Effect of Heat Treatments under High Isostatic Pressure on the Transport Critical Current Density at 4.2 K and 20 K in Doped and Undoped MgB2 Wires

Annealing undoped MgB2 wires under high isostatic pressure (HIP) increases transport critical current density (Jtc) by 10% at 4.2 K in range magnetic fields from 4 T to 12 T and significantly increases Jtc by 25% in range magnetic fields from 2 T to 4 T and does not increase Jtc above 4 T at 20 K. Further research shows that a large amount of 10% SiC admixture and thermal treatment under a high isostatic pressure of 1 GPa significantly increases the Jtc by 40% at 4.2 K in magnetic fields above 6 T and reduces Jtc by one order at 20 K in MgB2 wires. Additionally, our research showed that heat treatment under high isostatic pressure is more evident in wires with smaller diameters, as it greatly increases the density of MgB2 material and the number of connections between grains compared to MgB2 wires with larger diameters, but only during the Mg solid-state reaction. In addition, our study indicates that smaller wire diameters and high isostatic pressure do not lead to a higher density of MgB2 material and more connections between grains during the liquid-state Mg reaction

Recent progress in MgB2 superconducting joint technology

Magnesium diboride (MgB2) magnets have the potential to be the next-generation liquid-helium-free magnet for magnetic resonance imaging (MRI) application due to their relatively high superconducting transition temperature, high current density and low raw material cost compared with current commercial niobium-titanium (Nb-Ti) magnets. A typical superconducting magnet includes several coils. To produce an ultra-stable magnetic field for imaging in MRI, a superconducting electromagnet operating in a persistent mode is crucial. Superconducting coils of the electromagnet in MRI are short-circuited to operate in the persistent mode by connecting coils with superconducting joints. Persistent joints have been demonstrated for in-situ and ex-situ wires of both mono- and multi-filamentary structures, made predominantly by PIT techniques similar to those used in wire production. To realise further engagement of MgB2 in MRI applications, enhancing the performance of MgB2 superconducting joints is essential. This literature review summarises research and development on MgB2 superconducting joining technology

Superconducting joints of reacted monofilament MgB2 wires sintered by hot uniaxial pressing system

Successful superconducting joints of reacted magnesium diboride (MgB2) monofilament wires are reported in this paper. The absence of a reliable method to develop superconducting joints between reacted MgB2 wires presents a major obstacle to the wider adoption of MgB2 as a material for magnet winding. A hot uniaxial pressing (HUP) system was exploited for sintering purposes since it can facilitate the formation of condensed in situ bulk on the wire filament. The wires were manufactured with an extra thick barrier material to protect the filament from damage during HUP sintering. The sintering temperature and pressure of the HUP system were varied to comprehend the best-performing joint. The performance of joints could be improved by depreciating the pores within the intermediate bulk of the joint. To prove this point, joints were cut to study their morphology. However, due to sintering in pressurised conditions, the reaction of the in situ intermediate bulk was not completed. The x-ray diffraction result detected a significant unreacted magnesium phase in the intermediate bulk. This work obtained joints of reacted MgB2 wires which can be considered for industrial MgB2 magnetic resonance imaging magnets fabrication.</p