Book of abstracts of the 14th International Symposium of Croatian Metallurgical Society - SHMD \u272020, Materials and metallurgy

Book of abstracts of the 14th International Symposium of Croatian Metallurgical Society - SHMD \u272020, Materials and metallurgy held in Šibenik, Croatia, June 21-26, 2020. Abstracts are organized in four sections: Materials - section A; Process metallurgy - Section B; Plastic processing - Section C and Metallurgy and related topics - Section D

Future Trends in Advanced Materials and Processes

The Special Issue “Future Trends in Advanced Materials and Processes” contains original high-quality research papers and comprehensive reviews addressing the relevant state-of-the-art topics in the area of materials focusing on relevant or innovative applications such as radiological hazard evaluations of non-metallic materials, composite materials' characterization, geopolymers, metallic biomaterials, etc

Effect of press slide speed and stroke on cup forming using a plain-woven carbon fiber thermoplastic composite sheet

Carbon-fiber-reinforced thermoplastic (CFRTP) is viewed as a prospective material for high-cycle production of CFRP parts. This paper deals with a process whereby a preheated thermoplastic plain-woven carbon fiber fabric sheet is formed into a circular cup by a mechanical servo-press. The effects of press parameters, specifically the bottom dead center and slide speed in the forming of CFRTP cup, on the press load, pressure, internal temperature, shape accuracy, and internal structure have been investigated. A plain-woven carbon-fiber-reinforced PA6 thermoplastic sheet was used. The sheet consisted of four layers of woven 3K carbon and had a thickness of 1 mm. The sheet was heated to 320°C under a halogen heater so that it would be around the recommended temperature for forming 260°C after transfer to the mold. The sheet was pressed into a circular cup shape by a cold mold while the periphery was cramped by a heated holder so as not to cool the sheet before it was pulled into the mold cave. Die clearance was designed considering the thickness increase due to the fiber concentration during the forming. By increasing the slide stroke to the bottom dead center, the applied press load was increased and the internal structure was improved, showing no voids. By increasing the slide speed, the final press load was reduced and shape accuracy was improved through a good pressure distribution on the mold. Measurement of the surface temperature of the sheet during the forming revealed that it remained in the melting region of the resin in the case of fast slide speed, but dropped below the melting temperature in the case of low slide speed. This difference apparently led to spring-in or spring-back after the forming. The experimental results indicate that appropriate balance among press speed, bottom dead center, and sheet temperature is important in the high-cycle forming of CFRTP. © 2016, Fuji Technology Press. All rights reserved

Metals Processing Laboratory Users (MPLUS) Facility Annual Report FY 2002 (October 1, 2001-September 30, 2002)

The Metals Processing Laboratory Users Facility (MPLUS) is a Department of Energy (DOE), Energy Efficiency and Renewable Energy, Industrial Technologies Program, user facility designated to assist researchers in key industries, universities, and federal laboratories in improving energy efficiency, improving environmental aspects, and increasing competitiveness. The goal of MPLUS is to provide access to the specialized technical expertise and equipment needed to solve metals processing issues that limit the development and implementation of emerging metals processing technologies. The scope of work can also extend to other types of materials. MPLUS has four primary user centers: (1) Processing--casting, powder metallurgy, deformation processing (including extrusion, forging, rolling), melting, thermomechanical processing, and high-density infrared processing; (2) Joining--welding, monitoring and control, solidification, brazing, and bonding; (3) Characterization--corrosion, mechanical properties, fracture mechanics, microstructure, nondestructive examination, computer-controlled dilatometry, and emissivity; and (4) Materials/Process Modeling--mathematical design and analyses, high-performance computing, process modeling, solidification/deformation, microstructure evolution, thermodynamic and kinetic, and materials databases A fully integrated approach provides researchers with unique opportunities to address technologically related issues to solve metals processing problems and probe new technologies. Access is also available to 16 additional Oak Ridge National Laboratory (ORNL) user facilities ranging from state-of-the-art materials characterization capabilities, and high-performance computing to manufacturing technologies. MPLUS can be accessed through a standardized user-submitted proposal and a user agreement. Nonproprietary (open) or proprietary proposals can be submitted. For open research and development, access to capabilities is provided free of charge, while for proprietary efforts, the user pays the entire project costs based on DOE guidelines for ORNL costs

Some Critical Issues for Injection Molding

This book is composed of different chapters which are related to the subject of injection molding and written by leading international academic experts in the field. It contains introduction on polymer PVT measurements and two main application areas of polymer PVT data in injection molding, optimization for injection molding process, Powder Injection Molding which comprises Ceramic Injection Molding and Metal Injection Molding, ans some special techniques or applications in injection molding. It provides some clear presentation of injection molding process and equipment to direct people in plastics manufacturing to solve problems and avoid costly errors. With useful, fundamental information for knowing and optimizing the injection molding operation, the readers could gain some working knowledge of the injection molding

Rational Design of Flexible and Stretchable Electronics based on 3D Printing

Flexible and stretchable electronics have been considered as the key component for the next generation of flexible devices. There are many approaches to prepare the devices, such as dip coating, spin coating, Mayer bar coating, filtration and transfer, and printing, etc. The effectiveness of these methods has been proven, but some drawbacks cannot be ignored, such as lacking pattern control, labor consuming, requiring complex pretreatment, wasting conductive materials, etc. In this investigation, we propose to adopt 3D printing technology to design flexible and stretchable electronics. The objective is to rationally design flexible and stretchable sensors, simplify the preparation process, form the sample with the complex desirable patterns, and promote the performance of the samples. The dissertation comprises of three major parts: water-induced polymer swelling and its application in soft electronics, utilizing 3D printing to transfer conductive layer into elastomer for building soft electronics, and 3D printing of functional devices. In the first part, we developed the soft electronics with wrinkled structure via 3D printing and water-induced polymer swelling, which can avoid some disadvantages in conventional method, e.g., pre-stretching and organic solvent-induced polymer swelling, including mechanical loss, negative effect to human health, and unidirectionally response to external deformation. Water-induced polymer swelling was achieved by introducing soluble particles into silicone matrixes and soaking the polymer composites in aqueous solution. We have investigated the characteristics and mechanisms of water-induced polymer swelling. Then, the conductive materials were deposited on the swollen sample to form the desired wrinkled structures for stretchable sensors. Furthermore, a dopamine layer was adopted to enhance the adhesion of matrix and conductive layer. The improvement was a key enabler to achieve superior electrical properties of 3D printed stretchable sensors for long-term cyclic stretching. We have demonstrated a series of human motion detection by using these stretchable strain sensors. Another part is designing flexible electrodes with desirable complex pattern by transferring a conductive layer into soft substrates during a 3D printing process. Taking advantage of extrusion pressure and polymer adhesion, the thin conductive layers were embedded into the printed polymer patterns, which can achieve conductive flexible electronics with desirable complex patterns. High-quality transfer has been achieved through adjusting conductive layer thickness, nozzle-to-substrate distance, and printing parameters, etc. Moreover, various printing patterns were created, and their properties were exhibited. The stretchable sensors showed an outstanding stress-strain relationship and electrical response to external deformations. The third part is about 3D printing of functional devices. In the collaborated study, the drug particles were introduced into silicone matrix to prepare the drug-eluting devices. When water molecules transported into the silicone matrix, the loaded drug particles decomposed and released nitric oxide (NO) enabling antibacterial properties. It is noted that 3D printing is creatively employed to form the desirable patterns. We also observed a self-wiring effect in the printing process, i.e., the printed device is covered by a drug-free layer due to the diffusion of a low viscosity silicone component during printing, which can be utilized to prevent drug release bursts and to form a gradient drug-loaded device. The printed samples showed a sustainable NO release and good antibacterial property. Furthermore, the water-induced polymer swelling was possible to be used as actuator in humidity environment. There are some highlights deserving emphasis in the dissertation. Firstly, the water-induced polymer swelling is proposed to develop the flexible and stretchable electronics. The findings have a wide potential application. Additionally, a drug-eluting polymer device with a drug-loaded bulk and a drug-free coating is prepared via leveraging self-wiring effect in 3D printing. The structure can regulate the drug release rate. On the other hand, the additive manufacturing platform offers unique opportunities to produce drug-eluting silicone devices in a customized manner. Finally, 3D printing is employed to encapsulate the conductive layers to achieve the flexible electronics with patterned structure and high performances. The facile and effective approach provides a distinctive view in advancing the development of stretchable electronics

Polymer Processing: Modeling and Correlations Finalized to Tailoring the Plastic Part Morphology and Properties

The analysis of polymer processing operations is a wide and complex subject; during polymer processing, viscoelastic fluids are forced to deform into desired geometries using non-homogeneous velocity and temperature fields down to solidification. The objective of analysis is the identification of processing conditions, which are finalized in the optimization of product final properties, which, in turn, are determined by the final part morphology. Depending on the operating conditions, the properties of the final part can change more than one order of magnitude. Properties of interest include the mechanical, optical, barrier, permeability, and biodegradability, and any other property of practical relevance including the characteristics of the surfaces as its finishing and wettability, which are connected to one another. The scope of this Special Issue is to select progress in or reviews of the understanding/description of the phenomena involved along the chain of processing–morphology–properties. Along this virtual chain, modeling may be a useful approach, and within the objective of understanding fundamental aspects, it may also be relevant to compare selected characteristics of the process and the material with the characteristics of the resulting morphology and then with the properties of the final part. This approach suggests the title: “Polymer Processing: Modeling and Correlations Finalized to Tailoring the Plastic Part Morphology and Properties”

Technology 2003: Conference Proceedings from the Fourth National Technology Transfer Conference and Exposition, Volume 1

Proceedings from symposia of the Technology 2003 Conference and Exposition, December 7-9, I993, Anaheim, CA. Volume 1 features the Plenary Session and the Plenary Workshop, plus papers presented in Advanced Manufacturing, Biotechnology/Medical Technology, Environmental Technology, Materials Science, and Power and Energy

Advanced Gas Turbine (AGT) powertrain system

A 74.5 kW(100 hp) advanced automotive gas turbine engine is described. A design iteration to improve the weight and production cost associated with the original concept is discussed. Major rig tests included 15 hours of compressor testing to 80% design speed and the results are presented. Approximately 150 hours of cold flow testing showed duct loss to be less than the design goal. Combustor test results are presented for initial checkout tests. Turbine design and rig fabrication is discussed. From a materials study of six methods to fabricate rotors, two have been selected for further effort. A discussion of all six methods is given

The use of stereolithography and related technologies to produce short run tooling

ThesisWhere material properties are critical to a polymer part, rapid prototype (RP) models are inappropriate for evaluation purposes and actual parts moulded in a range of materials are required for evaluation. Conventional tool making processes have extremely long lead times considering that numerous iterations may be required. The aim of this project was to generate polymer parts, utilising various approaches to Rapid Tooling (RT) , including Stereolithography or related technologies, as part of the process. The objective was to establish decision-making criteria for deciding on the appropriateness of various processes and the risks involved to assist prospective users of these technologies. The first phase of the project focused on the process validation of utilising Stereolithography as a direct means to generate injection mould tooling inserts, which were fitted into an injection mould designed for the trial purposes. The objective was to obtain process information with regard to insert generation for Stereolithography. A three dimensional model of the part was generated with CAD and the associated mould was generated around the part. The insert halves were processed and solid epoxy inserts were generated with the 3D Systems SLA500 Stereolithography machine. These inserts were post-finished and fitted to the injection mould . Additional features were added to the inserts to test cooling and gating and wear resistance of the cavity material. The author attended the basic injection tool setting course of the Plastics Federation to enable him to contribute more directly to this process. This also highlighted some of the design issues to facilitate ease of production . Initial difficulties were experienced in finding optimal process parameters. A total of 70 parts were produced, with measurable insert degradation. During the author's training at 3D Systems in the USA, he obtained additional insight in current methods of insert modelling and insert generation. If these process problems could be overcome, it would be possible to produce in excess of a 100 parts with one set of inserts, assuming a tolerance specification of 0.2mm. The cost of producing the inserts was approximately 50% that of conventional tooling fabrication . The time lapse between growing of the inserts and production of parts was one week compared to 6 to 8 weeks tool manufacture time with conventional methods. The second phase of the project focused on methods to enhance the cavity surface. Electroplating of inserts and inserts generated from Aluminium filled epoxy were tested , to investigate the effects that plating has on tool life, dimensional accuracy, temperature distribution, and the cost implications for these subsequent process steps. Stereolithography inserts were generated, taking into account the design considerations. Aluminium filled epoxy inserts were subsequently cast from silicone moulds drawn off the Stereolithography master patterns. Two sets of Stereolithography inserts were plated with 20 ~m of electrolytic nickel plating. One set of aluminium filled epoxy inserts were plated with electrolytic copper followed by electroless nickel. The mould sets were subjected to the same injection moulding trials using Polypropylene. The third phase of the project evaluated the use of Stereolithography investment casting masters to produce tool steel inserts, through the QuickCast process. Porosity was evident, with substantial machining required to fit the inserts. Not all the detail was retained during the casting process. Thin rib features on the part were thus lost. Due to the porosity the cooling was changed to copper tubes fitted into the rear of the tool and back-filled with aluminium epoxy. As the Stereolithography patterns were not polished the metal inserts had to be hand finished. This was a time consuming process and skill is required to obtain a good finish. A cost comparison indicated that machining aluminium inserts would be more cost effective. The tool manufacture time and eventual cost is not significantly less than conventional machining . In fact, trials with aluminium High speed CNC machining proved to be more time, finish and cost effective. This is discussed as part of the trial examples. Wax injection into AIM tooling was investigated on behalf of a client, with good results . As ceramic and polymer injection are very similar, apart from the ceramic being far more abrasive, it is the author's opinion that AIM tooling would be applicable, taking into account that fewer parts may be achieved. The KelTool process was also investigated during the author's USA visit. The licensing fees and additional equipment are extremely costly due to the Rand IDollar exchange rate. Issues related to this process are documented in this report. Clearly the deciding factors remain the quantity of parts required and the complexity of form. Each manufacturing process has a certain level of risk involved. Accumulative risk not only sets manufactured parts at risk but could jeopardise project time scales and iterations of a process have significant impact on a project budget