2,961 research outputs found

    Op die voetspoor van Harold Henry Rowley (1890-1969)

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    On the trail of Harold Heniy Rowley (1890-1969)H H Rowley can he described as an enigmatic Old Testament scholar. Hailed as one of the leading Old Testament biblical theologians of the forties and fifties, he was also criticized for his ‘middle-of-the-road’ conclusions. This article takes a brief look at his academic career and biblical scholarship, it is argued that he is an exponent of the biblical theology movement in his attempts to reconcile the results of the historical-critical method with the traditional creeds of Christianity. Unfortunately he was not very successful because he did not regard the results of New Testament historical-critical research seriously. He was reluctant to admit that there was a difference between the historical Jesus and Christ as proclaimed by the church. Perhaps there are a few lessons to be learned from his timidity

    Improvement of the efficient referencing and sample positioning system for micro focused synchrotron X-ray techniques

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    An efficient referencing and sample positioning system is a basic tool for a micro focus beamline at a synchrotron. The seven years ago introduced command line based system was upgraded at SUL-X beamline at ANKA [1]. A new combination of current server client techniques offers direct control and facilitates unexperienced users the handling of this frequently used tool

    Safe, accurate, and precise sulfur isotope analyses of arsenides, sulfarsenides, and arsenic and mercury sulfides by conversion to barium sulfate before EA/IRMS

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    The stable isotope ratios of sulfur (δ(34)S relative to Vienna Cañon Diablo Troilite) in sulfates and sulfides determined by elemental analysis and isotope ratio mass spectrometry (EA/IRMS) have been proven to be a remarkable tool for studies of the (bio)geochemical sulfur cycles in modern and ancient environments. However, the use of EA/IRMS to measure δ(34)S in arsenides and sulfarsenides may not be straightforward. This difficulty can lead to potential health and environmental hazards in the workplace and analytical problems such as instrument contamination, memory effects, and a non-matrix-matched standardization of δ(34)S measurements with suitable reference materials. To overcome these practical and analytical challenges, we developed a procedure for sulfur isotope analysis of arsenides, which can also be safely used for EA/IRMS analysis of arsenic sulfides (i.e., realgar, orpiment, arsenopyrite, and arsenian pyrite), and mercury sulfides (cinnabar). The sulfur dioxide produced from off-line EA combustion was trapped in an aqueous barium chloride solution in a leak-free system and precipitated as barium sulfate after quantitative oxidation of hydrogen sulfite by hydrogen peroxide. The derived barium sulfate was analyzed by conventional EA/IRMS, which bracketed the δ(34)S values of the samples with three international sulfate reference materials. The protocol (BaSO(4)-EA/IRMS) was validated by analyses of reference materials and laboratory standards of sulfate and sulfides and achieved accuracy and precision comparable with those of direct EA/IRMS. The δ(34)S values determined by BaSO(4)-EA/IRMS in sulfides (arsenopyrite, arsenic, and mercury sulfides) samples from different origins were comparable to those obtained by EA/IRMS, and no sulfur isotope fractionations were introduced during sample preparation. We report the first sulfur isotope data of arsenides obtained by BaSO(4)-EA/IRMS. GRAPHICAL ABSTRACT: [Image: see text] SUPPLEMENTARY INFORMATION: The online version contains supplementary material available at 10.1007/s00216-021-03854-y

    Ultrathin epitaxial Fe films in vicinal GaAs(001): A study by spin-resolved photoelectron spectroscopy

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    Thin epitaxial Fe films have been grown on vicinal GaAs(001) substrates and their remanent magnetic properties and the degree of substrate atom diffusion investigated using synchrotron-based photoelectron spectroscopy. The vicinal Fe films, though exhibiting greater As diffusion than their singular homologues, displayed better film quality both from the structural and the magnetic points of view. The spin-resolved valence spectra of the vicinal films resemble those for crystalline bulk Fe at lower film thicknesses than for singular films

    Contrasting motivation and learning strategies of ex-mathematics and ex-mathematical literacy students

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    Abstract: This inquiry contrasts motivation and learning strategies of ex-Mathematics (Maths) and ex-Mathematical Literacy (ML) students. ML ideally delivers candidates who can make sense of and actively participate in a world of numbers and numerical arguments, but ex-ML students are excluded from many undergraduate studies at most South African higher education institutions (HEIs). Institutions employ various strategies in enhancing student transition to higher education (HE), however, such options are rare for ex-ML students. A year-long foundation programme offered by a private HEI is one exception. This inquiry employed the Motivated Strategies for Learning Questionnaire and t-test, detecting significant differences in motivation and learning strategies between 111 ex-Maths and 81 ex-ML students. The intrinsic goal orientation, task value, self-efficacy, effort regulation and test anxiety-handling abilities of ex-Maths students were significantly superior. An integrated solution process addressing academic content and social-psychological attributes to improve the motivation of ex-ML students in support of their academic development is proffered
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