Finite element simulation of powder compaction via shock consolidation using gas-gun system

Shock consolidation is a promising method for consolidation of nanocrystalline metallic powders since it can prevent grain growth of nanopowders during the process due to very short processing time. However, internal cracks often occurs in powder compacts during the shock consolidation process. In this paper, finite element simulations showed that reflected tensile wave causes spall phenomena resulting internal crack of powder compaction during shock compaction process. To reduce spall phenomena, FEM simulation with changing compaction die's geometry was performed to find out relationship between shape and tensile wave intensity. Based on FEM results, new compaction die was designed and bulk nanocrystalline Cu are obtained using new compaction die. (C) 2014 Published by Elsevier Ltd.open1111Ysciescopu

Experimental investigation of the elastoplastic response of aluminum silicate spray dried powder during cold compaction

Mechanical experiments have been designed and performed to investigate the elasto-plastic behaviour of green bodies formed from an aluminum silicate spray dried powder used for tiles production. Experiments have been executed on samples obtained from cold compaction into a cylindrical mould and include: uniaxial strain, equi-biaxial flexure and high-pressure triaxial compression/extension tests. Two types of powders have been used to realize the green body samples, differing in the values of water content, which have been taken equal to those usually employed in the industrial forming of traditional ceramics. Yielding of the green body during compaction has been characterized in terms of yield surface shape, failure envelope, and evolution of cohesion and void ratio with the forming pressure, confirming the validity of previously proposed constitutive models for dense materials obtained through cold compaction of granulates.Comment: 17 pages; Journal of the European Ceramic Society, 201

Formation of bi-lobed shapes by sub-catastrophic collisions: A late origin of comet 67P/C-G's structure

The origin of the particular shape of a small body like comet 67P/Churyumov-Gerasimenko (67P/C-G) is a topic of active research. How and when it acquired its peculiar characteristics has distinct implications on the origin of the solar system and its dynamics. We investigate how shapes like the one of comet 67P/C-G can result from a new type of low-energy, sub-catastrophic impacts involving elongated, rotating bodies. We focus on parameters potentially leading to bi-lobed structures. We also estimate the probability for such structures to survive subsequent impacts. We use a smooth particle hydrodynamics (SPH) shock physics code to model the impacts, the subsequent reaccumulation of material and the reconfiguration into a stable final shape. The energy increase as well as the degree of compaction of the resulting bodies are tracked in the simulations. Our modelling results suggest that the formation of bi-lobed structures like 67P/C-G is a natural outcome of the low energy, sub-catastrophic collisions considered here. Sub-catastrophic impacts have the potential to alter the shape of a small body significantly, without leading to major heating or compaction. The currently observed shapes of cometary nuclei, such as 67P/C-G, maybe a result of such a last major shape forming impact.Comment: Astronomy & Astrophysics, accepted pending minor revision

Using small-angle X-ray scattering to investigate the compaction behaviour of a granulated clay

The compaction behaviour of a commercial granulated clay (magnesium aluminium smectite, gMgSm) was investigated using macroscopic pressure-density measurements, X-ray diffraction (XRD), scanning electron microscopy (SEM), X-ray microtomography (XμT) and small-angle X-ray scattering (SAXS). This material was studied as a potential compaction excipient for pharmaceutical tabletting, but also as a model system demonstrating the capabilities of SAXS for investigating compaction in other situations. Bulk compaction measurements showed that the gMgSm was more difficult to compact than polymeric pharmaceutical excipients such as spheronised microcrystalline cellulose (sMCC), corresponding to harder granules. Moreover, in spite of using lubrication (magnesium stearate) on the tooling surfaces, rather high ejection forces were observed, which may cause problems during commercial tabletting, requiring further amelioration. Although the compacted gMgSm specimens were more porous, however, they still exhibited acceptable cohesive strengths, comparable to sMCC. Hence, there may be scope for using granular clay as one component of a tabletting formulation. Following principles established in previous work, SAXS revealed information concerning the intragranular structure of the gMgSm and its response to compaction. The results showed that little compression of the intragranular morphology occurred below a relative density of 0 · 6, suggesting that granule rearrangements or fragmentation were the dominant mechanisms during this stage. By contrast, granule deformation became considerably more important at higher relative density, which also coincided with a significant increase in the cohesive strength of compacted specimens. Spatially-resolved SAXS data was also used to investigate local variations in compaction behaviour within specimens of different shape. The results revealed the expected patterns of density variations within flat-faced cylindrical specimens. Significant variations in density, the magnitude of compressive strain and principal strain direction were also revealed in the vicinity of a debossed feature (a diametral notch) and within bi-convex specimens. The variations in compaction around the debossed notch, with a small region of high density below and low density along the flanks, appeared to be responsible for extensive cracking, which could also cause problems in commercial tabletting

Competition and cooperation:aspects of dynamics in sandpiles

In this article, we review some of our approaches to granular dynamics, now well known to consist of both fast and slow relaxational processes. In the first case, grains typically compete with each other, while in the second, they cooperate. A typical result of {\it cooperation} is the formation of stable bridges, signatures of spatiotemporal inhomogeneities; we review their geometrical characteristics and compare theoretical results with those of independent simulations. {\it Cooperative} excitations due to local density fluctuations are also responsible for relaxation at the angle of repose; the {\it competition} between these fluctuations and external driving forces, can, on the other hand, result in a (rare) collapse of the sandpile to the horizontal. Both these features are present in a theory reviewed here. An arena where the effects of cooperation versus competition are felt most keenly is granular compaction; we review here a random graph model, where three-spin interactions are used to model compaction under tapping. The compaction curve shows distinct regions where 'fast' and 'slow' dynamics apply, separated by what we have called the {\it single-particle relaxation threshold}. In the final section of this paper, we explore the effect of shape -- jagged vs. regular -- on the compaction of packings near their jamming limit. One of our major results is an entropic landscape that, while microscopically rough, manifests {\it Edwards' flatness} at a macroscopic level. Another major result is that of surface intermittency under low-intensity shaking.Comment: 36 pages, 23 figures, minor correction

The Effectiveness of Using Models of Cylinder and Cube in the Clay Soil Compaction Test

According to R.F. Craig (1974), soil is any uncemented or weakly cemented accumulation of mineral particles formed by the weathering of rocks, the void space between the particles containing water and/or air. According to SNI 03- 1743- 1989, soil compaction test with laboratory compaction method, using four methods with four molds which is different diameter. The formulation of this research problem is whether the test result of soil compaction is same if the mold that usually use cylindrical shape turned into cube shape. This research includes comparison of standard proctor and modified proctor soil compaction result either using manual rammers or a modified compactor. Two type of mold are used, which is cylindrical mold with 101,60 mm diameter, and cube mold with a size of 10 x 10 cm. it is known that the standard proctor soil compaction of the collision method, the moisture content correction is 100%. Meanwhile, the correction of dry volume weight is 99,58%. In modified proctor soil compaction of collision method, the moisture content correction is 93,2882%. Meanwhile, the correction of dry volume weight is 98,8082%. In standard proctor soil compaction of the pressure method, the moisture content correction is 99,03%. Meanwhile the correction of dry volume weight is 99,27%. In modified proctor soil compaction of the pressure method, the moisture content correction is 96,07%. Meanwhile the correction dry volume weight is 98,60%

A column of grains in the jamming limit: glassy dynamics in the compaction process

We investigate a stochastic model describing a column of grains in the jamming limit, in the presence of a low vibrational intensity. The key control parameter of the model, $\epsilon$, is a representation of granular shape, related to the reduced void space. Regularity and irregularity in grain shapes, respectively corresponding to rational and irrational values of $\epsilon$, are shown to be centrally important in determining the statics and dynamics of the compaction process.Comment: 29 pages, 14 figures, 1 table. Various minor changes and updates. To appear in EPJ