Critical limit of copper in soil and plant for predicting response of oat (Avena sativa) in soils of Haryana

In order to evaluate critical level in oat (Avena sativa L.), laboratory and a screen house experiment was conducted at CCS HAU, Hisar. Bulk surface soil samples (0-15 cm) were collected from eighteen (18) different locations, in the state representing major soil groups of Haryana. The results of the study revealed that the relationship between Bray's per cent yield against DTPA-Cu in soil and Cu concentration in plants indicated critical deficiency level of Cu in soil as 0.30 mg/kgand for oat plant it was 11.7 mg/kg which was statistically also at par

Stability indicating method development and validation for simultaneous estimation of atorvastatin calcium and celecoxib in bulk and niosomal formulation by RP-HPLC

The present work describes development and validation of a specific, sensitive, precise and stability-indicating high-performance liquid chromatographic method of analysis of atorvastatin calcium and celecoxib, both as a bulk drug and in niosomal formulation. The analysis has been performed by using Cosmosil-C18 column (4.6 mm´250 mm, 5 m) at 25 °C using acetonitrile: ammonium acetate buffer pH 5.0: methanol (50:25:25 v/v/v) as mobile phase. The detection was carried out at 277nm with a flow rate of 1.0mL/min. The retention times of Atorvastatin calcium and Celecoxib were 6.195 and 3.989min, respectively. The method was validated according to ICH guidelines, for specificity, precision, linearity, accuracy and robustness. Atorvastatin calcium and Celecoxib were subjected to stress conditions of hydrolysis, oxidation, photolysis and thermal degradation. The degradation was observed in oxidation and acid hydrolysis. The linearity for atorvastatin calcium and celecoxib were in the range of 100-500 µg/mL. The recovery study of atorvastatin and celecoxib were found to be in the range of 98.96 - 99.92% and 98.90-100%, respectively. The proposed method was validated and successfully applied to the estimation of Atorvastatin calcium and Celecoxib in combined in-house niosomal formulation.O presente trabalho descreve o desenvolvimento e a validação de método de análise por cromatografia de alta eficiência específico, sensível, preciso e indicador de estabilidade de atorvastatina cálcica e celecoxibe, ambos como fármaco e como formulação niosômica. A análise foi realizada utilizando coluna Cosmosil-C18 (4,6 mm´250 mm, 5 m) a 25 °C, e acetonitrila: tampão acetato de amônio pH 5,0: metanol (50:25:25 v/v/v) como fase móvel. A detecção foi realizada a 277 nm, com fluxo de 1,0 mL/min. Os tempos de retenção de atorvastatina cálcica e de celecoxibe foram 6,195 e 3,989 min, respectivamente. O método foi validado de acordo com as regras da ICH para especificidade, precisão, exatidão e robustez. A atorvastatina cálcica e o celecoxibe foram submetidos a condições de estresse por hidrólise, oxidação, fotólise e degradação térmica. A degradação foi observada por oxidação e hidrólise ácida. Observou-se a linearidade da atorvastatina cálcica e do celecoxibe na faixa de 100-500 µg/mL. A recuperação da atorvastatina e do celecoxibe foi observada na faixa de 98,96-99,92% e 98,90-100%, respectivamente. O método proposto foi validado e aplicado com sucesso para a determinação de atorvastatina cálcica e celecoxibe em formulação niosômica caseira combinada

Residual effects of natural Zn chelates on navy bean response, Zn leaching and soil status

greenhouse experiment was conducted on weakly acidic and calcareous soils to evaluate the aging and residual effects of three natural organic Zn chelates [Zn-ethylenediaminedisuccinate (Zn-EDDS), Zn-polyhydroxyphenylcarboxylate and Zn-aminelignosulfonate] each administered in a single application to a first navy bean (Phaseolus vulgaris L.) crop at several different Zn application rates. In a second navy bean crop, we determined the following parameters: the extent of Zn leaching, the amount of available Zn remaining in soils, the amount of easily leachable Zn, the size of Zn fractions in soils, the pH and redox potential, the dry matter yield, and the soluble and total Zn concentrations in plants. The residual effect after 2 years of Zn fertilization mainly depended on the aging effect of Zn chelates and losses due to Zn leaching. The data relating to the evolution from the first to the second crop showed that the aging effect was noticeable in the calcareous soil. In the latter soil, the Zn-S,S-EDDS treatments showed greater decreases in the Zn uptake by plants than the other Zn treatments and the greatest Zn uptake by plants occurred when Zn was applied as Zn-aminelignosulfonate (10 mg Zn kg−1 rate, 6.85 mg Zn per lysimeter; 5 mg Zn kg−1 rate, 3.36 mg Zn per lysimeter). In contrast, in the calcareous soil, the maximum amount of Zn uptake, for the three chelates was 0.82 mg Zn per lysimeter. Consequently, a further application of Zn would be needed to prevent Zn deficiencies in the plants of a subsequent crop. The behaviour of the pH and Eh parameters in the soils and leachates did not depend on the natural Zn sources applied. In this study, the easily leachable Zn estimated by BaCl2 extraction was not adequate to predict Zn leaching from the soils in subsequent crops

Measurement of Angular Coefficients of Bˉ→D∗ℓνˉℓ\bar{B} \to D^* \ell \bar{\nu}_\ell: Implications for ∣Vcb∣|V_{cb}| and Tests of Lepton Flavor Universality

We measure the complete set of angular coefficients $J_i$ for exclusive $\bar{B} \to D^* \ell \bar{\nu}_\ell$ decays ($\ell = e, \mu$). Our analysis uses the full $711\,\mathrm{fb}^{-1}$ Belle data set with hadronic tag-side reconstruction. The results allow us to extract the form factors describing the $B \to D^*$ transition and the Cabibbo-Kobayashi-Maskawa matrix element $|V_{\rm cb}|$. Using recent lattice QCD calculations for the hadronic form factors, we find $|V_{\rm cb}| = (41.0 \pm 0.7) \times 10^3$ using the BGL parameterization, compatible with determinations from inclusive semileptonic decays. We search for lepton flavor universality violation as a function of the hadronic recoil parameter $w$, and investigate the differences of the electron and muon angular distributions. We find no deviation from Standard Model expectations

First measurement of the Q^2 distribution of X(3915) single-tag two-photon production

We report the first measurement of the $Q^2$ distribution of $X(3915)$ produced by single-tag two-photon interactions. The decay mode used is $X(3915) \rightarrow J/\psi\omega$. The covered $Q^2$ region is from 1.5 (GeV/$c$)$^2$ to 10.0 (GeV/$c$)$^2$. The observed number of events is $7.9\pm 3.1({\rm stat.})\pm 1.5({\rm syst.})$, in comparison to the expectation of $4.1\pm 0.7$ derived from the standard value at $Q^2=0$ measured in the no-tag two-photon process and extrapolated to the higher $Q^2$ region using a $c\bar{c}$ model. The measured $Q^2$ distribution does not show a significant shift to lower $Q^2$ in contrast to the expectation from some types of non-$c\bar{c}$ models. It agrees with $X(3915)$ being a charmonium state, though it does not exclude a non-$c\bar{c}$ state with compact size or large compact components.Comment: 10 pages, 9 figures, 3 table

First measurement of the Michel parameter ξ′\xi^\prime in the τ−→μ−νˉμντ\tau^-\to\mu^-\bar{\nu}_\mu\nu_\tau decay at Belle

We report the first measurement of the Michel parameter $\xi^\prime$ in the $\tau^-\to\mu^-\bar{\nu}_\mu\nu_\tau$ decay with a new method proposed just recently. The measurement is based on the reconstruction of the $\tau^-\to\mu^-\bar{\nu}_\mu\nu_\tau$ events with subsequent muon decay-in-flight in the Belle central drift chamber. The analyzed data sample of $988\,\text{fb}^{-1}$ collected by the Belle detector corresponds to approximately $912\times10^6$ $\tau^+ \tau^-$ pairs. We measure $\xi^\prime=0.22\pm0.94(\text{stat})\pm0.42(\text{syst})$, which is in agreement with the Standard Model prediction of $\xi^\prime=1$. Statistical uncertainty dominates in this study, being a limiting factor, while systematic uncertainty is well under control. Our analysis proved the practicability of this promising method and its prospects for further precise measurement in future experiments.Comment: 6 pages, 4 figures, submitted to Phys. Rev. Let

Search for a Light Higgs Boson in Single-Photon Decays of ϒ(1S) Using ϒ(2S)→π+^{+}π−^{-}ϒ(1S) Tagging Method

We search for a light Higgs boson (A$^{0}$) decaying into a τ$^{+}$τ$^{-}$ or μ$^{+}$μ$^{-}$ pair in the radiative decays of Υ(1S). The production of Υ(1S) mesons is tagged by Υ(2S)→π$^{+}$π$^{-}$Υ(1S) transitions, using 158×10$^{6}$ Υ(2S) events accumulated with the Belle detector at the KEKB asymmetric energy electron positron collider. No significant A$^{0}$ signals in the mass range from the τ$^{+}$τ$^{-}$ or μ$^{+}$μ$^{-}$ threshold to 9.2 GeV/c$^{2}$ are observed. We set the upper limits at 90% credibility level (C.L.) on the product branching fractions for Υ(1S)→γA$^{0}$ and A$^{0}$→τ$^{+}$τ$^{-}$ varying from 3.8×10$^{-6}$ to 1.5×10$^{-4}$. Our results represent an approximately twofold improvement on the current world best upper limits for the Υ(1S)→γA$^{0}$(→τ$^{+}$τ$^{-}$) production. For A$^{0}$→μ$^{+}$μ$^{-}$, the upper limits on the product branching fractions for Υ(1S)→γA$^{0}$ and A$^{0}$→μ$^{+}$μ$^{-}$ are at the same level as the world average limits, and vary from 3.1×10$^{-7}$ to 1.6×10$^{-5}$. The upper limits at 90% credibility level on the Yukawa coupling fΥ(1S) and mixing angle sin θ$_{A0}$ are also given

Search for the decay Bs0→π0π0B^0_s \rightarrow \pi^0 \pi^0 at Belle

We report the results of the first search for the decay $B_s^0\rightarrow\pi^0\pi^0$ using $121.4\ \rm fb^{-1}$ of data collected at the $\Upsilon(5\rm S)$ resonance with the Belle detector at the KEKB asymmetric-energy $e^+e^-$ collider. We observe no signal and set a 90\% confidence level upper limit of $7.7\times 10^{-6}$ on the $B_s^0\rightarrow\pi^0\pi^0$ decay branching fraction

Search for the radiative penguin decays B0^{0} → K0^{0}S_{S}K0^{0}Sγ_{Sγ} in the Belle experiment

We report the first search for the penguin-dominated process $B^0 \rightarrow K_S^0 K_S^0 \gamma$ using the full data sample of $772\times 10^6$ $B\bar{B}$ pairs collected with the Belle detector at the KEKB asymmetric-energy $e^+ e^-$ collider. We do not observe any statistically significant signal yield in the $K_S^0$-pair invariant mass range 1 GeV/$c^2 < M_{K_S^0 K_S^0} <$ 3 GeV/$c^2$, and set the following upper limits at 90% confidence level: $\mathcal{B}(B^0 \to K_S^0 K_S^0 \gamma) < 5.8\times10^{-7}$, $\mathcal{B}(B^0 \to f_2 \gamma)\times \mathcal{B}(f_2 (1270) \to K_S^0 K_S^0 ) < 3.1\times10^{-7}$, and $\mathcal{B}(B^0 \to f_2^{\prime} \gamma)\times \mathcal{B}(f_2^{\prime} (1525) \to K_S^0 K_S^0 ) < 2.1\times10^{-7}$. Further, 90% confidence upper limits have also been set in the range of [0.7-2.9]$\times10^{-7}$ on the $B^0 \rightarrow K_S^0 K_S^0 \gamma$ branching fraction in bins of $M_{K_S^0 K_S^0}$.Comment: To be submitted to Physical Review