9 research outputs found

    Strategies for developing NADH detector based on meldola blue in different immobilization methods: A comparative study

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    A comparative study was accomplished between two immobilization methodologies for the meldola's blue (MB), used to decrease the oxidation potential of NADH. The study was performed with glassy carbon electrode by electropolymerization of pyrrole and MB through the technique of cyclic voltammetry being evaluated the effect of the number of cycles to define the thickness and the stability of the film. With 25 cycles it was obtained the best result. They were also investigated the modification of the graphite electrode with film formed by the system sol-gel PPO 300 or PPO 4000 for the dip-coating, through two methods: occlusion and adsorption. The best method was it of adsorption of MB during 10 min, following by deposit of the film PPO 300, favored for the time of drying (24 hours). The adsorption of MB followed by PPO 300 deposition presented broader linear range than PPy methodology. ©2006 Sociedade Brasileira de Química

    The Influence of the Heat Treatment Temperatures in Calcium Phosphate Synthesis

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    The aim of this work was to explore the use of economically viable sol-gel precursors to synthesize calcium phosphate, hydroxyapatite phase. The influence of heat treatment temperature was evaluated. The powders were calcined at different temperatures ranging from 300 to 600 degrees C. Chemical phase compositions were evaluated by X-ray diffraction (XRD), thermal analysis (TG-DTA/DSC) and diffuse reflectance Fourier transform infrared spectroscopy (DRIFTS). The hydroxyapatite phase was obtained above 500 degrees C. The morphology and particle size were analyzed by scanning electron microscopy (SEM). This work showed that hydroxyapatite (HA) can be obtained using a simple, fast and low-cost apparatus method at low temperature synthesis. It could be concluded that this method can be also applied to bioactive calcium phosphates coatings of implant surfaces.Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq

    Proceedings of the 2017 WAO Symposium on Hot Topics in Allergy: Pediatric & Regulatory Aspects

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    Proceedings of the 2017 WAO Symposium on Hot Topics in Allergy : Pediatric & Regulatory Aspects

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    Transverse polarisation measurement of Λ\Lambda hyperons in ppNe collisions at sNN\sqrt{s_{NN}}=68.4 GeV with the LHCb detector

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    A measurement of the transverse polarization of the Λ\Lambda and Λˉ\bar{\Lambda}hyperons in ppNe fixed-target collisions at sNN\sqrt{s_{NN}}=68.4 GeV is presented using data collected by the LHCb detector. The polarization is studied using the decay Λpπ\Lambda \rightarrow p \pi^- together with its charge conjugated process, the integrated values measured are PΛ=0.029±0.019(stat)±0.012(syst), P_{\Lambda} = 0.029 \pm 0.019 \, (\rm{stat}) \pm 0.012 \, (\rm{syst}) \, , PΛˉ=0.003±0.023(stat)±0.014(syst) P_{\bar{\Lambda}} = 0.003 \pm 0.023 \, (\rm{stat}) \pm 0.014 \,(\rm{syst}) \, Furthermore, the results are shown as a function of the Feynman xx variable, transverse momentum, pseudorapidity and rapidity of the hyperons, and are compared with previous measurements.A measurement of the transverse polarization of the Λ\Lambda and Λˉ\bar{\Lambda} hyperons in ppNe fixed-target collisions at sNN\sqrt{s_{NN}} = 68.4 GeV is presented using data collected by the LHCb detector. The polarization is studied using the decay Λpπ\Lambda \rightarrow p \pi^- together with its charge conjugated process, the integrated values measured are PΛ=0.029±0.019(stat)±0.012(syst), P_{\Lambda} = 0.029 \pm 0.019 \, (\rm{stat}) \pm 0.012 \, (\rm{syst}) \, , PΛˉ=0.003±0.023(stat)±0.014(syst). P_{\bar{\Lambda}} = 0.003 \pm 0.023 \, (\rm{stat}) \pm 0.014 \,(\rm{syst}) \,. Furthermore, the results are shown as a function of the Feynman~xx~variable, transverse momentum, pseudorapidity and rapidity of the hyperons, and are compared with previous measurements

    Measurement of the Branching Fraction of B0J/ψπ0B^{0} \rightarrow J/\psi \pi^{0} Decays

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    International audienceThe ratio of branching fractions between B0J/ψπ0B^{0} \rightarrow J/\psi \pi^{0} and B+J/ψK+B^{+} \rightarrow J/\psi K^{*+} decays is measured with proton-proton collision data collected by the LHCb experiment, corresponding to an integrated luminosity of 9 fb1^{-1}. The measured value is BB0J/ψπ0BB+J/ψK+=(1.153±0.053±0.048)×102\frac{\mathcal{B}_{B^{0} \rightarrow J/\psi \pi^{0}}}{\mathcal{B}_{B^{+} \rightarrow J/\psi K^{*+}}} = (1.153 \pm 0.053 \pm 0.048 ) \times 10^{-2}, where the first uncertainty is statistical and the second is systematic. The branching fraction for B0J/ψπ0B^{0} \rightarrow J/\psi \pi^{0} decays is determined using the branching fraction of the normalisation channel, resulting in BB0J/ψπ0=(1.670±0.077±0.069±0.095)×105\mathcal{B}_{B^{0} \rightarrow J/\psi \pi^{0}} = (1.670 \pm 0.077 \pm 0.069 \pm 0.095) \times 10^{-5}, where the last uncertainty corresponds to that of the external input. This result is consistent with the current world average value and competitive with the most precise single measurement to date
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