Investigation of Nanoparticles in High Resolution Scanning Electron Microscopy (SEM) and Low Voltage SEM by Digital Image-Analysis

Small particles (Cu, Ag, In, Sn, Au, also MgO and NaCl) were prepared in the diameter range from 1 nm to 100 nm on different conductive substrates by thermal evaporation in high-vacuum or in an inert gas atmosphere. Imaging of the particles was performed in a high resolution scanning electron microscope (HRSEM) that can also be operated at low beam voltages of a few hundred volts. This mode of operation is called low voltage SEM (LVSEM). Scanning electron micrographs were taken at different beam voltages VO (0.5-30 kV). The micrographs were digitally recorded and analyzed with an image processing system operated on-line to the HRSEM. Grey-value line profiles and densitometric quantities of single particles, as well as the contrast between particle and substrate, changed with VO. The results for tin-particles on a bulk carbon substrate are shown. In all cases considered, only positive contrasts, i.e., particles looking brighter than the substrate, were obtained. The main contrast producing mechanism is, therefore, assigned to effects that include the particle\u27s geometrical properties of size, shape and surface. Sn-, In-, and Ag-particles, imaged in the secondary electron (SE) mode showed significantly larger particle diameters, as did images simultaneously recorded with transmitted electrons; however, Au-particles did not show that difference. This effect may be qualitatively explained by SE resulting from decaying plasmons

Investigation of the Dzyaloshinskii-Moriya interaction and room temperature skyrmions in W/CoFeB/MgO thin films and microwires

Recent studies have shown that material structures, which lack structural inversion symmetry and have high spin-orbit coupling can exhibit chiral magnetic textures and skyrmions which could be a key component for next generation storage devices. The Dzyaloshinskii-Moriya Interaction (DMI) that stabilizes skyrmions is an anti-symmetric exchange interaction favoring non-collinear orientation of neighboring spins. It has been shown that material systems with high DMI can lead to very efficient domain wall and skyrmion motion by spin-orbit torques. To engineer such devices, it is important to quantify the DMI for a given material system. Here we extract the DMI at the Heavy Metal (HM) /Ferromagnet (FM) interface using two complementary measurement schemes namely asymmetric domain wall motion and the magnetic stripe annihilation. By using the two different measurement schemes, we find for W(5 nm)/Co20Fe60B20(0.6 nm)/MgO(2 nm) the DMI to be 0.68 +/- 0.05 mJ/m2 and 0.73 +/- 0.5 mJ/m2, respectively. Furthermore, we show that this DMI stabilizes skyrmions at room temperature and that there is a strong dependence of the DMI on the relative composition of the CoFeB alloy. Finally we optimize the layers and the interfaces using different growth conditions and demonstrate that a higher deposition rate leads to a more uniform film with reduced pinning and skyrmions that can be manipulated by Spin-Orbit Torques

Tunneling magneto thermo power in magnetic tunnel junction nanopillars

We study the tunneling magneto thermo power (TMTP) in CoFeB/MgO/CoFeB magnetic tunnel junction nanopillars. Thermal gradients across the junctions are generated by a micropatterned electric heater line. Thermo power voltages up to a few tens of \muV between the top and bottom contact of the nanopillars are measured which scale linearly with the applied heating power and hence with the applied temperature gradient. The thermo power signal varies by up to 10 \muV upon reversal of the relative magnetic configuration of the two CoFeB layers from parallel to antiparallel. This signal change corresponds to a large spin-dependent Seebeck coefficient of the order of 100 \muV/K and a large TMTP change of the tunnel junction of up to 90%.Comment: Revised version containing additional data and analyis. 13 pages, 3 figure

Biased quasi ballistic spin torque magnetization reversal

We explore the fundamental time limit of ultra fast spin torque induced magnetization reversal of a magnetic memory cell. Spin torque precession during a spin torque current pulse and free precessional magnetization ringing after spin torque pulse excitation is detected by time resolved magneto transport. Adapting the duration of the spin torque excitation pulse to the spin torque precession period allows suppression of the magnetization ringing and thus coherent control of the final orientation of the magnetization. In the presence of a hard axis bias field such coherent control enables an optimum ultra fast, quasi ballistic spin torque magnetization reversal by a single precessional turn directly from the initial to the reversed equilibrium state.Comment: 13 pages 3 Figure

Determination of spin-dependent Seebeck coefficients of CoFeB/MgO/CoFeB magnetic tunnel junction nanopillars

We investigate the spin-dependent Seebeck coefficient and the tunneling magneto thermopower of CoFeB/MgO/CoFeB magnetic tunnel junctions (MTJ) in the presence of thermal gradients across the MTJ. Thermal gradients are generated by an electric heater on top of the nanopillars. The thermo power voltage across the MTJ is found to scale linearly with the heating power and reveals similar field dependence as the tunnel magnetoresistance. The amplitude of the thermal gradient is derived from calibration measurements in combination with finite element simulations of the heat flux. Based on this, large spin-dependent Seebeck coefficients of the order of (240 \pm 110) \muV/K are derived. From additional measurements on MTJs after dielectric breakdown, a tunneling magneto thermopower up to 90% can be derived for 1.5 nm MgO based MTJ nanopillars

Effect of annealing on the interfacial Dzyaloshinskii-Moriya interaction in Ta/CoFeB/MgO trilayers

The interfacial Dzyaloshinskii-Moriya interaction (DMI) has been shown to stabilize homochiral N´eel-type domain walls in thin films with perpendicular magnetic anisotropy and as a result permit them to be propagated by a spin Hall torque. In this study, we demonstrate that in Ta/Co20Fe60B20/MgO the DMI may be influenced by annealing. We find that the DMI peaks at D = 0.057 ± 0.003 mJ/m2 at an annealing temperature of 230 ◦C. DMI fields were measured using a purely field-driven creep regime domain expansion technique. The DMI field and the anisotropy field follow a similar trend as a function of annealing temperature. We infer that the behavior of the DMI and the anisotropy are related to interfacial crystal ordering and B expulsion out of the CoFeB layer as the annealing temperature is increased

Scattering variability detected from the circumsource medium of FRB 20190520B

Fast radio bursts (FRBs) are millisecond-timescale radio transients, the origins of which are predominantly extragalactic and likely involve highly magnetized compact objects. FRBs undergo multipath propagation, or scattering, from electron density fluctuations on sub-parsec scales in ionized gas along the line-of-sight. Scattering observations have located plasma structures within FRB host galaxies, probed Galactic and extragalactic turbulence, and constrained FRB redshifts. Scattering also inhibits FRB detection and biases the observed FRB population. We report the detection of scattering times from the repeating FRB 20190520B that vary by up to a factor of two or more on minutes to days-long timescales. In one notable case, the scattering time varied from $7.9\pm0.4$ ms to less than 3.1 ms ($95\%$ confidence) over 2.9 minutes at 1.45 GHz. The scattering times appear to be uncorrelated between bursts or with dispersion and rotation measure variations. Scattering variations are attributable to dynamic, inhomogeneous plasma in the circumsource medium, and analogous variations have been observed from the Crab pulsar. Under such circumstances, the frequency dependence of scattering can deviate from the typical power-law used to measure scattering. Similar variations may therefore be detectable from other FRBs, even those with inconspicuous scattering, providing a unique probe of small-scale processes within FRB environments.Comment: 10 pages, 9 figures, accepted to MNRA