双伺服电动机控制万向指示器的设计

万向指示器在机电一体化演示系统、检测与自动控制系统中有广泛的用途,本文采用两台伺服电动机控制万向指示器的水平转动与垂直转动,通过两种转动的合成来达到任意方向精确指向的目的。实验结果表明,本系统实时性好,反应敏捷。而且体积小、重量轻、造价低,易于实现

Influence of Particle Damper Configurations on the Dynamic Characteristic for Gear Transmission System

齿轮传动正朝着高速、重载和高精度方向发展,对其动态性能要求越来越高。颗粒阻尼通过颗粒间、颗粒与阻尼器壁间的非弹性碰撞和摩擦作用耗能,具有减振效果; 显著、耐高温、各向同性、对原结构改动小等优点。利用有限元法对齿轮进行了有预应力的模态分析,通过齿轮系统动力学分析,研究单双齿啮合激励对齿轮传动的; 影响;同时建立齿轮传动离心场中颗粒系统耗能模型,将离散元法计算颗粒系统耗能和试验测试对比,分析阻尼器配置对齿轮传动系统动特性的影响。结果显示,阻; 尼器配置方案是影响齿轮传动系统动特性的一个重要因素,在阻尼孔中填充一定数量的颗粒,当阻尼器总体积相同且齿轮结构静刚度相差不大时,阻尼器个数越多颗; 粒系统能耗越大;当阻尼孔直径相同时,阻尼孔个数越多颗粒系统总能耗越小;当阻尼孔个数相同时,阻尼孔直径越大颗粒系统能耗越小。通过试验和仿真对比验证; 了模型的正确性,为颗粒阻尼在离心场中的应用提供重要的理论依据。The gear transmission is advancing towards high speed, heavy load and; high precision. The requirements for the dynamic performance of gear; system are urgently proposed. The particle damping dissipates mechanical; system energy through inelastic collisions and friction between; particles. It is an effective and simple measure for vibration; reduction. It has many advantages, such as isotropy, high temperature; resistance and less modification to the original structure. This paper; has conducted the prestressed modal analysis of gear system by the; finite element method. Based on the dynamics analysis of gear system,; the effect of single tooth and double teeth meshing incentive on gear; transmission has been analyzed. The energy dissipation model of particle; damping for gear transmission in centrifugal field has been established.; By contrasting theoretical analysis and the test, the effect of damper; configuration on dynamic characteristic of gear transmission system is; analyzed. The results show that damper configuration is an important; factor of the dynamic characteristic for gear transmission system.; Filling a certain number of particles, when the gears static stiffness; are similar and the total dampers volume are equal, the more damping; hole, the greater the total energy loss. When the damping holes diameter; are the same, the more number of damping hole, the smaller the total; energy loss. When the damping hole number is the same, the bigger the; diameter, the less the total energy loss. Experimental results are; consistency with the theoretical analysis. These results can provide; guidelines for the application of particle damping in centrifugal field.国家自然科学基金; 福建省重点科技专项; 中央高校基本科研业务费专项资金; 福建省高端装备制造协同创新中心资助项

稠环烯烃芳香性的碳数规则

稠环烯烃芳香性的碳数规则张强黄伟杰石磊黄荣彬郑兰荪（厦门大学化学系固体表面物理化学国家重点实验室３６１００５）１Ｈｃｋｅｌ规则与其应用范围Ｈüｃｋｅｌ规则是判断环烯烃芳香性的重要规则。这个规则是：π电子数为４ｎ＋２个的环烯烃是芳香性的，而π电子数为..

Effects of salinity on the growth and proline,soluble sugar and protein contents of Spartina alterniflora

研究了互花米草在不同培养盐度下,株高、茎粗、叶长、叶宽、叶面积、鲜重等生长指标以及脯氨酸、可溶性糖和蛋白质含量的变化情况。结果表明,随着盐度增加,米草株高呈下降趋势,在高盐度(5 0‰)下,米草叶面积、叶长等指标与对照组相比明显下降,鲜重与低盐度组比较显著下降。米草叶片中可溶性糖、脯氨酸含量随盐度增加总体上呈上升趋势;可溶性蛋白质含量随盐度增加亦呈上升趋势,表明蛋白质合成增强。在盐胁迫下,渗透调节物质的积累作用是互花米草对盐胁迫的主要响应过程,可以作为其抗盐性的生理参数。 【英文摘要】 Under different salinity conditions,variations of height,stem diameter,leaf length and width,leaf area,fresh weight,proline,soluble sugar and protein contents of Spartina alterniflora seedlings were investigated.The results showed that the height tended to decrease with the increaseing salinity in the medium.In high salinity (50‰) treatment,the leaf area and length decreased significantly compared with control,and single plant fresh weight decreased more than those of low salinity treatments.The sugar ...国家自然科学基金项目 (3 0 2 710 65 ,3 9970 43 8,3 9870 63 0 );; 福建省自然科学基金资助项目 (D0 2 10 0 0 1

Design of Ultra-wideband Printed Rectangular Monopole Antenna

针对超宽带通信应用,研究影响印制单极天线阻抗带宽的主要因素,设计基于微带馈电的小型化印制矩形单极天线。按照等效性原理,采用黄金分割比设计矩形振子体;通过接地面上端引入渐变梯形或凹形结构,同时调整馈入端接地面间隙,可实现印制矩形单极天线的超宽带特性。对具有渐变梯形或凹形接地面结构的微带馈电矩形印制单极天线结构进行优化,仿真结果表明,前者的阻抗带宽为2.96~17.94gHz,后者的阻抗带宽为2.9~13.3gHz,而两者的辐射方向基本保持不变。实测结果与仿真结果基本一致,达到了超宽带通信应用的要求。To achieve ultra-wideband(UWB)radio applications,the microstrip-fed printed rectangular monopole antenna is analyzed and devised.Using golden section ratio the rectangular monopole is of layout based on equivalent principle.To maximize the impedance bandwidth,it is necessary introducing the taper or concave ground plane and feed gap of microstrip line.The simulated results of the optimized-size antennas show that the impedance bandwidth defined by return loss less than-10dB is from 2.96GHz to 17.94GHz with a ratio of about 6.06∶1 for taper ground antenna and from 2.9GHz to 13.3GHz with a ratio of about 4.59∶1 for concave ground antenna.At the same time a nearly omnidirectional radiation pattern is exhibited.These results are confirmed by the experimental test and these compact size antennas are suitable for various wideband applications.福建省科技计划重点资助项目(2007H0036

Design of Wideband Bi-directional Microstrip Antenna

针对室内走廊或狭长街道小功率基站应用要求,采用微带结构设计了一款具有双向辐射特性的宽带线极化低剖面天线。天线辐射元为平行四边形结构,馈电点在其几何中心,通过在靠近馈点两侧开两个反对称l形槽,实现了宽带双向辐射特性。低剖面原型天线的相对带宽为5.8%,两端射方向增益约为4.3dbI,在工作频带内天线辐射场为有一定倾角的线极化。该天线结构可置于小功率基站内部,有助于减少系统体积。A linearly polarized wideband microstrip patch antenna with the bi-directional radiation pattern is proposed for the low-power indoor or narrow-street base station systems.The proposed antenna,which has a parallelogram radiator,is fed by a coaxial line at its geometric center.In order to achieve the wideband bi-directional radiation characteristics,two anti-symmetric L-shaped slots were etched near the feed point.The simulation and measurement show that the low profile prototype antenna provides a relative bandwidth of about 5.8%,and the endfire direction gain of 4.3dBi.In the working band its linear polarization direction has incline angles with the vertical.This antenna can be placed inside the low-power base stations to help reduce the system size.福建省重大科技专项(2010HZ0004-1

Studies on the Interactions between Bioactive Peroxovanadium Complexes Bearing Organic Ligands and Histidine

在合成和表征了 4种具有较强生物活性双过氧钒配合物K3 [VO(O2 ) 2 (ox) ]·2H2 O ,Na[VO(O2 ) 2 (bipy) ]·5H2 O ,K[VO(O2 ) 2 (phen) ]·3H2 O和K2 [VO(O2 ) 2 (pic) ]·2H2 O [分别缩写为pV(ox) ,pV(bipy) ,pV(phen)和pV(pic) ,其中ox为草酸根 ,bipy为 2 ,2′ 联吡啶 ,phen为邻菲咯啉 ,pic为 2 羧酸吡啶负离子 ]的基础上 ,利用多种NMR技术和电喷雾质谱 (ESI MS)研究了这 4种含有机配体双过氧钒配合物与组氨酸 (His)在溶液中的相互作用以及反应物浓度、时间、pH等对相互作用体系的影响 .51VNMR跟踪监测的结果表明 :双过氧钒配合物pV(ox)和pV(pic)与His在中性水溶液中存在强配位相互作用 ,而pV(bipy)和pV(phen)与His在中性水溶液中无明显作用 .我们还利用谱学方法确定了pV(ox)和His相互作用后所生成产物是pV(ox)分别与His咪唑基上的 3 N和 1 N配位的一对异构体. 　In order to explore the structure2activity relationship and molecular mechanism of the specific recognition between peroxovanadium (pV) complexes bearing organic ligands and the target enzymes of tyrosine phosphatase , several NMR techniques and ESI2MS were used to study the interactions of four pV complexes {pV(ox) , pV ( bipy) , pV (phen) and pV (pic) , where pV = [VO (O2 ) 2L ] n - , in which L = oxalic acid dianion (ox) , bipyridine (bipy) , 1 ,102phenanthroline (phen) , and pyridine222carboxylic acid (pic) } towards histidine. Strong coordination interactions between imidazole of histidine and vanadium of pV(ox) or pV(pic) were observed in neutral solution , while there are not obvious interactions between histidine and pV(bipy) or pV(phen) . All 13C and 1H NMR signals of 1∶1 stoichiometric mixture of pV(ox) and histidine were assigned. Spectroscopic studies demonstrated that new complexes in the mixture of pV(ox) and histidine are a pair of isomers in which the vanadium in pV(ox) binding to the 32N and 12N of the imidazole ring. Moreover , the results of effective factors on the interaction system indicated that the new isomers were stable under the condition of physiological pH and the structure2activity relationship of these pV complexes may be relevant to their specific recognition towards histidine residues in tyrosine phosphatase.国家自然科学基金 (Nos.2 0 172 0 42 ,2 9832 0 2 0 )资助项

Progress of Organic Chemistry(2011～2012)

本文综述了中国大陆地区有机化学研究人员2011至2012年两年内在合成方法学、有机合成化学、元素有机化学以及天然产物化学等领域获得的重要成果。文章中共引用参考文献355篇,其中110多篇手性金属配合物和有机小分子催化的不对称反应、金属催化的碳氢键活化等合成方法学论文和30余篇氟有机化学论文基本来源于德国《应用化学》(国际版)和《美国化学杂志》。本文汇集了中国有机化学家两年中合成的150多个具有生物活性和化学结构多样性的天然产物,其中不乏具有高度挑战性的复杂天然分子。在近两年中中国有机化学家从陆地和海洋的生物体内发现各种不同类型新天然产物90多个。This biennale report reviewed the major achievements of organic chemistry involved to synthetic methodologies,synthetic chemistry,element-organic chemistry,and natural product chemistry in Mainland of China.There were 355 references cited in this report.Among them,about 110 papers related to the synthetic methodologies as well as about 30 papers of organofluorine chemistry reported herein were collected solely from ACIE and JACS.The report presented the synthesis of more than 150 natural products with diverse chemical structures and bioactivities,including some complex molecules with high synthetic challenge as well as the isolation of more than 90 new natural products with various structural types from continental or /and marine creatures,which were reported by Chinese chemists in 2011 ~ 2012

大肠杆菌重组颗粒性戊型肝炎疫苗对恒河猴的免疫保护

大肠杆菌表达的戊型肝炎病毒 (HEV)衣壳蛋白ORF2片段HEV 2 39重组蛋白颗粒 ,经铝佐剂吸附后 ,分别以5 μg、1 0 μg和 2 0 μg剂量免疫恒河猴 ,2 8天时以相同剂量加强免疫 1次 ,3周后分别以不同病毒滴度的基因Ⅰ型或基因Ⅳ型HEV静脉攻击。结果 ,加强后 3周 ,3个免疫剂量组猴的抗体几何平均滴度分别为 1∶2 71 75、1∶344 0 9、1∶4 16 0 7,以世界卫生组织参比血清定量 ,则分别为 1 0 98IU/ml,1 35 7IU/ml、1 72 4IU/ml。每个剂量免疫组及对照组各有 3只猴接受 1 0 7病毒滴度基因Ⅰ型HEV感染 ,对照组 3只猴均被成功感染 ,2只出现肝炎 ;2 0 μg免疫组 3只猴均未被感染 ;1 0 μg和 5 μg免疫组各有 2只猴未被感染 ,另 1只猴出现短暂感染 ,免疫猴均未出现肝炎。 3个剂量免疫组及对照组另外 3只猴 ,接受 1 0 4病毒滴度基因Ⅰ型HEV感染 ,对照组 3只猴均被感染 ,1只出现肝炎 ;而免疫猴均未被感染 ,也未出现肝炎。 3只 1 0 μg免疫猴和 3只对照猴分别接受 1 0 7病毒滴度基因Ⅳ型HEV感染 ,对照组均被感染并出现肝炎 ,而免疫组均未出现肝炎 ,有 2只未被感染 ,另 1只被短暂感染。另有 3只 1 0 μg免疫猴和 3只对照猴分别接受 1 0 4病毒滴度基因Ⅳ型HEV感染 ,对照组均被感染 ,而免疫组均未被感染。这些结果表明 :HE

Studies on the interactions between bioactive peroxovanadium complexes bearing organic ligands and histidine

In order to explore the structure-activity relationship and molecular mechanism of the specific recognition between peroxovanadium. (pV) complexes bearing organic ligands and the target enzymes of tyrosine phosphatase, several NMR techniques and ESI-MS were used to study the interactions of four pV complexes {pV(ox), pV(bipy), pV(phen) and pV(pic), where pV=[VO(O-2)(2)L](n-), in which L=oxalic acid dianion (ox), bipyridine (bipy), 1, 10-phenanthroline (phen), and pyridine-2-carboxylic acid (pic)} towards histidine, Strong coordination interactions between imidazole of histidine and vanadium of pV(ox) or pV(pic) were observed in neutral solution, while there are not obvious interactions between histidine and pV(bipy) or pV (phen). All C-13 and H-1 NMR signals of 1:1 stoichiometric mixture of pV (ox) and histidine were assigned. Spectroscopic studies demonstrated that new complexes in the mixture of pV (ox) and histidine are a pair of isomers in which the vanadium in pV(ox) binding to the 3-N and 1-N of the imidazole ring. Moreover, the results of effective factors on the interaction system indicated that the new isomers were stable under the condition of physiological pH and the structure-activity relationship of these pV complexes may be relevant to their specific recognition towards histidine residues in tyrosine phosphatase