136 research outputs found
Anisotropic Superparamagnetism of Monodispersive Cobalt-Platinum Nanocrystals
Based on the high-temperature organometallic route (Sun et al. Science 287,
1989 (2000)), we have synthesized powders containing CoPt_3 single crystals
with mean diameters of 3.3(2) nm and 6.0(2) nm and small log-normal widths
sigma=0.15(1). In the entire temperature range from 5 K to 400 K, the
zero-field cooled susceptibility chi(T) displays significant deviations from
ideal superparamagnetism. Approaching the Curie temperature of 450(10) K, the
deviations arise from the (mean-field) type reduction of the ferromagnetic
moments, while below the blocking temperature T_b, chi(T) is suppressed by the
presence of energy barriers, the distributions of which scale with the particle
volumes obtained from transmission electron microscopy (TEM). This indication
for volume anisotropy is supported by scaling analyses of the shape of the
magnetic absorption chi''(T,omega) which reveal distribution functions for the
barriers being also consistent with the volume distributions observed by TEM.
Above 200 K, the magnetization isotherms M(H,T) display Langevin behavior
providing 2.5(1) mu_B per CoPt_3 in agreement with reports on bulk and thin
film CoPt_3. The non-Langevin shape of the magnetization curves at lower
temperatures is for the first time interpreted as anisotropic
superparamagnetism by taking into account an anisotropy energy of the
nanoparticles E_A(T). Using the magnitude and temperature variation of E_A(T),
the mean energy barriers and 'unphysical' small switching times of the
particles obtained from the analyses of chi''(T,omega) are explained. Below T_b
hysteresis loops appear and are quantitatively described by a blocking model,
which also ignores particle interactions, but takes the size distributions from
TEM and the conventional field dependence of E_A into account.Comment: 12 pages with 10 figures and 1 table. Version accepted for
publication in Phys. Rev. B . Two-column layou
The BMC Medicine breast cancer collection: an illustration of contemporary research and clinical care
Análise da aplicabilidade do custeio-meta na etapa de concepção de empreendimentos habitacionais de interesse social
Breast cancer risk variants at 6q25 display different phenotype associations and regulate ESR1, RMND1 and CCDC170.
We analyzed 3,872 common genetic variants across the ESR1 locus (encoding estrogen receptor α) in 118,816 subjects from three international consortia. We found evidence for at least five independent causal variants, each associated with different phenotype sets, including estrogen receptor (ER(+) or ER(-)) and human ERBB2 (HER2(+) or HER2(-)) tumor subtypes, mammographic density and tumor grade. The best candidate causal variants for ER(-) tumors lie in four separate enhancer elements, and their risk alleles reduce expression of ESR1, RMND1 and CCDC170, whereas the risk alleles of the strongest candidates for the remaining independent causal variant disrupt a silencer element and putatively increase ESR1 and RMND1 expression.This is the author accepted manuscript. The final version is available from Nature Publishing Group via http://dx.doi.org/10.1038/ng.352
Adoção da modularidade em produto e em produção na indústria automotiva: uma análise comparativa em projetos de veículos com participação da engenharia brasileira
Effects of photochemical riboflavin-mediated crosslinks on the physical properties of collagen constructs and fibrils
Evaluation of methods for calculating maximum allowable standing height in amputees competing in Paralympic athletics
The International Paralympic Committee has a maximum allowable standing height (MASH) rule that limits stature to a pre-trauma estimation. The MASH rule reduces the probability that bilateral lower limb amputees use disproportionately long prostheses in competition. Although there are several methods for estimating stature, the validity of these methods has not been compared. To identify the most appropriate method for the MASH rule, this study aimed to compare the criterion validity of estimations resulting from the current method, the Contini method, and four Canda methods (Canda-1, Canda-2, Canda-3, and Canda-4). Stature, ulna length, demispan, sitting height, thigh length, upper arm length, and forearm length measurements in 31 males and 30 females were used to calculate the respective estimation for each method. Results showed that Canda-1 (based on four anthropometric variables) produced the smallest error and best fitted the data in males and females. The current method was associated with the largest error of those tests because it increasingly overestimated height in people with smaller stature. The results suggest that the set of Canda equations provide a more valid MASH estimation in people with a range of upper limb and bilateral lower limb amputations compared with the current method
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