Correlations among microfibril angle, density, modulus of elasticity, modulus of rupture and shrinkage in 6-year-old Eucalyptus urophylla × E. Grandis

The cellulose microfibril angle (MFA) in the cell wall is known to have major effects on wood stiffness and shrinkage. However, its influence on juvenile wood traits is not fully understood, especially in Eucalyptus. The aim of this study was to evaluate the relationships among MFA, density (ρ), dynamic modulus of elasticity (E), modulus of rupture (MOR), and shrinkage (δ) in 6-year-old Eucalyptus urophylla × E. grandis. Small clear specimens (L 410 mm x R 25 mm x T 25 mm) were cut from central boards for the determination of E and MOR. Cubic samples (25 mm³) were removed after the dynamic and static tests to evaluate ρ and δ. MFA was finally measured by X-ray diffraction on small strips coming from the cubic samples. A quasi-absence of statistical link was found for MFA - δ and MFA - ρ (R²<0.20). The parameter ρ/MFA was used to estimate E (R²=0.66) and MOR (R²=0.37). In a next step, the additive and interaction effects were investigated using multiple linear regressions with a forward selection method. The property E was found to be linked only with the additive effects of ρ and 1/MFA (R²=0.76). The additive and interaction effects were all significant for MOR (R²=0.54). This study showed that a general model including both additive and interaction effects should be used for the prediction of the modulus of elasticity and the modulus of rupture

Correlations among microfibril angle, density, modulus of elasticity, modulus of rupture and shrinkage in 6-year-old Eucalyptus urophylla × E. Grandis

The cellulose microfibril angle (MFA) in the cell wall is known to have major effects on wood stiffness and shrinkage. However, its influence on juvenile wood traits is not fully understood, especially in Eucalyptus. The aim of this study was to evaluate the relationships among MFA, density (ρ), dynamic modulus of elasticity (E), modulus of rupture (MOR), and shrinkage (δ) in 6-year-old Eucalyptus urophylla × E. grandis. Small clear specimens (L 410 mm x R 25 mm x T 25 mm) were cut from central boards for the determination of E and MOR. Cubic samples (25 mm³) were removed after the dynamic and static tests to evaluate ρ and δ. MFA was finally measured by X-ray diffraction on small strips coming from the cubic samples. A quasi-absence of statistical link was found for MFA - δ and MFA - ρ (R²<0.20). The parameter ρ/MFA was used to estimate E (R²=0.66) and MOR (R²=0.37). In a next step, the additive and interaction effects were investigated using multiple linear regressions with a forward selection method. The property E was found to be linked only with the additive effects of ρ and 1/MFA (R²=0.76). The additive and interaction effects were all significant for MOR (R²=0.54). This study showed that a general model including both additive and interaction effects should be used for the prediction of the modulus of elasticity and the modulus of rupture

Improving returns from southern pine plantations through innovative resource characterisation

The southern pine resource includes slash pine (Pinus elliottii var. elliottii) [PEE], Caribbean pine (P. caribaea var. hondurensis) [PCH] and a locally-developed hybrid [PEE × PCH] (hybrid pine). These pines as well as smaller areas of loblolly pine (P. taeda) have been the main taxa planted in the coastal areas of southern Queensland and subcoastal areas of northern New South Wales for the last 25 years. The standard structural grade ranking of the southern pine resource is limited by its stiffness as characterised by the measurement of the Modulus of Elasticity (MOE). The MOE dictates the mechanical grade of the board (or other structural products, extracted from the log). A board’s market value is directly linked to its stress grade based on individual grading performance (e.g. MGP10). For example, 1 m³ of structural board (i.e. MGP10 and above) is worth about $350 whereas non-structural board (i.e. <MGP10) is worth about$80. Based on the importance of MOE, this report focusses on it as the key attribute for the southern pine. Non-destructive tools that accurately measure board MOE will allow enhanced genetic selection, site matching, harvest planning schedules, improved allocation of the resource to different processors and facilitate improved processor settings and product performance

Correction of moisture effects on near infrared calibration for the analysis of phenol content in eucalyptus wood extracts

Les méthodes basées sur la spectroscopie proche infrarouge pour estimer les propriétés du bois sont sensibles aux variations des paramètres physiques (température, granulométrie. . . ). Le bois étant un matériau hygroscopique sensible, l'influence de l'humidité sur l'absorbance et l'étalonnage proche infrarouge a été étudiée afin de mieux considérer les possibilités d'applications dans des conditions réelles.Un étalonnage de référence de la quantité de polyphénols présents dans les extraits a été établi à partir de spectres d'une collection de bois d'hybrides d'Eucalyptus urophylla × E. grandis à humidité constante fixée. D'autres spectres ont été obtenus sur des échantillons de même provenance mais à 8 teneurs en eau couvrant une large plage de variation. L'influence de l'humidité sur l'absorbance proche infrarouge puis sur l'estimation par le modèle de référence a été analysée. / Methods based on near infrared spectroscopy used to assess wood properties are susceptible to variations in physical parameters (temperature, grain size, etc). As wood is a hygroscopically sensitive material, we studied the effects of moisure on near infrared absorbance and calibration to accurately determine the application potential of this technique under routine. A collection of Eucalyptus urophylla x E. grandis hybrid wood pieces were analysed to obtain reference calibration of polyphenol contents in wood extracts via NIR spectra acquired under constant moisture conditions.Others specimens from the same source were assessed to obtain spectra for eight moisture contents spanning a broad variation range. The effects of moisture on absorption and on estimates based on a reference model were analysed. An increase in moisture content prompteda rise in near infrared absorption over the entire spectrum and the water O-H absorption bands. The polyphenol content estimates obtained by assessing specimens against the reference calibration at variable moisture contents revealed prediction bias. Five correction methods were then tested on enhance the robustness relative to moisture. In-depth calibration and external parameter orthogonalization were found to be the most efficient methods for offsetting this factor

Density, extractives and decay resistance variabilities within branch wood from four agroforestry hardwood species

Agroforestry practices like pruning trees to control the light flux to crops produce every year a large volume of branches which is valorized by farmers as mulching or energy fuel. However, according to the literature, the wood of branches shows higher rates of polyphenols than stem wood and this can open some new perspectives for branch exploitation. In this study, the wood properties (density, mechanical properties, extractive content and decay resistance) were determined on branches of different sizes from oak, chestnut, poplar and walnut trees collected in two agroforestry systems. These properties were evaluated according to the wood age and the sampling position along the radial and longitudinal axes of the branch. All samples were analyzed by NIR-Spectroscopy and a predicting model aimed to assess the branch wood properties has been developed. Wood characteristics largely vary between species and do not exactly follow the same trends from one species to another. Overall, hardwood density of branches is similar to that of trunks, the content in wood extractives follows similar evolutions, and the decay resistance of branch wood does not seem to be really impacted by its position along the branch. Reliable NIRS models were built to easily predict the wood density and extractives content of agroforestry branches. The extractives content and the decay resistance of branch hardwood appear to be substantially lower than those of trunks, which suggests a non-suitability of branch wood for developing highvalued green chemistry

Characterisation and categorisation of the diversity in viscoelastic vibrational properties between 98 wood types

International audienceContext Increased knowledge on diversity in wood properties would have implications both for fundamental research and for promoting a diversification of uses as material. *Aims The objective is to contribute to overcoming the critical lack of data on the diversity of wood dynamic mechanical/viscoelastic vibrational properties, by testing lesser-known species and categorizing sources of variability. *Methods Air-dry axial specific dynamic modulus of elasticity (E'/γ) and damping coefficient (tanδ) were measured on a wide sampling (1792 specimens) of 98 wood types from 79 species. An experimental device and protocol was designed for conducting systematic (i.e. rapid and reproducible) characterizations. *Results Diversity at the specimens' level corroborates the "standard" relationship between tanδ and E'/γ, which is discussed in terms of orientation of wood elements and of chemical composition. Diversity at the species level is expressed on the basis of results for normal heartwood, with specific gravity (γ) ranging from 0.2 to 1.3. Axial E'/γ ranges from 9 to 32 GPa and tanδ from 4×10-3 to 19×10-3. Properties distribution follows a continuum, but with group characteristics. The lowest values of tanδ are only found in certain tropical hardwoods. Results can also suggest alternative species for musical instruments making

Comprehensive genetic dissection of wood properties in a widely-grown tropical tree: Eucalyptus

Background: Eucalyptus is an important genus in industrial plantations throughout the world and is grown for use as timber, pulp, paper and charcoal. Several breeding programmes have been launched worldwide to concomitantly improve growth performance and wood properties (WPs). In this study, an interspecific cross between Eucalyptus urophylla and E. grandis was used to identify major genomic regions (Quantitative Trait Loci, QTL) controlling the variability of WPs. Results: Linkage maps were generated for both parent species. A total of 117 QTLs were detected for a series of wood and end-use related traits, including chemical, technological, physical, mechanical and anatomical properties. The QTLs were mainly clustered into five linkage groups. In terms of distribution of QTL effects, our result agrees with the typical L-shape reported in most QTL studies, i.e. most WP QTLs had limited effects and only a few (13) had major effects (phenotypic variance explained &gt; 15%). The co-locations of QTLs for different WPs as well as QTLs and candidate genes are discussed in terms of phenotypic correlations between traits, and of the function of the candidate genes. The major wood property QTL harbours a gene encoding a Cinnamoyl CoA reductase (CCR), a structural enzyme of the monolignol-specific biosynthesis pathway. Conclusions: Given the number of traits analysed, this study provides a comprehensive understanding of the genetic architecture of wood properties in this Eucalyptus full-sib pedigree. At the dawn of Eucalyptus genome sequence, it will provide a framework to identify the nature of genes underlying these important quantitative traits. (Résumé d'auteur

Correlations among microfibril angle, density, modulus of elasticity, modulus of rupture and shrinkage in 6-year-old Eucalyptus urophylla × E. grandis

The cellulose microfibril angle (MFA) in the cell wall is known to have major effects on wood stiffness and shrinkage. However, its influence on juvenile wood traits is not fully understood, especially in Eucalyptus. The aim of this study was to evaluate the relationships among MFA, density (&#961;), dynamic modulus of elasticity (E), modulus of rupture (MOR), and shrinkage (&#948;) in 6-year-old Eucalyptus urophylla × E. grandis. Small clear specimens (L 410 mm x R 25 mm x T 25 mm) were cut from central boards for the determination of E and MOR. Cubic samples (25 mm³) were removed after the dynamic and static tests to evaluate &#961; and &#948;. MFA was finally measured by X-ray diffraction on small strips coming from the cubic samples. A quasi-absence of statistical link was found for MFA - &#948; and MFA - &#961; (R²<0.20). The parameter &#961;/MFA was used to estimate E (R²=0.66) and MOR (R²=0.37). In a next step, the additive and interaction effects were investigated using multiple linear regressions with a forward selection method. The property E was found to be linked only with the additive effects of &#961; and 1/MFA (R²=0.76). The additive and interaction effects were all significant for MOR (R²=0.54). This study showed that a general model including both additive and interaction effects should be used for the prediction of the modulus of elasticity and the modulus of rupture