251 research outputs found
在线调解与传统调解制度之比较
网络技术为传统的纠纷解决方式提供了新的发展空间,调解作为传统纠纷解决方式之一自然也不例外,即调解也可以在网络上进行。从在线调解技术手段和实践情况入手,可以对在线调解进行一定的价值分析,并对传统的调解方式能否在线进行的问题进行初步的探讨
Effect of Ti-Si Mixed Oxide Support on Gold Catalysts for Gas-Phase Epoxidation of Propylene
以TiCl4和SiCl4为原料,采用水解和非水水解溶胶-凝胶两种方法制备了一系列不同Ti含量的Ti-Si复氧化物载体,继而用沉积-沉淀法制得载金催化剂.采用X射线衍射、紫外-可见漫反射光谱、N2吸附和高分辨透射电镜对催化剂进行了表征,并考察了催化剂在氢气和氧气存在下的丙烯气相环氧化催化性能.研究表明,钛含量在6%~14%范围内时,两种方法制得的Ti-Si复氧化物均为无定形结构,但采用非水水解溶胶-凝胶法制得的载体比表面积较高.以非水水解溶胶-凝胶法制备的钛含量10%的Ti-Si复氧化物为载体得到的载金催化剂表现出较高的活性和选择性,反应60min时,丙烯转化率为5.7%,240min后降为3.3%,环氧丙烷的选择性稳定于95%左右.还考察了非水水解溶胶-凝胶的陈化时间和金沉积-沉淀溶液的pH值等对反应结果的影响.Titania-silica mixed oxides prepared by hydrolytic and one-step non-hydrolytic sol-gel routes using TiCl_4 and SiCl_4 as precursors were employed as the gold catalyst supports for gas-phase epoxidation of propylene in O_2 and H_2. Characterization studies of the supports and catalysts were performed by means of X-ray diffraction, ultraviolet-visible absorption spectroscopy, N_2 adsorption, and high-resolution transmission electron microscopy. The results indicated that the amorphous Ti-Si mixed oxides containing 6%-14% of Ti could be prepared by both sol-gel routes, but those by non-hydrolytic sol-gel afforded higher surface area and significant mesopores. A superior catalytic performance was obtained with the gold catalyst supported on the non-hydrolytic sol-gel Ti-Si mixed oxide containing 10% of Ti. The propylene conversion was 5.7% at the initial 60 min and 3.3% at 240 min of time on stream. The selectivity for propylene oxide was as high as 95%. The influences of aging time for the non-hydrolytic sol-gel and pH value for the Au deposition-precipitation on the performance of the Au catalyst were also discussed.国家自然科学基金(20021002,20473065,20433030);; 福建省科技重大专项(2005HZ01-3)资助项目
Theoretical Model to Compute Specific Area of Activated Carbon
在分析比较各种吸附理论的基础上,介绍5种可用于计算活性炭比表面积的吸附等温方程式,并实际计算6种不同类型活性炭的比表面积.结果表明:不同吸附等温式之间的差异在16%以内.Adsorption isothem equations which are suited to calculate the specific area of activated carbon are recommended based on the analysis and the comparison of various adsorptive theoriesThe specific areas of six activated carbons of different types are computerd by beans of five adsorption isothem equations separatelyThe results showed that the maximum deviation within 16% among calculation values of six carbons in terms of five different adsorptive models国家自然科学基金资助项目(30271057)
Therapeutic effects comparison between platelet-rich plasma and sodium hyaluronate intra-articular injection in treatment of knee osteoarthritis
目的关节腔内注射自体富血小板血浆(PRP)与透明质酸钠(SH),观察并比较其疗效。方法于2012年2月至12月,漳州市解放军第175医院骨科收治的81例Kellgren-Lawrence(KL)分级标准为Ⅱ、Ⅲ级膝关节骨关节炎的患者,年龄48~60岁,平均(52.6±3.6)岁;男性27例,女性53例;左膝38例,右膝43例。K-L分级标准,Ⅱ级47例,Ⅲ级34例,按就诊顺序序贯随机平行分为SH组(40例)和PRP组(41例),分别采用SH和PRP关节腔内注射进行治疗。治疗前和治疗后3、6、9、12个月对患者进行随访并进行美国西部Ontario与Mc Master大学骨关节炎指数(WOMAC)评分评估,两组间各时间点WOMAC评分比较采用t检验,两组内各时间点WOMAC评分比较采用重复测量方差分析;分别于治疗前和治疗后12个月进行膝关节磁共振检查,评价关节腔内积液的吸收情况。结果治疗前及治疗后3个月PRP组WOMAC评分[(48.42±4.95)分,(25.38±5.12)分]和SH组[(47.17±5.12)分,(25.17±5.09)分]比较,t值分别为-0.625和0.413,差异无统计学意义(P均〉0.05);治疗后6、9、12个月PRP组WOMAC评分[(21.44±4.73)分,(20.54±4.46)分,(16.53±7.35)分]和SH组[(25.87±5.16)分,(27.22±4.21)分,(29.63±8.21)分]比较,PRP组低于SH组,t值分别为-2.765、-3.447和-4.657,差异具有统计学意义(P均〈0.05),治疗后12个月复查磁共振,可见PRP组的关节积液吸收例数高于SH组,差异有统计学意义(P〈0.05)。结论膝关节腔内注射自体PRP,临床效果优于透明质酸钠,中长期疗效好。Objective To compare the efficacy of platelet rich plasma (PRP) and sodium hyaluronate (SH) intra-articular injection in the patients with knee osteoarthritis of grade Ⅱand Ⅲ. Methods A total of 81 patients with knee osteoarthritis of grade Ⅱ and Ⅲ ( Kellgren-Lawrence standard) were randomly assigned to the PRP and SH group. All 81 patients were treated in the 175th hospital of PLA, Zhangzhon, with the average age of (52.6 ± 3.6) years. There were 27 males and 53 females. Forty cases in SH group and 41 cases in PRP group had got the complete follow-up. Both the two groups adopted 4 ml of 5% lidocaine for intra-articular injection. All the patients were prospectively evaluated before the treatment and at the 34 , 6th , 9th and 12th month after the treatment by the Western Ontario and McMaster Universities (WOMAC) osteoarthritis index. The swelling subsiding knee was observed. Between the two groups WOMAC scores were compared using t test at each time point, within the groups the scores were compared by repeated measures analysis of variance. The absorption of accumulated fluid in the joint cavity was observed and compared by MRI before and 12 months after the treatment. Results No serious adverse event was detected in the two groups. According to the follow-up evaluations, both the groups presented clinical improvements. The comparison between the two groups showed no statistically significant difference before therapy and three months after the treatment ( t =- 0. 625, 0. 413, P 〉 0. 05 ). Six months, nine months and 12 months after the treatment, WOMAC score in the PRP group[ (21.44 ±4. 73), (20. 54 ± 4. 46) ,(16. 53 ± 7. 35 ) pointsl were lower than the SH group[(25.87 ±5.16), (27.22 ±4.21), (29. 63 ± 8.21 ) points] ; the difference was statistically signifieant( t = - 2. 765, - 3. 447, - 4. 657, P 〈 0. 05 ). Conclusion PRP intra-artieular injection in the treatment of knee osteoarthritis of gradeⅡ and Ⅲ may be more suitable compared to南京军区医学科技创新重点课题项目(15ZD027
暹罗鳄多肽粉提高机体免疫力及抗疲劳的效应
为研究暹罗鳄多肽粉对小鼠免疫力及抗疲劳效应的影响,对小鼠的免疫能力和相关血清指标进行了测定,同时也对小鼠的运动能力及疲劳代谢指标进行了测定.实验结果显示:暹罗鳄多肽粉可以促进小鼠胸腺和脾脏的生长,免疫力得到提高.相对于对照组小鼠,暹罗鳄多肽粉组小鼠血清中的总蛋白、血钙、白蛋白含量升高(p<0.05),谷丙转氨酶(ALT)的活力和血糖浓度下降(p<0.05).小鼠爬绳及负重游泳实验发现服用了暹罗鳄多肽粉的小鼠垂直爬绳时间和负重游泳时间均高于对照组的(p<0.01),小鼠的耐力增强.进一步通过建立抗疲劳小鼠力竭游泳模型研究了暹罗鳄多肽粉的抗疲劳动物学功效,结果显示相对于对照组,暹罗鳄多肽粉组小鼠血液中尿素氮(BUN)和乳酸(LA)的含量以及乳酸脱氢酶(LDH)的酶活力均降低(p<0.05),而超氧化物歧化酶(SOD)的酶活力升高(p<0.05).综上结果表明暹罗鳄多肽粉可能有保肝护肝,提高肌体免疫力以及抗疲劳等功效.福建省自然科学基金项目(2016J05105);;广东省自然科学基金博士启动项目(2016A030310374);;厦门大学生命科学学院-福建鼍龙鳄鱼生物制品研发协同创新中心项目(XDHT2017004C
Correlation between use of social software and high risk behaviors of HIV infection among MSM in Beijing
目的了解北京市男男性行为者(MSM)社交软件的使用与人类免疫缺陷病毒(HIV)感染及其影响因素的相关性,为今后干预工作提供依据。方法 2016年3—5月,由社区小组招募MSM进行问卷调查,同时进行HIV抗体检测。结果共招募215名MSM,回收有效问卷214份。214人的平均年龄为30.8岁;学历在大专及以上者占73.4%;同性恋者占72.4%;84.6%的人主要通过社交软件寻找性伴。214人中确证HIV感染5人,阳性率为2.3%。分析显示,是否使用社交软件、是否使用同性社交软件和是否使用普通人群社交软件均与HIV感染不相关。多因素分析结果显示,受教育程度高、性取向为同性恋的人更多地使用同性社交软件。63.1%被调查者自述曾经在社交软件上了解到艾滋病防治相关知识,但自述了解程度与是否通过社交软件获得相关信息不相关。结论 MSM社交软件的使用与HIV感染情况无关,也没有增加其对艾滋病知识的了解。但可以考虑改进同性社交软件功能,增加艾滋病防治知识内容,对MSM尤其是高学历、自我定位为同性恋的MSM进行艾滋病防治宣传。[Objective] To understand the correlation between the use of social software and human immunodeficiency virus(HIV)infection and its influencing factors among men who have sex with men(MSM)in Beijing,provide the basis for future intervention work.[Methods]From May to March in 2016,MSM was recruited by community groups to carry out a questionnaire survey and HIV antibody of them was detected.[Results]A total of 215 MSM were recruited and 214 valid questionnaires were recovered. The average age of the 214 MSM was 30.8 years old,73.4% had the education level in college and above,the homosexuals accounted for 72.4%,and84.6% of the respondents mainly found sexual partners through the social software. There were 5 cases of confirmed HIV infection among 214 MSM with the positive rate of 2.3%. The analysis revealed that whether the respondents use the social software,the homosexual social software and the general social software were not related to HIV infection. The results of multivariate analysis showed that people with higher educational level and homosexual orientation were more likely to use the homosexual social software. 63.1% of respondents reported that they had been obtained the knowledge of AIDS prevention and control from social software,but the understanding level was not related to whether the relevant information was obtained through social software or not.[Conclusion]The use of social software has no correlation with HIV infection among MSM,and does not increase their knowledge level of AIDS prevention and control. However,it is necessary to improve the function of the homosexual social software and increase the content of AIDS prevention and control knowledge to carry out the AIDS education among MSM,especially those with higher educational level and homosexual orientation
XPS Analysis of the HgCdTe Surface Etched by ICP
文章将ICP刻蚀技术应用于刻蚀HgCdTe,使用微区X射线光电子光谱学(XPS)、扫描电子显微镜(SEM)等表面分析技术研究了ICP各工艺参数,包括ICP功率、气体成分与配比、腔体压力等对刻蚀表面形貌、刻蚀后表面成分、聚合物形成的影响。XPS分析结果发现,使用光刻胶作掩模时,刻蚀气体CH4会与光刻胶发生反应,生成物可能为C6H5(CH3)。如果腔体压力较高,生成物不能及时被带走,就会附着在样品表面上,使样品表面发黑;当腔体压力较低时,生成物被及时带走,则样品表面光亮,无聚合物残留。光刻胶也会与H2发生反应,生成多种含C有机物。SiO2作掩模时,在一定的条件下,CH4会与SiO2或者真空硅脂发生反应,生成聚脂薄膜。ICP(Inductively Coupled Plasma) etching technique has been applied to HgCdTe providing significant benefits such as high uniformity, low damage and anisotropic profile,etc.We have studied the dependence of surface profile,post-etch composition,formation of polymer on the effect of ICP parameters(ICP power,gas ratio,chamber pressure) by using micro regional XPS and SEM(scanning electron microscopy).We have found that methane can react with photoresist(PR) which is used as mask,the product may be C_6H_5(CH_3).The product can't be pumped out if the chamber pressure is high,then it will be left on the sample surface forming so-called polymer.Otherwise if the chamber pressure is low,the product is pumped away the chamber in time,and there is no polymer on the surface.H_2 can react with PR,and the products are several organic compounds with carbon.Under certain condition,methane can reacts with SiO_2 or high vacuum grease,generating Mylar Polyster
Effects of a Sliding Plate on Morphology of the Epiphyseal Plate in Goat Distal Femur
The aim of this study was to observe the effects of a sliding plate on the morphology of the epiphyseal plate in goat distal femur. Eighteen premature female goats were divided randomly into sliding plate, regular plate and control groups. Radiographic analysis and histological staining were performed to evaluate the development of epiphyseal plate at 4 and 8 weeks after surgery. In the sliding plate group, the plate extended accordingly as the epiphyseal plate grows, and the epiphyseal morphology was kept essential normal. However, the phenomenon of the epiphyseal growth retardation and premature closure were very common in the regular plate group. In addition, the sliding plate group exhibited more normal histologic features and Safranin O staining compared to the regular plate group. Our results suggest that the sliding plate can provide reliable internal fixation of epiphyseal fracture without inhibiting epiphyseal growth
基于强化学习的能量采集物联网视频编码技术
物联网设备的视频压缩码率和量化参数等编码方案决定着视频质量和物联网设备的使用寿命.针对未知视频传输模型和能量采集模型的物联网设备,提出一种基于强化学习的视频编码方案,能够动态优化视频编码码率和量化参数.该技术根据物联网设备的无线信道带宽、电池水平和采集的能量,结合反馈的视频质量和时延等信息,采用强化学习算法优化选择视频编码码率和量化参数.在动态的网络环境下,物联网设备不需预知视频传输模型就可以综合优化视频质量和设备能量损耗.仿真结果表明,该方案可以提高视频质量,降低设备能量损耗和时延,改善物联网设备效益.国家自然科学基金(61671396)福建省自然科学基金(2019J01843)东南大学移动通信国家重点实验室开放基金(2018D08
Analysis of the Content of Stevia Sweeteners by Capillary Zone Electrophoresis
本文介绍了一种用毛细管区带电泳法筛选甜菊糖苷突变体的有效方法。根据实验结果 ,优化的电泳条件为 :60mmol/LTris 硼酸缓冲液 (pH 8.0 ) ,柱温 30℃ ,工作电压 2 5kV。优化条件下 ,甜菊苷 (Ste vioside)迁移时间的R .S .D为 0 .45% (1 5次 ) ,且在 7.45× 1 0 - 5~ 1 .74× 1 0 - 2 mol/L的浓度范围内存在良好的线性关系 (r=0 .9994) ,甜菊主要糖苷在 5min内均可实现分离。在优化条件下 ,本实验研究了低能离子注入后甜菊主要糖苷含量变化 ,结果令人满意。This paper introduced an effect capillary zone electrophoresis method for screening of stevia mutation. According to the experimental results, the optimum separation conditions were selected as: 60 mmol/L Tris tetraborate buffer of pH 8.0, 30 ℃ and 25 KV. Under optimum conditions, the R.S.D. of stevioside migration time for 15 runs was 0.45%. The detector response for stevioside was linear over the range of 7.45×10 -5 ~1.74×10 -2 mol/L (r=0.9994). Stevia main sweeteners cound be separated effectively in less than five minutes. This method was applied for determining the variation of stevia main sweeteners after low_energy ions implantation
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