Recherche numérique et expérimentale sur les propriétés de décharge et les caractéristiques de propagation électromagnétique dans les torches à plasma micro-ondes

Ce travail vise à mieux comprendre les décharges dans les torches à plasma micro-ondes, en étudiant les caractéristiques de propagation des ondes électromagnétiques et les propriétés diélectriques de plasma dans les torches à plasma micro-ondes à base d’un guide d'onde rectangulaire dans différentes conditions de fonctionnement. En premier lieu, le mode de propagation des ondes électromagnétiques dans le tube à décharge plasma, leurs conditions d'existence ont été étudiés théoriquement étudiés et validés numériquement par un outil de modélisation électromagnétique rigoureux, avec l'hypothèse de propriétés de plasma constantes lorsque de la production de décharge plasma. Ensuite, sur la base de l’hypothèse selon laquelle la torche à plasma micro-ondes deviendra un convertisseur de mode guide d'onde-ligne quasicoaxiale lorsque la décharge se produit, des expériences sont menées pour étudier les effets du tube de verre sur l'efficacité du conversion en fonction de la puissance micro-onde, de pressions et de débits d'entrée de gaz afin d'explorer la possibilité d'améliorer l'efficacité du couplage par micro-ondes plasma en faisant une étude paramétrique complète. Troisièmement, un modèle de fluide bidimensionnel est proposé pour simuler les décharges d'argon dans la torche à plasma à micro-ondes sous pression atmosphérique, en utilisant l'approximation de la diffusion ambipolaire et la distribution axisymétrique du champ micro-ondes dans le tube à décharge. Avec ce modèle simplifié, le mécanisme du changement de longueur de la colonne de plasma sous différentes puissances hyperfréquences et débits entrants de gaz, ainsi que le mécanisme du problème de surchauffe du tube de verre ont été étudiés numériquement. Enfin, un modèle tridimensionnel est également proposé pour étudier les décharges dans les torches à plasma micro-ondes. Les décharges d'argon sous pression atmosphérique dans deux types de torches à plasma microondes avec différents tubes en verre ont été modélisées et comparées à la simulation bidimensionnelle. Il est montré que le tube à décharge avec enveloppe métallique dans les torches à plasma micro-ondes peut devenir un guide d’ondes de type quasi-coaxial lorsque les propriétés de décharge répondent à certaines exigences. Avec cette transition de structure de guide d’ondes, le tube à décharge cylindrique permet à l’onde hyperfréquence de pénétrer dans le tube à décharge et de se propager le long de la colonne de plasma vers les deux extrémités du tube en verre sans être limité par une fréquence de coupure. Ces conclusions peuvent aider à mieux comprendre les propriétés de décharge et les caractéristiques de propagation des microondes dans les torches à plasma micro-ondes et à contribuer à l'optimisation des torches à microondes actuelles ou à la conception de nouveaux types de torches à plasm

Temperature- and Time-Dependent Dielectric Measurements and Modelling on Curing of Polymer Composites

In this book a test set for dielectric measurements at 2.45 GHz during curing of polymer composites is developed. Fast reconstruction is solved using a neural network algorithm. Modeling of the curing process at 2.45 GHz using both dielectric constant and dielectric loss factor results in more accurate model compared to low frequency modelling that only uses the loss factor. Effect of various hardeners and different amount of filler is investigated

Temperature- and Time-Dependent Dielectric Measurements and Modelling on Curing of Polymer Composites

In this book a test set for dielectric measurements at 2.45 GHz during curing of polymer composites is developed. Fast reconstruction is solved using a neural network algorithm. Modeling of the curing process at 2.45 GHz using both dielectric constant and dielectric loss factor results in more accurate model compared to low frequency modelling that only uses the loss factor. Effect of various hardeners and different amount of filler is investigated

MICROWAVE HEATING SIMULATION OF METALS AND DIELECTRIC CERAMICS

The research objectives proposed to study metal processing using a modular industrial microwave oven. The intent of the oven was to perform casting for metal processing purposes. The research objectives were to validate the ovens performance for melting copper and then to compare the results to modeling data. The initial intent was to test the oven for its capability to melt metals. Most researchers would argue that the industrial microwave could not be used for metal processing. However, this research proposed to answer the question as to whether the industrial microwave oven could be used for processing metals or not. The strength of the research lies in the fact that the technology had not been tested on a global scale and industry has not accepted the capabilities of the oven. Nevertheless, developmental efforts have continued and the microwave technology has not ceased to be developed. Although there would be problematic issues, the focus was not to prove the theoretical equations and derive large data sets for the experiments; but to validate that the oven could be used for processing metals and used in an industrial setting where alternative metal processing technologies exist. In order to perform the research, the unit was designed and manufactured and auxiliary components purchased. The research proposed to cast copper in the experimental modular microwave oven and compare the data to the modeling data. Data collection was basically coordinated using thermocouples along the mold and an optical pyrometer for the metal. The final casts were analyzed for both metallurgical and chemical characteristics. A model was designed based upon the dimensions and operational parameters of the experimental oven and data comparison was made. A simulator was then derived using computer code to formulate a user interface panel and simulation environment representative of a laboratory environment. In order to pursue the research goals, material properties were derived as functions of temperature. For the electromagnetic properties the dielectric permittivity was required along with suggestions for the electromagnetic boundary conditions. An experiment was developed and the properties were measured for several dielectric materials; thus the most suitable ceramic material chosen

An Investigation of Radiometer and Antenna Properties for Microwave Thermography

Microwave thermography obtains information about the subcutaneous body temperature by a spectral measurement of the intensity of the natural thermally generated radiation emitted by the body tissues. At lower microwave frequencies the thermal radiation can penetrate through biological tissue for significant distances. The microwave thermal radiation from inside the body can be detected and measured non-invasively at the skin surface by the microwave thermography technique, which uses a radiometer to measure the radiation which is received from an antenna on the skin. In the microwave region the radiative power received from a volume of material has a dependence on viewed tissue temperature T(r) of the form, where k is the Boltzmann's constant, B the measurement bandwidth, c(r) is the relative contribution from a volume element dv (the antenna weighting function). The weighting function, c(r), depends on the structure and the dielectric properties of the tissue being viewed, the measurement frequency and the characteristics of the antenna. In any practical radiometer system the body microwave thermal signal has to be measured along with a similar noise signal generated in the radiometer circuits. The work described in this thesis is intended to lead to improvement in the performance of microwave thermography equipment through investigations of antenna weighting functions and radiometer circuit noise sources. All work has been carried out at 3.2 GHz, the central operating frequency of the existing Glasgow developed microwave thermography system. The effects of input circuit losses on the operation of the form of Dicke radiometer used for the Glasgow equipment have been investigated using a computational model and compared with measurements made on test circuits. Very good agreement has been obtained for modelled and measured behaviour. The losses contributed by the microstrip circuit structure, that must be used in the radiometer at 3.2 GHz, have been investigated in detail. Microwave correlation radiometry, by "add and square" method, has been applied to the received signals from a crossed-pair antenna arrangement, the antennas being arranged to view a common region at a certain depth. The antenna response has been investigated using a noise source and by the nonresonant perturbation technique. The received pattern formed by the product of the individual antenna patterns gives a maximum depth in phantom dielectric material. The depth can be adjusted by changing the spacing of the antennas and the phase in an antenna path. However, the pattern is modulated by a set of positive and negative interference fringes so that the complete receive pattern has a complicated form. On uniform temperature distributions the total radiometric signal is zero with the positive and negative contributions cancelling each other out. The fringe modulation can be removed by placing the antennas close enough together, The pattern is then simple and gives a modest maximum response at a known depth in a known material. The radiometer system remains sensitive to the temperature gradients only and the wide range of dielectric properties and tissue structures in the region being investigated usually makes the system response difficult to interpret. For crossed-pair antennas in phase the effective penetration depth in high-and medium-water content tissues is about 2.5 cm at a frequency of 3.2 GHz. The field pattern observed was of the form expected from the measurements of the individual antenna behaviour with the appropriate interference pattern superimposed. The nonresonant perturbation technique has been developed and applied to assist the development of the medical application of both microwave thermographic temperature measurement and microwave hyperthermia induction. These techniques require the electromagnetic field patterns of the special antennas used to be known. These antennas are often formed by short lengths of rectangular or cylindrical waveguide loaded with a low-loss dielectric material to achieve good coupling to body tissues. The high microwave attenuation in biological materials requires the field configurations to be measured close to the antenna aperture in the near-field wave. The nonresonant perturbation is a simple technique which can be used to measure electromagnetic fields in lossy material close to the antenna. It has been applied here to measure accurately the antenna weighting function and the effective penetration depth in tissue simulating dielectric phantom materials. (Abstract shortened by ProQuest.)

Printing conductive traces to enable high frequency wearable electronics applications

With the emergence of the Internet of Things (IoT), wireless body area networks (WBANs) are becoming increasingly pervasive in everyday life. Most WBANs are currently working at the IEEE 802.15.4 Zigbee standard. However there are growing interests to investigate the performance of BANs operating at higher frequencies (e.g. millimetre-wave band), due to the advantages offered compared to those operating at lower microwave frequencies. This thesis aims to realise printed conductive traces on flexible substrates, targeted for high frequency wearable electronics applications. Specifically, investigations were performed in the areas pertaining to the surface modification of substrates and the electrical performance of printed interconnects. Firstly, a novel methodology was proposed to characterise the dielectric properties of a non-woven fabric (Tyvek) up to 20 GHz. This approach utilised electromagnetic (EM) simulation to improve the analytical equations based on transmission line structures, in order to improve the accuracy of the conductor loss values in the gigahertz range. To reduce the substrate roughness, an UV-curable insulator was used to form a planarisation layer on a non-porous substrate via inkjet printing. The results obtained demonstrated the importance of matching the surface energy of the substrate to the ink to minimise the ink de-wetting phenomenon, which was possible within the parameters of heating the platen. Furthermore, the substrate surface roughness was observed to affect the printed line width significantly, and a surface roughness factor was introduced in the equation of Smith et al. to predict the printed line width on a substrate with non-negligible surface roughness (Ra ≤ 1 µm). Silver ink de-wetting was observed when overprinting silver onto the UV-cured insulator, and studies were performed to investigate the conditions for achieving electrically conductive traces using commercial ink formulations, where the curing equipment may be non-optimal. In particular, different techniques were used to characterise the samples at different stages in order to evaluate the surface properties and printability, and to ascertain if measurable resistances could be predicted. Following the results obtained, it was demonstrated that measurable resistance could be obtained for samples cured under an ambient atmosphere, which was verified on Tyvek samples. Lastly, a methodology was proposed to model for the non-ideal characteristics of printed transmission lines to predict the high frequency electrical performance of those structures. The methodology was validated on transmission line structures of different lengths up to 30 GHz, where a good correlation was obtained between simulation and measurement results. Furthermore, the results obtained demonstrate the significance of the paste levelling effect on the extracted DC conductivity values, and the need for accurate DC conductivity values in the modelling of printed interconnects

Mesoscale Optoelectronic Design of Wire-Based Photovoltaic and Photoelectrochemical Devices

The overarching theme of this thesis is mesoscale optical and optoelectronic design of photovoltaic and photoelectrochemical devices. In a photovoltaic device, light absorption and charge carrier transport are coupled together on the mesoscale, and in a photoelectrochemical device, light absorption, charge carrier transport, catalysis, and solution species transport are all coupled together on the mesoscale. The work discussed herein demonstrates that simulation-based mesoscale optical and optoelectronic modeling can lead to detailed understanding of the operation and performance of these complex mesostructured devices, serve as a powerful tool for device optimization, and efficiently guide device design and experimental fabrication efforts. In-depth studies of two mesoscale wire-based device designs illustrate these principles—(i) an optoelectronic study of a tandem Si|WO3 microwire photoelectrochemical device, and (ii) an optical study of III-V nanowire arrays. The study of the monolithic, tandem, Si|WO3 microwire photoelectrochemical device begins with development and validation of an optoelectronic model with experiment. This study capitalizes on synergy between experiment and simulation to demonstrate the model’s predictive power for extractable device voltage and light-limited current density. The developed model is then used to understand the limiting factors of the device and optimize its optoelectronic performance. The results of this work reveal that high fidelity modeling can facilitate unequivocal identification of limiting phenomena, such as parasitic absorption via excitation of a surface plasmon-polariton mode, and quick design optimization, achieving over a 300% enhancement in optoelectronic performance over a nominal design for this device architecture, which would be time-consuming and challenging to do via experiment. The work on III-V nanowire arrays also starts as a collaboration of experiment and simulation aimed at gaining understanding of unprecedented, experimentally observed absorption enhancements in sparse arrays of vertically-oriented GaAs nanowires. To explain this resonant absorption in periodic arrays of high index semiconductor nanowires, a unified framework that combines a leaky waveguide theory perspective and that of photonic crystals supporting Bloch modes is developed in the context of silicon, using both analytic theory and electromagnetic simulations. This detailed theoretical understanding is then applied to a simulation-based optimization of light absorption in sparse arrays of GaAs nanowires. Near-unity absorption in sparse, 5% fill fraction arrays is demonstrated via tapering of nanowires and multiple wire radii in a single array. Finally, experimental efforts are presented towards fabrication of the optimized array geometries. A hybrid self-catalyzed and selective area MOCVD growth method is used to establish morphology control of GaP nanowire arrays. Similarly, morphology and pattern control of nanowires is demonstrated with ICP-RIE of InP. Optical characterization of the InP nanowire arrays gives proof of principle that tapering and multiple wire radii can lead to near-unity absorption in sparse arrays of InP nanowires.</p

Modeling EMI Resulting from a Signal Via Transition Through Power/Ground Layers

Signal transitioning through layers on vias are very common in multi-layer printed circuit board (PCB) design. For a signal via transitioning through the internal power and ground planes, the return current must switch from one reference plane to another reference plane. The discontinuity of the return current at the via excites the power and ground planes, and results in noise on the power bus that can lead to signal integrity, as well as EMI problems. Numerical methods, such as the finite-difference time-domain (FDTD), Moment of Methods (MoM), and partial element equivalent circuit (PEEC) method, were employed herein to study this problem. The modeled results are supported by measurements. In addition, a common EMI mitigation approach of adding a decoupling capacitor was investigated with the FDTD method

Microwave NDT&E using open-ended waveguide probe for multilayered structures

Ph. D. Thesis.Microwave NDT&E has been proved to be suitable for inspecting of dielectric structures due to low attenuation in dielectric materials and free-space. However, the microwave responses from multilayered structures are complex as an interrogation of scattering electromagnetic waves among the layers and defects. In many practical applications, electromagnetic analysis based on analytic- and forward structural models cannot be generalised since the defect shape and properties are usually unknown and hidden beneath the surface layer. This research proposes the design and implementation of microwave NDT&E system for inspection of multilayered structures. Standard microwave open-ended rectangular waveguides in X, Ku and K bands (frequency range between 8-26.5 GHz) and vector network analyser (VNA) generating sweep frequency of wideband monochromatic waves have been used to obtain reflection coefficient responses over three types of challenging multilayered samples: (1) corrosion progression under coating, (2) woven carbon fibre reinforced polymer (CFRP) with impact damages, and (3) thermal coated glass fibre reinforced polymer (GFRP) pipe with inner flat-bottom holes. The obtained data are analysed by the selected feature extraction method extracting informative features and verify with the sample parameters (defect parameters). In addition, visualisation methods are utilised to improve the presentation of the defects and material structures resulting in a better interpretation for quantitative evaluation. The contributions of this project are summarised as follows: (1) implementation of microwave NDT&E scanning system using open-ended waveguide with the highest resolution of 0.1mm x 0.1 mm, based on the NDT applications for the three aforementioned samples; (2) corrosion stages of steel corrosion under coating have been successfully characterised by the principal component analysis (PCA) method; (3) A frequency selective based PCA feature has been used to visualise the impact damage at different impact energies with elimination of woven texture influences; (4) PCA and SAR (synthetic aperture radar) tomography together with time-offlight extraction, have been used for detection and quantitative evaluation of flat-bottom hole defects (i.e., location, size and depth). The results conclude that the proposed microwave NDT&E system can be used for detection and evaluation of multilayered structures, which its major contributions are follows. (1) The early stages (0-12month) of steel corrosion undercoating has been successfully characterised by mean of spectral responses from microwave opened rectangular waveguide probe and PCA. (2) The detection of low energy impact damages on CFRP as low as 4 Joules has been archived with microwave opened rectangular waveguide probe raster scan together with SAR imaging and PCA for feature extraction methods. (3) The inner flat-bottom holes beneath the thermal coated GFRP up to 11.5 mm depth has been successfully quantitative evaluated by open-ended waveguide raster scan using PCA and 3-D reconstruction based on SAR tomography techniques. The evaluation includes location, sizing and depth. Nevertheless, the major downside of feature quantities extracted from statistically based methods such as PCA, is it intensely relies on the correlation of the input dataset, and thus hardly link them with the physical parameters of the test sample, in particular, the complex composite architectures. Therefore, there are still challenges of feature extraction and quantitative evaluation to accurately determine the essential parameters from the samples. This can be achieved by a future investigation of multiple features fusion and complementary features.Ministry of Science and Technology of Royal Thai Government and Office of Educational Affairs, the Royal Thai Embass