Effects of gravity reduction on phase equilibria. Part 2: Binary two-phase solids

Phase diagrams for two-phase solids and eutectic, monotectic, peritectic, and syntectic reactions in low gravity applications to processes and products are considered

SPAR VI Technical Report for Experiment 76-22: Directional Solidification of Magnetic Composites

Samples of eutectic Bi/MnBi were directionally solidified during a low-g interval aboard the SPAR 6 flight and in a l-g environment under identical furnace velocity and thermal conditions. The Bi/MnBi eutectic is characterized by a regular rod eutectic whose morphology may be sensitive to thermo-solutal convection and by its components, MnBi, which is ferromagnetic. Morphological analyses on samples show statistically smaller interrod spacings and rod diameters with respect to samples grown under identical solidification furnace conditions in l-g. An adjustment between the interrod spacing, growth velocity, and total undercooling at the solidification interface is proposed. Morphological analyses on samples grown in l-g indicate little difference between results for different growth orientations with respect to the gravity vector. The magnetic properties are significantly affected, however, by the presence of a nonequilibrium magnetic phase and the nonequilibrium phase transforms to the equilibrium ferromagnetic phase during isothermal heat treatment

Developmental testing of a programmable multizone furnace

A multizone furnace was evaluated for its potential utilization for process experimentation on board the Space Shuttle. A temperature gradient can be created through the use of a series of connected temperature zones and can be translated by the coordinated sequencing of zone temperatures. The Bridgman-Stockbarger thermal configuration for directional solidification was implemented so that neither the sample nor furnace was translated. The thermal behavior of the furnace was measured and characterized. Limitations due to both thermal and electronic (computer) factors are identified. The results indicate that the multizone design is limited to low temperature gradients because of the indirect furnace-to-sample thermal coupling needed to blend the discrete thermal zones. The multizone furnace design inherently consumes more power than a similar (two temperature) conventional Bridgman type directional solidification furnace because every zone must be capable of the high cooling rates needed to produce the maximum desired temperature drop. Typical achievable static temperature gradients for the furnace tested were between 6 and 75 C/in. The maximum gradient velocity was approximately 10 in./hr. Several aspects of the tested system could be improved, but the dependence of the multizone design on high heat loss will limit Space Shuttle applications in the form tested unless additional power is available. The multizone furnace offers great flexibility but requires a high level of operator understanding for full advantage to be obtained

Research study on materials processing in space experiment number M512: Nickel - 12 wt percent tin alloy evaluation

Nickel-tin (12 wt percent tin) samples were processed in the sphere forming experiment on Skylab 2. The results were characterized for sphericity, density, microhardness, porosity, surface morphology, segregation, chemical composition, Curie point, and crystallography. These results are discussed along with conclusions and recommendations

Research on metal solidification in zero-g state

The containerless solidification of several pure metals and metallic alloys was studied in a low gravity environment. The tests were performed in the MSFC 4.2 s drop tower using a rapid wire melting apparatus designed and built for this purpose. Pure iron and nickel, and alloys of iron-nickel, iron-carbon, nickel-aluminum and tungsten-rhenium were all melted and solidified at a gravity level of approximately 100.000/-4 g. Interpretation of the results has led to an appreciation of the factors controlling the successful execution of this drop test experiment and to a delineation of the limits of applicability of the apparatus. Preliminary metallurgical evaluations are presented of the overall shapes, lattice parameters, surface microstructure,, cross-sectional microstructures, solidification and transformation sequences, evaporative segregation, and localized solute redistribution observed in the low-gravity specimens. The effects of low gravity on metallic solidification are discussed with particular emphasis on observations of spontaneous undercooling and evaporative segregation in uncontained melts

COTTON CULTIVAR, PLANTING, IRRIGATING, AND HARVESTING DECISIONS UNDER RISK

Producers in southwest Oklahoma lack adequate information about optimal planting decisions for cotton. This study uses a cotton growth simulation model to evaluate alternative cultivar, planting date, irrigation, and harvest choices. Effects of using information about soil moisture at reproduction and revenue loss at harvest in making cultivar and planting data decisions are evaluated. Using soil temperature information to plant at an early date produced high net revenue some years, but reduced mean net revenue and increased risk. Producers maximizing expected net revenue should plant a short-season cultivar in late May and use soil moisture information to schedule irrigation at reproduction.Crop Production/Industries,

The growth of metastable peritectic compounds

The influence of gravitationally driven thermosolutal convection on the directional solidification of peritectic alloys is considered as well as the relationships between the solidification processing conditions, and the microstructure, chemistry, and magnetic properties of such alloys. Analysis of directionally solidified Pb-Bi peritectic samples indicates that appreciable macrosegregation occurs due to thermosolutal convection and/or Soret diffusion. A peritectic solidification model which accounts for partial mixing in the liquid ahead of the planar solidification interface and describes macrosegregation has been developed. Two-phase dendritic and banded microstructures were grown in the Pb-Bi peritectic system, refined two-phase microstructures have were observed, and candidate formation mechanisms proposed. Material handling, containment, casting, microstructural and magnetic characterization techniques were developed for the Sm-Co system. Alloys produced with these procedures are homogeneous

Research of metal solidification in zero-g state

An experiment test apparatus that allows metal melting and resolidification in the three seconds available during free fall in a drop tower was built and tested in the tower. Droplets (approximately 0.05 cm) of pure nickel and 1090 steel were prepared in this fashion. The apparatus, including instrumentation, is described. As part of the instrumentation, a method for measuring temperature-time histories of the free floating metal droplets was developed. Finally, a metallurgical analysis of the specimens prepared in the apparatus is presented

CRIMINAL LAW-PROCEDURE-RIGHT OF DEFENDANT TO INSPECT GRAND JURY MINUTES

Defendant was indicted for murder by a grand jury. The trial court denied a motion by defendant requesting that the district attorney be ordered to furnish him with a transcript of the evidence offered before the grand jury. On appeal, held, affirmed. It was within the discretion of the trial court to grant or refuse the motion. Commonwealth v. Galvin, (Mass. 1948) 80 N.E. (2d) 825

AGENCY-LIABILITY OF EMPLOYER FOR EMPLOYEE\u27S INTENTIONAL TORTS

Plaintiff, a spectator occupying a front seat at a hockey game, was struck and injured by one of the players who was attempting to strike an opponent. Beyond the fact that a hockey game was in progress, there was nothing to indicate the player\u27s motive. Plaintiff recovered judgment against appellant, the corporation that employed the player who had struck her. The lower court instructed the jury that the player who had struck the plaintiff was as a matter of law acting as a servant, agent, or employee and within the scope of his employment at the time the plaintiff was injured. On appeal, held, reversed. The question of whether or not the blow was struck within the scope of the player\u27s employment should have been submitted to the jury. M. J. Uline Co. v. Cashdan, (App. D.C. 1948) 171 F. (2d) 132