Characterization of Ceramic Particle Reinforced Titanium Composite Produced Via Powder Metallurgy

Nowadays, titanium is one of the most popular materials for aeronautical applications due to its good corrosion resistance, formability and strength. In this paper, rutile reinforced titanium matrix composites were produced via powder metallurgy. The steps included high energy ball milling of raw titanium and rutile powders in a planetary ball mill, which was followed by cold-pressing and sintering without external pressure. For the characterization of the milled powders and the sintered composites, scanning electron microscope, X-ray diffraction and compressive strength examinations were carried out. The results showed that the rutile has a strengthening effect on the titanium matrix. 1 wt% rutile increased the compressive strength compared to the raw titanium. Increasing the milling time of the metal matrix decreased the compressive strength values

A szinterelő közegek hatása a porkohászati úton előállított Ti-TiB2 kompozitok mechanikai tulajdonságára

Ebben a kutatásban 0, 1, 3, 5 tömeg% TiB2-ot tartalmazó Ti alapú kompozit mintákat állítottunk elő, három lépéses (porkeverék létrehozása, hidegzömítés, nyomás nélküli szinterelés) porkohászati módszerrel. A szintereléshez argont, illetve vákuumot alkalmaztunk és ezen szinterelési paraméter relatív sűrűségre, folyáshatárra és alakváltozó képességre kifejtett hatását vizsgáltuk. A 0 és 1 tömeg% TiB2 tartalom esetében az argonban szinterelt kompozit minták minden esetben nagyobb relatív sűrűség, folyáshatár és alakváltozó képességgel rendelkeztek, amíg a 3 és 5 tömeg% TiB2 tartalom esetében a kompozit minták közel azonos értékeket mutattak

Additive Manufacturing of 17-4PH Alloy: Tailoring the Printing Orientation for Enhanced Aerospace Application Performance

Additive manufacturing (AM) is one of the fastest-growing markets of our time. During its journey in the past 30 years, its key to success has been that it can easily produce extremely complex shapes and is not limited by tooling problems when a change in geometry is desired. This flexibility leads to possible solutions for creating lightweight structural elements while keeping the mechanical properties at a stable reserve factor value. In the aerospace industry, several kinds of structural elements for fuselage and wing parts are made from different kinds of steel alloys, such as 17-4PH stainless steel, which are usually milled from a block material made using conventional processing (CP) methods. However, these approaches are limited when a relatively small element must withstand greater forces that can occur during flight. AM can bridge this problem with a new perspective, mainly using thin walls and complex shapes while maintaining the ideal sizes. The downside of the elements made using AM is that the quality of the final product is highly dependent on the build/printing orientation, an issue extensively studied and addressed by researchers in the field. During flight, some components may experience forces that predominantly act in a single direction. With this in mind, we created samples with the desired orientation to maximize material properties in a specific direction. The goal of this study was to demonstrate that an additively manufactured part, produced using laser powder bed fusion (LPBF), with a desired build orientation has exceptional properties compared to parts produced via conventional methods. To assess the impact of the build orientation on the LPBF parts’ properties, one-dimensional tensile and dynamic fracture toughness tests were deployed

Deformability Tests of Pure Niobium

research team at the University of Miskolc's Faculty of Materials Science and Technology has signed a cooperation agreement with the Geneva-based European Organization for Nuclear Research (CERN) for testing of the materials employed in the Crab Cavities will be installed in the next generation of the LHC (the so-called High Luminosity Large Hadron Collider – HL-LHC). At the University of Miskolc, high purity niobium rolling experiments were carried out in conventional (unidirectional) and cross-rolled manners in order to increase the deep drawability of the final sheet. The deformability of niobium was measured by Watts- Ford and compression tests. The microstructure and anisotropy (texture) results of the initial material and the straight-rolled products are reported

The pathogenic c.1171A>G (p.Arg391Gly) and c.2359G>A (p.Val787Ile) ABCC6 variants display incomplete penetrance causing pseudoxanthoma elasticum in a subset of individuals

ABCC6 promotes ATP efflux from hepatocytes to bloodstream. ATP is metabolized to pyrophosphate, an inhibitor of ectopic calcification. Pathogenic variants of ABCC6 cause pseudoxanthoma elasticum, a highly variable recessive ectopic calcification disorder. Incomplete penetrance may initiate disease heterogeneity, hence symptoms may not, or differently manifest in carriers. Here, we investigated whether incomplete penetrance is a source of heterogeneity in pseudoxanthoma elasticum. By integrating clinical and genetic data of 589 patients, we created the largest European cohort. Based on allele frequency alterations, we identified two incomplete penetrant pathogenic variants, c.2359G>A (p.Val787Ile) and c.1171A>G (p.Arg391Gly), with 6.5% and 2% penetrance, respectively. However, when penetrant, the c.1171A>G (p.Arg391Gly) manifested a clinically unaltered severity. After applying in silico and in vitro characterization, we suggest that incomplete penetrant variants are only deleterious if a yet unknown interacting partner of ABCC6 is mutated simultaneously. The low penetrance of these variants should be contemplated in genetic counseling

A Novel Process to Produce Ti Parts from Powder Metallurgy with Advanced Properties for Aeronautical Applications

Titanium and its alloys have excellent corrosion resistance, heat, and fatigue tolerance, and their strength-to-weight ratio is one of the highest among metals. This combination of properties makes them ideal for aerospace applications; however, high manufacturing costs hinder their widespread use compared to other metals such as aluminum alloys and steels. Powder metallurgy (PM) is a greener and more cost and energy-efficient method for the production of near-net-shape parts compared to traditional ingot metallurgy, especially for titanium parts. In addition, it allows us to synthesize special microstructures, which result in outstanding mechanical properties without the need for alloying elements. The most commonly used Ti alloy is the Ti6Al4V grade 5. This workhorse alloy ensures outstanding mechanical properties, demonstrating a strength which is at least twice that of commercially pure titanium (CP-Ti) grade 2 and comparable to the strength of hardened stainless steels. In the present research, different mixtures of both milled and unmilled Cp-Ti grade 2 powder were utilized using the PM method, aiming to synthesize samples with high mechanical properties comparable to those of high-strength alloys such as Ti6Al4V. The results showed that the fine nanoparticles significantly enhanced the strength of the material, while in several cases the material exceeded the values of the Ti6Al4V alloy. The produced sample exhibited a maximum compressive yield strength (1492 MPa), contained 10 wt.% of fine (milled) particles (average particle size: 3 μm) and was sintered at 900 °C for one hour

Effect of a balance-training programme on postural balance, aerobic capacity and frequency of falls in women with osteoporosis: A randomized controlled trial

Objective: To investigate the effect of a 12-month complex balance-training programme on static and dynamic postural balance, aerobic capacity and frequency of falls in women with established osteoporosis. Design: Randomized controlled trial in which the intervention group was assigned a 12-month exercise programme (3 times a week for 30 min) and the control group had no intervention. Subjects: A total of 100 osteoporotic women with at least one previous fracture. Methods: Performance-based Timed Up and Go (TUG), Berg Balance Scale (BBS) and stabilometric platform tests were used to evaluate balance. Aerobic capacity was measured by bicycle ergometry. Frequency of falls was assessed using a falls diary. Results: After 1 year, there was a statistically significant difference between the improvement achieved in the intervention and control groups on the performance-based TUG, BBS and stabilometric platform tests (p < 0.05). Mean metabolic equivalent (MET) value decreased in the intervention group, from 4.91 to 3.82 (a significant difference from the change achieved in the control group; p = 0.05). Relative risk of falls was 0.534 at 1 year (p = 0.17). Conclusion: The 12-month balance-training programme significantly improved postural balance and increased aerobic capacity in women with established osteoporosis

Phase Transformation and Morphology Evolution of Ti50Cu25Ni20Sn5 during Mechanical Milling

Nanocrystalline/amorphous powder was produced by ball milling of Ti50Cu25Ni20Sn5 (at.%) master alloy. Both laser diffraction particle size analyzer and scanning electron microscope (SEM) were used to monitor the changes in the particle size as well as in the shape of particles as a function of milling time. During ball milling, the average particle size decreased with milling time from &gt;320 &micro;m to ~38 &micro;m after 180 min of milling. The deformation-induced hardening and phase transformation caused the hardness value to increase from 506 to 779 HV. X-ray diffraction (XRD) analysis was used to observe the changes in the phases/amorphous content as a function of milling time. The amount of amorphous fraction increased continuously until 120 min milling (36 wt % amorphous content). The interval of crystallite size was between 1 and 10 nm after 180 min of milling with 25 wt % amorphous fractions. Cubic Cu(Ni,Cu)Ti2 structure was transformed into the orthorhombic structure owing to the shear/stress, dislocations, and Cu substitution during the milling process