16 research outputs found

    Application of a lab-made electronic nose for extra virgin olive oils commercial classification according to the perceived fruitiness intensity

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    An electronic nose, comprising nine metal oxide sensors, has been built aiming to classify olive oils according to the fruity intensity commercial grade (ripely fruity or light, medium and intense greenly fruity), following European regulated complementary terminology. The lab-made sensor device was capable to differentiate standard aqueous solutions (acetic acid, cis-3-hexenyl, cis-3-hexen-1-ol, hexanal, 1-hexenol and nonanal) that mimicked positive sensations (e.g., fatty, floral, fruit, grass, green and green leaves attributes) and negative attributes (e.g., sour and vinegary defects), as well as to semi-quantitatively classify them according to the concentration ranges (0.05 to 2.25 mg/kg). For that, unsupervised (principal component analysis) and supervised (linear discriminant analysis: sensitivity of 92% for leave-one-out cross validation) classification multivariate models were established based on nine or six gas sensors, respectively. It was also showed that the built E-nose allowed differentiating/discriminating (sensitivity of 81% for leave-one-out cross validation) extra virgin olive oils according to the perceived intensity of fruitiness as ripely fruity, light, medium or intense greenly fruity. In conclusion, the gas sensor device could be used as a practical preliminary non-destructive tool for guaranteeing the correctness of olive oil fruitiness intensity labelling.The authors are grateful to the Foundation for Science and Technology (FCT, Portugal) for financial support by national funds FCT/ MCTES to CIMO (UIDB/00690/2020), to CEB (UIDB/04469/2020) and to BioTecNorte operation (NORTE-01-0145-FEDER-000004) and Project “GreenHealth - Digital strategies in biological assets to improve wellbeing and promote green health” (Norte-01-0145-FEDER-000042) funded by the European Regional Development Fund (ERDF) under the scope of Regional Operational Program North 2020. ´Itala Marx acknowledges the Ph.D. research grant (SFRH/BD/137283/2018) provided by FCT. Nuno Rodrigues thanks the National funding by FCTFoundation for Science and Technology, P.I., through the Institutional Scientific Employment Program-contract.info:eu-repo/semantics/publishedVersio

    Volatile-olfactory profiles of cv. Arbequina olive oils extracted without/with olive leaves addition and their discrimination using an electronic nose

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    Oils from cv. Arbequina were industrially extracted together with olive leaves of cv. Arbequina or Santulhana (1%, w/w), and their olfactory and volatile profiles were compared to those extracted without leaves addition (control). The leaves incorporation resulted in green fruity oils with fresh herbs and cabbage olfactory notes, while control oils showed a ripe fruity sensation with banana, apple, and dry hay grass notes. In all oils, total volatile contents varied from 57.5 to 65.5mg/kg (internal standard equivalents), being aldehydes followed by esters, hydrocarbons, and alcohols the most abundant classes. No differences in the number of volatiles were observed. The incorporation of cv. Arbequina or Santulhana leaves significantly reduced the total content of alcohols and esters (minus 3756% and 1013%, respectively). Contrary, cv. Arbequina leaves did not influence the total content of aldehydes or hydrocarbons, while cv. Santulhana leaves promoted a significant increase (plus 49 and 10%, respectively). Thus, a leaf-cultivar dependency was observed, tentatively attributed to enzymatic differences related to the lipoxygenase pathway. Olfactory or volatile profiles allowed the successful unsupervised differentiation of the three types of studied cv. Arbequina oils. Finally, a lab-made electronic nose was applied to allow the nondestructive discrimination of cv. Arbequina oils extracted with or without the incorporation of olive leaves (100% and 99±5% of correct classifications for leave-one-out and repeated K-fold cross-validation variants), being a practical tool for ensuring the label correctness if future commercialization is envisaged. Moreover, this finding also strengthened that olive oils extracted with or without olive leaves incorporation possessed quite different olfactory patterns, which also depended on the cultivar of the olive leaves.The authors are grateful to the Foundation for Science and Technology (FCT, Portugal) for financial support by national funds FCT/MCTES to CIMO (UIDB/00690/2020), CEB (UIDB/04469/2020), REQUIMTE-LAQV (UIDB/ 50006/2020) units, and the Associate Laboratories for Green Chemistry-LAQV (UIDB/50006/2020) and SusTEC (LA/P/0007/2020), as well as to BioTecNorte operation (NORTE01-0145-FEDER-000004) funded by the European Regional Development Fund under the scope of Norte2020—Programa Operacional Regional do Norte. ´Itala M.G. Marx also acknowledges the PhD research grant (SFRH/BD/137283/2018) provided by FCT. Nuno Rodrigues likes to thank national funding by FCT—Foundation for Science and Technology, P.I., through the institutional scientific employment program contract.info:eu-repo/semantics/publishedVersio

    Assessment of E-Senses Performance through Machine Learning Models for Colombian Herbal Teas Classification

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    This paper describes different E-Senses systems, such as Electronic Nose, Electronic Tongue, and Electronic Eyes, which were used to build several machine learning models and assess their performance in classifying a variety of Colombian herbal tea brands such as Albahaca, Frutos Verdes, Jaibel, Toronjil, and Toute. To do this, a set of Colombian herbal tea samples were previously acquired from the instruments and processed through multivariate data analysis techniques (principal component analysis and linear discriminant analysis) to feed the support vector machine, K-nearest neighbors, decision trees, naive Bayes, and random forests algorithms. The results of the E-Senses were validated using HS-SPME-GC-MS analysis. The best machine learning models from the different classification methods reached a 100% success rate in classifying the samples. The proposal of this study was to enhance the classification of Colombian herbal teas using three sensory perception systems. This was achieved by consolidating the data obtained from the collected samples

    EUROSENSORS XVII : book of abstracts

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    Fundação Calouste Gulbenkien (FCG).Fundação para a Ciência e a Tecnologia (FCT)

    12th International Conference on Vibrations in Rotating Machinery

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    Since 1976, the Vibrations in Rotating Machinery conferences have successfully brought industry and academia together to advance state-of-the-art research in dynamics of rotating machinery. 12th International Conference on Vibrations in Rotating Machinery contains contributions presented at the 12th edition of the conference, from industrial and academic experts from different countries. The book discusses the challenges in rotor-dynamics, rub, whirl, instability and more. The topics addressed include: - Active, smart vibration control - Rotor balancing, dynamics, and smart rotors - Bearings and seals - Noise vibration and harshness - Active and passive damping - Applications: wind turbines, steam turbines, gas turbines, compressors - Joints and couplings - Challenging performance boundaries of rotating machines - High power density machines - Electrical machines for aerospace - Management of extreme events - Active machines - Electric supercharging - Blades and bladed assemblies (forced response, flutter, mistuning) - Fault detection and condition monitoring - Rub, whirl and instability - Torsional vibration Providing the latest research and useful guidance, 12th International Conference on Vibrations in Rotating Machinery aims at those from industry or academia that are involved in transport, power, process, medical engineering, manufacturing or construction

    12th International Conference on Vibrations in Rotating Machinery

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    Since 1976, the Vibrations in Rotating Machinery conferences have successfully brought industry and academia together to advance state-of-the-art research in dynamics of rotating machinery. 12th International Conference on Vibrations in Rotating Machinery contains contributions presented at the 12th edition of the conference, from industrial and academic experts from different countries. The book discusses the challenges in rotor-dynamics, rub, whirl, instability and more. The topics addressed include: - Active, smart vibration control - Rotor balancing, dynamics, and smart rotors - Bearings and seals - Noise vibration and harshness - Active and passive damping - Applications: wind turbines, steam turbines, gas turbines, compressors - Joints and couplings - Challenging performance boundaries of rotating machines - High power density machines - Electrical machines for aerospace - Management of extreme events - Active machines - Electric supercharging - Blades and bladed assemblies (forced response, flutter, mistuning) - Fault detection and condition monitoring - Rub, whirl and instability - Torsional vibration Providing the latest research and useful guidance, 12th International Conference on Vibrations in Rotating Machinery aims at those from industry or academia that are involved in transport, power, process, medical engineering, manufacturing or construction

    Abstracts on Radio Direction Finding (1899 - 1995)

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    The files on this record represent the various databases that originally composed the CD-ROM issue of "Abstracts on Radio Direction Finding" database, which is now part of the Dudley Knox Library's Abstracts and Selected Full Text Documents on Radio Direction Finding (1899 - 1995) Collection. (See Calhoun record https://calhoun.nps.edu/handle/10945/57364 for further information on this collection and the bibliography). Due to issues of technological obsolescence preventing current and future audiences from accessing the bibliography, DKL exported and converted into the three files on this record the various databases contained in the CD-ROM. The contents of these files are: 1) RDFA_CompleteBibliography_xls.zip [RDFA_CompleteBibliography.xls: Metadata for the complete bibliography, in Excel 97-2003 Workbook format; RDFA_Glossary.xls: Glossary of terms, in Excel 97-2003 Workbookformat; RDFA_Biographies.xls: Biographies of leading figures, in Excel 97-2003 Workbook format]; 2) RDFA_CompleteBibliography_csv.zip [RDFA_CompleteBibliography.TXT: Metadata for the complete bibliography, in CSV format; RDFA_Glossary.TXT: Glossary of terms, in CSV format; RDFA_Biographies.TXT: Biographies of leading figures, in CSV format]; 3) RDFA_CompleteBibliography.pdf: A human readable display of the bibliographic data, as a means of double-checking any possible deviations due to conversion
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