441 research outputs found
Пористая структура продуктов электрохимического синтеза на переменном токе нанодисперсных оксидов олова
Методами электронной микроскопии и низкотемпературной адсорбции азота изучена пористая структура продуктов электролиза металлического олова на переменном токе промышленной частоты. Установлено, что продукты синтеза характеризуются высокими значениями удельной площади поверхности и мезапористой структурой. Показано, что средний размер частиц варьирует в интервале 10…30 нм
Phenomenological theory of the 3 Kelvin phase in Sr2RuO4
We model the 3K-phase of Sr2RuO4 with Ru-metal inclusion as interface state
with locally enhanced transition temperatures. The resulting 3K-phase must have
a different pairing symmetry than the bulk phase of Sr2RuO4, because the
symmetry at the interface is lower than in the bulk. It is invariant under time
reversal and a second transition, in general, above the onset of bulk
superconductivity is expected where time reversal symmetry is broken. The
nucleation of the 3K-phase exhibits a ``capillary effect'' which can lead to
frustration phenomena for the superconducting states on different
Ru-inclusions. Furthermore, the phase structure of the pair wave function gives
rise to zero-energy quasiparticle states which would be visible in
quasiparticle tunneling spectra. Additional characteristic properties are
associated with the upper critical field Hc2. The 3K-phase has a weaker
anisotropy of Hc2 between the inplane and z-axis orientation than the bulk
superconducting phase. This is connected with the more isotropic nature
Ru-metal which yields a stronger orbital depairing effect for the inplane
magnetic field than in the strongly layered Sr$_2RuO4. An anomalous temperature
dependence for the z-axis critical field is found due to the coupling of the
magnetic field to the order parameter texture at the interface. Various other
experiments are discussed and new measurements are suggested.Comment: 10 pages, 5 figure
A zone melting device for the in situ observation of directional solidification using high-energy synchrotron x rays editors-pick
Directional solidification (DS) is an established manufacturing process to produce high-performance components from metallic materials with optimized properties. Materials for demanding high-temperature applications, for instance in the energy generation and aircraft engine technology, can only be successfully produced using methods such as directional solidification. It has been applied on an industrial scale for a considerable amount of time, but advancing this method beyond the current applications is still challenging and almost exclusively limited to post-process characterization of the developed microstructures. For a knowledge-based advancement and a contribution to material innovation, in situ studies of the DS process are crucial using realistic sample sizes to ensure scalability of the results to industrial sizes. Therefore, a specially designed Flexible Directional Solidification (FlexiDS) device was developed for use at the P07 High Energy Materials Science beamline at PETRA III (Deutsches Elektronen–Synchrotron, Hamburg, Germany). In general, the process conditions of the crucible-free, inductively heated FlexiDS device can be varied from 6 mm/h to 12 000 mm/h (vertical withdrawal rate) and from 0 rpm to 35 rpm (axial sample rotation). Moreover, different atmospheres such as Ar, N2, and vacuum can be used during operation. The device is designed for maximum operation temperatures of 2200 °C. This unique device allows in situ examination of the directional solidification process and subsequent solid-state reactions by x-ray diffraction in the transmission mode. Within this project, different structural intermetallic alloys with liquidus temperatures up to 2000 °C were studied in terms of liquid–solid regions, transformations, and decompositions, with varying process conditions
Spontaneous Hall effect in chiral p-wave superconductor
In a chiral superconductor with broken time-reversal symmetry a ``spontaneous
Hall effect'' may be observed. We analyze this phenomenon by taking into
account the surface properties of a chiral superconductor. We identify two main
contributions to the spontaneous Hall effect. One contribution originates from
the Bernoulli (or Lorentz) force from spontaneous currents running along the
surfaces of the superconductor. The other contribution has a topological origin
and is related to the intrinsic angular momentum of Cooper pairs. The latter
can be described in terms of a Chern-Simons-like term in the low-energy field
theory of the superconductor and has some similarities with the quantum Hall
effect. The spontaneous Hall effect in a chiral superconductor is, however,
non-universal. Our analysis is based on three approaches to the problem: a
self-consistent solution of the Bogoliubov-de Gennes equation, a generalized
Ginzburg-Landau theory, and a hydrodynamic formulation. All three methods
consistently lead to the same conclusion that the spontaneous Hall resistance
of a two-dimensional superconducting Hall bar is of order h/(e k_F\lambda)^2,
where k_F is the Fermi wave vector and \lambda is the London penetration depth;
the Hall resistance is substantially suppressed from a quantum unit of
resistance. Experimental issues in measuring this effect are briefly discussed.Comment: 22 pages including 12 figure
Cell surface antigens in renal tumour cells: detection by immunoluminescence and enzymatic analysis
Two renal cell carcinoma cell lines (49RC 43STR and 75RC 2STR) were characterized by detection of the cell surface proteins: CD44(var), intercellular adhesion molecule-1 (ICAM-1), urokinase-type plasminogen activator (uPA) and its receptor and aminopeptidase N (APN). To detect their localization the immunoluminescent technique was used. In addition, the enzyme activity of uPA and APN was investigated in cell suspensions as well as in monolayers. The latter procedure was more advantageous since the additional use of HPLC permits a single registration of the fluorescent hydrolysis-product AMC (7-amino-4-methylcoumarin) without interference by cellular autofluorescence or non-reacted fluorescent substrate. Unlike 75RC 2STR, the cell line 49RC 43STR expressed high levels of uPA and APN. Contrary to that the cell line 75RC 2STR expressed high levels of ICAM-1 and CD44(v6), whereas 49RC 43STR showed a low level of ICAM-1 and no distinct light signal with anti-CD44(v6). The uPA activity was measured directly as well as indirectly (via plasmin) with the substrate Z-Gly-Gly-Arg-AMC. Both activator and plasmin activity were inhibited by D-Val-Phe-Lys-CMK and phenylmethylsulfonyl fluoride. The anti-catalytic antibody to uPA and that to uPA receptor were found to be inhibiting the uPA activity in a concentration-dependent manner. APN activity was assayed using alanine-p-nitroanilide. Peptidase activity was effectively inhibited by 1,10-phenanthroline and partly inhibited by ethylenediamine-tetraacetic acid. © 2001 Cancer Research Campaignhttp://www.bjcancer.co
Phonon structure in I-V characteristic of MgB point-contacts
The search of the phonon structure at the above-gap energies was carried out
for spectra of MgB point contacts with a normal metal.
The two-band model is assumed not only for the gap structure in
-characteristics, but also for phonons in
point-contact spectra, with up to the maximum lattice vibration energy. Since
the current is carried mostly by charges of 3D-band, whereas the strong
electron-phonon interaction occurs in 2D-band, we observe the phonon
peculiarities due to ''proximity'' effect in {\it k}-space, which depends on
the variation of interband coupling through the elastic scattering.Comment: 6 pages, 4 figures, revtex4, reported in International Conference
"Modern Problems in Superconductivity", 9-13 September, Yalta, Ukrain
Comparison of serious inhaler technique errors made by device-naïve patients using three different dry powder inhalers: a randomised, crossover, open-label study
Background: Serious inhaler technique errors can impair drug delivery to the lungs. This randomised, crossover, open-label study evaluated the proportion of patients making predefined serious errors with Pulmojet compared with Diskus and Turbohaler dry powder inhalers. Methods: Patients ≥18 years old with asthma and/or COPD who were current users of an inhaler but naïve to the study devices were assigned to inhaler technique assessment on Pulmojet and either Diskus or Turbohaler in a randomised order. Patients inhaled through empty devices after reading the patient information leaflet. If serious errors potentially affecting dose delivery were recorded, they repeated the inhalations after watching a training video. Inhaler technique was assessed by a trained nurse observer and an electronic inhalation profile recorder. Results: Baseline patient characteristics were similar between randomisation arms for the Pulmojet-Diskus (n = 277) and Pulmojet-Turbohaler (n = 144) comparisons. Non-inferiority in the proportions of patients recording no nurse-observed serious errors was demonstrated for both Pulmojet versus Diskus, and Pulmojet versus Turbohaler; therefore, superiority was tested. Patients were significantly less likely to make ≥1 nurse-observed serious errors using Pulmojet compared with Diskus (odds ratio, 0.31; 95 % CI, 0.19–0.51) or Pulmojet compared with Turbohaler (0.23; 0.12–0.44) after reading the patient information leaflet with additional video instruction, if required. Conclusions These results suggest Pulmojet is easier to learn to use correctly than the Turbohaler or Diskus for current inhaler users switching to a new dry powder inhaler
A polarized neutron-scattering study of the Cooper-pair moment in Sr2RuO4
We report a study of the magnetization density in the mixed state of the
unconventional superconductor S2RuO4. On entering the superconducting state we
find no change in the magnitude or distribution of the induced moment for a
magnetic field of 1 Tesla applied within the RuO2 planes. Our results are
consistent with a spin-triplet Cooper pairing with spins lying in the basal
plane. This is in contrast with similar experiments performed on conventional
and high-Tc superconductors.Comment: Submitted to Physical Review Letter
Inelastic neutron scattering study of magnetic excitations in SrRuO
Magnetic excitations in \srruo ~ have been studied by inelastic neutron
scattering. The magnetic fluctuations are dominated by incommensurate peaks
related to the Fermi surface nesting of the quasi-one-dimensional - and
-bands. The shape of the incommensurate signal agrees well with RPA
calculations. At the incommensurate {\bf Q}-positions the energy spectrum
considerably softens upon cooling pointing to a close magnetic instability :
\srruo ~does not exhibit quantum criticality but is very close to it. -scaling may be fitted to the data for temperatures above 30 K. Below the
superconducting transition, the magnetic response at the nesting signal is not
found to change in the energy range down to 0.4meV.Comment: 11 pages 9 figure
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