidal cargo to be carried with the micro-robot during translation, it poses challenges for cargo release. We find that rotation of this micro-robot generates a complex dynamic defect-sharing event with colloidal cargo that spurs cargo release. Thereafter, I demonstrate the ability to exploit NLC elastodynamics to construct reconfigurable colloidal structures in a micro-robotics platform. At the colloidal scale, rotation dynamics are easier to generate, and this motivated me to exploit the topological swimming modality of the micro-robot. Using programmable rotating fields to direct the micro-robot’s motion, I achieve fully autonomous cargo manipulations including approach, assembly, transport and release. The ability to dynamically manipulate micro-particles and their structures in soft matter systems with embedded energy landscapes, as demonstrated in this thesis, creates new possibilities for micro-robotics and reconfigurable systems

NASA Tech Briefs, June 2006

Topics covered include: Magnetic-Field-Response Measurement-Acquisition System; Platform for Testing Robotic Vehicles on Simulated Terrain; Interferometer for Low-Uncertainty Vector Metrology; Rayleigh Scattering for Measuring Flow in a Nozzle Testing Facility; "Virtual Feel" Capaciflectors; FETs Based on Doped Polyaniline/Polyethylene Oxide Fibers; Miniature Housings for Electronics With Standard Interfaces; Integrated Modeling Environment; Modified Recursive Hierarchical Segmentation of Data; Sizing Structures and Predicting Weight of a Spacecraft; Stress Testing of Data-Communication Networks; Framework for Flexible Security in Group Communications; Software for Collaborative Use of Large Interactive Displays; Microsphere Insulation Panels; Single-Wall Carbon Nanotube Anodes for Lithium Cells; Tantalum-Based Ceramics for Refractory Composites; Integral Flexure Mounts for Metal Mirrors for Cryogenic Use; Templates for Fabricating Nanowire/Nanoconduit- Based Devices; Measuring Vapors To Monitor the State of Cure of a Resin; Partial-Vacuum-Gasketed Electrochemical Corrosion Cell; Theodolite Ring Lights; Integrating Terrain Maps Into a Reactive Navigation Strategy; Reducing Centroid Error Through Model-Based Noise Reduction; Adaptive Modeling Language and Its Derivatives; Stable Satellite Orbits for Global Coverage of the Moon; and Low-Cost Propellant Launch From a Tethered Balloo