223 research outputs found
Issue of Money Laundering Risks Identification in the Activity of the Organizations and Individual Entrepreneurs Engaged in the Mining, Production, Use and Circulation of Precious Metals and Precious Stones
This article is distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use and redistribution provided that the original author and source are credited.Identification of money laundering risks in the sector of precious metals and precious stones is an important element in building an effective risk-based approach of money laundering risk assessment in the country. The article describes a mechanism of information exchange used in risk assessment of the organizations and individual entrepreneurs engaged in the mining, production, use and circulation of precious metals and precious stones. The mechanism is based on modern digital technologies such as a user’s cabinet on the Federal financial monitoring service website. The risk-score is obtained as a result of the analysis of the information contained in the database of Rosfinmonitoring, as well as monitoring and oversight activities conducted by Federal state institution «The risk-score shall be provided to all subjects of the sector allowing them to quickly resolve the shortcomings in their activities. Keywords: money laundering risk, sector of precious metals and precious stones, big data, information exchange, risk assessment, internal control
Perspective Non-Fluorinated and Partially Fluorinated Polymers for Low-Temperature PEM FC
The main requirement to the materials used to make membranes polymer electrolyte membrane fuel cells (PEM FC) is the combination of high proton conductivity and resistance to the FC operation conditions. Thus, the search for inexpensive and high-performance non-fluorinated or partially fluorinated materials for use as FC membranes is an actual task today, since the use of membranes based on perfluorosulfonate acid has a number of disadvantages limiting their application. The aim of this study is the investigation of sulfonated polyimide (SPI) and materials for use as FC membranes. The relevance of research stems from the fact that the use of the SPI will allow to increase the resistance of the membrane to the constantly changing environment in which PEM operates. The objects of research are sulfonated polyimides. SPIs, especially aromatic SPIs, are attractive to researchers, because of the possibility of obtaining a wide variety of chemical structures and also due to their excellent thermal, mechanical properties and high resistance to aggressive media. The results of this study will be methods of obtaining and evaluating the advantages and disadvantages of SPI-based materials. For the first time, special attention will be paid to advanced development based on SPI with the addition of crown-ether fragments
EFFICIENCY ANALYSIS OF ENERGY ACCUMULATING MECHANISM FOR TRACTOR WITH ELECTROMECHANICAL TRANSMISSION
Dependence of tractor wheel torque on theoretical tractor motion speed has been used for comparison of tractor operation with electromechanical transmission with installation of energy accumulating mechanism and without its installation. In this case a traction asynchronous electric motor is operating under nominal and limit conditions. The paper also considers dependence diagrams of actual input power for the traction asynchronous electric motor and its losses due to theoretical tractor motion speed. Tractor wheel torque is limited during the operation of the traction asynchronous electric motor with energy accumulating mechanisms by the following factors: maximum electric motor torque at the given frequency of supply voltage; maximum value of internal combustion motor output which can be transferred to the traction asynchronous electric motor; grip of the wheels. During the operation of the traction asynchronous electric motor with energy accumulating mechanisms there is a possibility for short power consumption without regard to the second limitation because it is possible to use power not only of internal combustion motor but also the power which is stored in the energy accumulating mechanisms. Comparison of characteristics has been made when a tractor is operating at high gear and when it is operating at all gears (that is two gears). Operation of the 5th class tractors has been analyzed for all possible cases (operation with energy accumulating mechanisms and without the mechanisms while being operated at all gears) and various types of work: tilling, sowing, cultivation, bulldozing work, transport mode. In this case equipment has been used which is aggregated with the 5th class tractor
In situ accurate determination of the zero time delay between two independent ultrashort laser pulses by observing the oscillation of an atomic excited wave packet
We propose a novel method that uses the oscillation of an atomic excited wave
packet observed through a pump-probe technique to accurately determine the zero
time delay between a pair of ultrashort laser pulses. This physically-based
approach provides an easy fix for the intractable problem of synchronizing two
different femtosecond laser pulses in a practical experimental environment,
especially where an in situ time zero measurement with high accuracy is
required.Comment: 12 pages, 3 figures, accepted to Optics Letter
Nanocomposite Polyimide Materials
The transition to nanosized fillers allows to significantly improve the characteristics of composites while reducing their degree of filling, and in some cases to achieve new properties unattainable with the use of traditional fillers and modifiers. Polymeric nanocomposites have unique barrier properties, electrical conductivity, thermal conductivity, increased strength, heat resistance, and thermal stability, as well as reduced flammability. It is known that the addition of nanodispersed layered silicates and various forms of carbon nanofillers to polymeric matrices can significantly affect the mechanisms of thermal and thermooxidative destruction and burning of nanocomposites. In this chapter, we compare the properties of composite materials based on nanostructured silicon carbide and carbon nanotubes with modified and unmodified surfaces obtained on three types of polyimide matrices (matrix No. 1 based on pyromellitic dianhydride and 4,4′-oxydianiline, matrix No. 2 based on 3,3‘,4,4’-benzophenone tetracarboxylic acid dianhydride and p-phenylenediamine, and matrix No. 3 based on pyromellitic dianhydride and 4-[4-(4-aminophenoxy) phenoxy] phenylamine). The dynamic viscosity of polyamide acid, the physicomechanical characteristics of film polymer composite materials, the determination of thermal stability, and thermooxidative destruction mechanism of composites were determined
Влияние высокотемпературного отжига на характеристики облученных быстрыми электронами p-n-структур на ядерно-легированном кремнии
The investigation results of the annealing influence (Тann = 300–800 ºС) on the minority charge currier lifetime tP in the n-base of p-n-structures, manufactured on the base of neutron transmutation doped silicon (NTD) КОФ300, irradiated at room temperature by different fluences (F = 1 · 1014 – 3 · 1016 cm–2) of electrons with the energy of Еe = 4 MeV are presented. It is established that at low electron fluences (F = 1 · 1014 cm–2), the annealing of minority charge currier lifetime tP in the n-base of p-n-structures occurs in two stages: the first – 320–400 ºС and the second – 550–650 ºС. At higher electron fluences (F = 5 · 1015–2 · 1016 cm–2), three annealing stages occur: the first – 400–450 ºС, the second – 520–650 ºС and the third – 710–770 ºС. At this, the structure barrier capacitance C dependences on Тann at high electron fluences show the geometry capacitance up to the annealing temperatures Тann = 400 ºС. In the annealing temperature range of Тann = 420–570 ºС, the increase in С with maximum is seen at Тann = 480 ºС and a subsequent decrease in the geometry capacitance is seen in the annealing temperature range of Тann = 600–670 ºС, and then again the increase in С occurs in the annealing temperature range of Тann = 720–770 ºС reaching the С values corresponding to those of the non-irradiated samples in the annealing temperature range of Тann = 770–800 ºС. The analysis of the DLTS-spectra of the investigated structures has allowed establishing the formation in the annealing process of the deep acceptor level ЕС – 0.68 eV at Тann > 400 ºС, the deep donor level ЕС – 0.32 eV in the annealing temperature range of Тann = 420–570 ºС and the deep acceptor level ЕС – 0.53 eV at Тann > 700 ºС, which satisfactorily explains the dependences of t P and С on Тann obtained in this paper.Приводятся результаты исследования влияния отжига (Тотж = 300–800 ºС) на время жизни неосновных носителей заряда tP в n-базе p-n-структур на базе высокоомного ядерно-легированного кремния (ЯЛК) КОФ300, облученных электронами с Еe = 4 МэВ при комнатной температуре флюенсами Ф = 1 · 1014–3 · 1016 см–2. Установлено, что при малых флюенсах электронов (Ф = 1 · 1014 см–2) отжиг времени жизни неосновных носителей заряда tP в n-базе структур проходит в две стадии: первая – 320–400 ºС, вторая – 550–650 ºС. При более высоких флюенсах облучения (Ф = 5 · 1015–2 · 1016 см–2) наблюдается три стадии отжига: первая – 400–450 ºС, вторая – 520– 650 ºС и третья – 710–770 ºС. При этом на зависимости барьерной емкости С структур от Тотж для высоких флюенсов облучения до Тотж = 400 ºС измеряется геометрическая емкость. В диапазоне Тотж = 420–570 ºС наблюдается рост С с максимумом при Тотж = 480 ºС и последующий спад до значений геометрической емкости в области Тотж = 600– 670 ºС, а затем рост в области Тотж = 720–770 ºС до значений, соответствующих необлученному образцу с выходом на плато при Тотж = 770–800 ºС. Анализ DLTS-спектров исследуемых структур позволил установить образование в процессе отжига глубокого акцепторного уровня ЕС – 0,68 эВ при Тотж > 400 ºС, глубокого донорного уровня ЕС – 0,32 эВ при отжиге в диапазоне Тотж = 420–570 ºС и глубокого акцепторного уровня ЕС – 0,53 эВ при Тотж > 700 ºС, что удовлетворительно объясняет полученные в данной работе зависимости tP и С от Тотж
ВНУТРІШНЬОПЕЧІНКОВИЙ ХОЛЕСТАЗ ВАГІТНИХ ПІСЛЯ ЗАСТОСУВАННЯ ДОПОМІЖНИХ РЕПРОДУКТИВНИХ ТЕХНОЛОГІЙ: КЛІНІЧНІ ОСОБЛИВОСТІ
80 pregnant women were examined after assisted reproductive technology (ART) programs: 40 women with manifestations of intrahepatic cholestasis of pregnant women (IHP) - the main group and 40 women without manifestations of IHP (comparison group).In the majority (62.5%) of patients after ART, the diagnosis of IHP established after 30 weeks of pregnancy. Some patients (27.5%) reported short-term episodes of IHP up to 24 weeks of gestation. In 17.5% of women, IHP had a severe course. Almost a third (27.5%) of women are over 35 years old. Women with IHP have a significantly higher frequency of allergies in the anamnesis (35.0%), liver pathology (20.0%) and diseases of the gastrointestinal tract (25.0%). In one third of women, IHP developed repeatedly, 42.5% of the main patients indicated a family history burdened with IHP. Almost a third of women (27.5% vs. 12.5%, p<0.05) had a history of polycystic ovary syndrome.The current pregnancy characterized by a high frequency of complications. A quarter of patients (25.0%) had early preeclampsia. In the second half of pregnancy, the threat of preterm birth noted in most women during the manifestation of IHP (60.0%). The incidence of fetal distress in women with IHP was almost 2 times higher than in patients without this complication (47.5% vs. 25.0%, respectively, p <0.05). The frequency of preeclampsia is also higher (40.0%).The vast majority of women in the main group were born by cesarean section (70.0%). Almost half of patients with IHP were premature (45.0%). A third of women (35.0%) had fetal distress in childbirth. In 27.5%, childbirth complicated by bleeding of more than 5% of body weight. The postpartum period was characterized by a 4-fold increase in the frequency of late bleeding (20.0% vs. 5.0%, p <0.05).One case of antenatal mortality noted in pregnant women after ART with IHP. Almost half of the children were born with asphyxia of varying severity (48.7%), with 10.3% diagnosed with severe asphyxia. One third of children were born with a body weight below 2500 g (30.8%). In 74.4% of newborns from mothers of the main group, various disorders of the period of early neonatal adaptation were noted, among which the most prominent were: RDS (35.9%), jaundice (43.6%) and gastrointestinal syndrome (30.8%). The 2-fold increased incidence of hemorrhagic syndrome (17.9%) is noteworthy.80 pregnant women were examined after assisted reproductive technology (ART) programs: 40 women with manifestations of intrahepatic cholestasis of pregnant women (IHP) - the main group and 40 women without manifestations of IHP (comparison group).In the majority (62.5%) of patients after ART, the diagnosis of IHP established after 30 weeks of pregnancy. Some patients (27.5%) reported short-term episodes of IHP up to 24 weeks of gestation. In 17.5% of women, IHP had a severe course. Almost a third (27.5%) of women are over 35 years old. Women with IHP have a significantly higher frequency of allergies in the anamnesis (35.0%), liver pathology (20.0%) and diseases of the gastrointestinal tract (25.0%). In one third of women, IHP developed repeatedly, 42.5% of the main patients indicated a family history burdened with IHP. Almost a third of women (27.5% vs. 12.5%, p<0.05) had a history of polycystic ovary syndrome.The current pregnancy characterized by a high frequency of complications. A quarter of patients (25.0%) had early preeclampsia. In the second half of pregnancy, the threat of preterm birth noted in most women during the manifestation of IHP (60.0%). The incidence of fetal distress in women with IHP was almost 2 times higher than in patients without this complication (47.5% vs. 25.0%, respectively, p <0.05). The frequency of preeclampsia is also higher (40.0%).The vast majority of women in the main group were born by cesarean section (70.0%). Almost half of patients with IHP were premature (45.0%). A third of women (35.0%) had fetal distress in childbirth. In 27.5%, childbirth complicated by bleeding of more than 5% of body weight. The postpartum period was characterized by a 4-fold increase in the frequency of late bleeding (20.0% vs. 5.0%, p <0.05).One case of antenatal mortality noted in pregnant women after ART with IHP. Almost half of the children were born with asphyxia of varying severity (48.7%), with 10.3% diagnosed with severe asphyxia. One third of children were born with a body weight below 2500 g (30.8%). In 74.4% of newborns from mothers of the main group, various disorders of the period of early neonatal adaptation were noted, among which the most prominent were: RDS (35.9%), jaundice (43.6%) and gastrointestinal syndrome (30.8%). The 2-fold increased incidence of hemorrhagic syndrome (17.9%) is noteworthy
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