992 research outputs found

    Anomaly of the geomagnetic Sq variation in Japan: effect from 3-D subterranean structure or the ocean effect?

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    Many years ago Rikitake et al. described the anomalous behaviour of the vertical component Z of the geomagnetic solar quiet (Sq) daily variation field at observatories in central and northern Japan - namely about 2 hr shift of the local noontime peak towards morning hours. They suggested that this anomaly is associated with the anomalous distribution of electrical conductivity in the mantle beneath central Japan. Although a few works have been done to confirm or argue this explanation, no clear answer has been obtained so far. The goal of this work is to understand the nature of this anomaly using our 3-D forward solution. The conductivity model of the Earth includes oceans of laterally variable conductance and conducting mantle either spherically symmetric or 3-D underneath. Data from six Japanese observatories at four seasons for two different years of the solar cycle are analysed. As an inducing ionospheric (Sq) current system, we use those provided by the Comprehensive Model (CM4) of Sabaka et al. Our analysis clearly demonstrates that 3-D induction in the ocean is responsible for the anomalous behaviour of Z daily variations in this region. We also show that the effects from a suite of 3-D mantle models that include mantle wedge and subducting slab are minor compared with the ocean effec

    Overheating of Waspaloy:Effect of cooling rate on flow stress behavior

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    During service of a gas turbine engine, components may suffer instant overheating which is a concern to safe operations. Effect of short overheating on the tensile properties of a Ni-based superalloy Waspaloy has been studied due to its significant importance for practical applications. The results have shown that a combination of near supersolvus overheating at 1000 °C with very rapid cooling at a rate of 50 K/s is most detrimental case to the tensile properties of the material. This is attributed to the absence of γ' and carbide re-precipitation and growth during cooling period. Microstructure change during overheating and cooling has been deduced using in-situ resistivity measurements. This work provides evidence that multilateral measurements including resistivity can shed light on the failure controlling parameters

    Overheating of Waspaloy:Effect of cooling rate on flow stress behavior

    Get PDF
    During service of a gas turbine engine, components may suffer instant overheating which is a concern to safe operations. Effect of short overheating on the tensile properties of a Ni-based superalloy Waspaloy has been studied due to its significant importance for practical applications. The results have shown that a combination of near supersolvus overheating at 1000 °C with very rapid cooling at a rate of 50 K/s is most detrimental case to the tensile properties of the material. This is attributed to the absence of γ' and carbide re-precipitation and growth during cooling period. Microstructure change during overheating and cooling has been deduced using in-situ resistivity measurements. This work provides evidence that multilateral measurements including resistivity can shed light on the failure controlling parameters

    Prediction and control of drop formation modes in microfluidic generation of double emulsions by single-step emulsification

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    Hypothesis Predicting formation mode of double emulsion drops in microfluidic emulsification is crucial for controlling the drop size and morphology. Experiments and modelling A three-phase Volume of Fluid-Continuum Surface Force (VOF–CSF) model was developed, validated with analytical solutions, and used to investigate drop formation in different regimes. Experimental investigations were done using a glue-free demountable glass capillary device with a true axisymmetric geometry, capable of readjusting the distance between the two inner capillaries during operation. Findings A non-dimensional parameter (ζ) for prediction of double emulsion formation mode as a function of the capillary numbers of all fluids and device geometry was developed and its critical values were determined using simulation and experimental data. At logζ > 5.7, drops were formed in dripping mode; the widening jetting occurred at 5 < logζ < 5.7; while the narrowing jetting was observed at logζ < 5. The ζ criterion was correlated with the ratio of the break-up length to drop diameter. The transition from widening to narrowing jetting was achieved by increasing the outer fluid flow rate at the high capillary number of the inner fluid. The drop size was reduced by reducing the distance between the two inner capillaries and the minimum drop size was achieved when the distance between the capillaries was zero

    <i style="">In-Situ</i> Monitoring of Phase Transition and Microstructure Evolution in Ni-Based Superalloys by Electrical Resistivity:Direct Comparison With Differential Scanning Calorimetry and Application to Case Studies

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    In this study, resistivity measurements are made during continuous heating and cooling on four different Ni-based superalloys of different grain structures and with different phases (i.e., γ′ and carbide). The results are directly compared with differential scanning calorimetry (DSC) profiles to identify the material’s resistivity response. The resistivity measurements have been performed using an electro-thermal mechanical testing (ETMT) system having a capability of heating and cooling a sample at a rate of up to 100 K/s by Joule heating, which is not possible with standard heating methods used in previous in-situ microstructure analysis approaches. By comparing different precipitate variations and thermal histories, γ′ volume fraction and precipitate number density are found to be the most important factors determining the resistivity of the materials. In-situ resistivity measurement was applied to several case studies to show that it can provide microstructural information in complex high temperature experiments.<br/

    <i style="">In-Situ</i> Monitoring of Phase Transition and Microstructure Evolution in Ni-Based Superalloys by Electrical Resistivity:Direct Comparison With Differential Scanning Calorimetry and Application to Case Studies

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    In this study, resistivity measurements are made during continuous heating and cooling on four different Ni-based superalloys of different grain structures and with different phases (i.e., γ′ and carbide). The results are directly compared with differential scanning calorimetry (DSC) profiles to identify the material’s resistivity response. The resistivity measurements have been performed using an electro-thermal mechanical testing (ETMT) system having a capability of heating and cooling a sample at a rate of up to 100 K/s by Joule heating, which is not possible with standard heating methods used in previous in-situ microstructure analysis approaches. By comparing different precipitate variations and thermal histories, γ′ volume fraction and precipitate number density are found to be the most important factors determining the resistivity of the materials. In-situ resistivity measurement was applied to several case studies to show that it can provide microstructural information in complex high temperature experiments.<br/

    Droplet Breakup in Flow Past an Obstacle: A Capillary Instability Due to Permeability Variations

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    In multiphase flow in confined geometries an elementary event concerns the interaction of a droplet with an obstacle. As a model of this configuration we study the collision of a droplet with a circular post that spans a significant fraction of the cross-section of a microfluidic channel. We demonstrate that there exist conditions for which a drop moves completely around the obstacle without breaking, while for the same geometry but higher speeds the drop breaks. Therefore, we identify a critical value of the capillary number above which a drop will break. We explain the results with a one-dimensional model characterizing the flow in the narrow gaps on either side of the obstacle, which identifies a surface-tension–driven instability associated with a variation in the permeability in the flow direction. The model captures the major features of the experimental observations.Harvard University (MRSEC (DMR-0820484))Schlumberger-Doll Research Cente

    A Comparative Study of High Temperature Tensile and Creep Testing Between Standard and Miniature Specimens:Applicability and Limits

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    This study concerns the quasi-static and time-dependent mechanical behavior obtained via the miniaturized electro-thermal mechanical testing (ETMT) approach for single crystal (SX) and conventional cast Mar-M-247 superalloy. The experimental outcome was benchmarked against standardized testing procedures. It is found that tensile yielding behavior can be captured accurately by the ETMT approach up to 1100 ºC, provided the appropriate type of thermocouple (T/C) is chosen. Furthermore, creep rupture behavior is underestimated by the miniaturized set-up. High repeatability of the rupture time was obtained for the SX case, whereas a significant scatter was observed for the conventional cast case. The discrepancies are assessed in detail; discussion centers around analytical and practical considerations, such as temperature uncertainty due to parasitic voltage and the choice of T/C, microstructural change as a result of the Joule heating, representative gauge volume, and strain rate non-linearity. Consequently, the applicability and limits of the miniaturized approach are examined critically, and improvements were suggested where appropriate

    Alloy Design for Additive Manufacturing:Early-Stage Oxidation of Nickel-Based Superalloys

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    This body of work aims to inform alloy design for additive manufacturing by investigating the early-stage oxidation behavior of Ni-based superalloys processed by laser-powder bed fusion. The oxidation of 14 Ni-based superalloys—some novel and some heritage—at 1000 °C for 24 hours is studied through thermo-gravimetric analysis. The mass gain, oxide layer thickness, oxide scale composition, and depletion γ' zone size are measured. The influence of the alloy composition on these variables is assessed in order to elucidate how increasingly processable and oxidation resistant alloys can be developed. The alloy compositions with Al content greater than 9 at. pct form continuous Al2O3 scales at 1000 °C and display markedly lower parabolic rate constants, mass gain, oxide layer thickness, and γ' depletion zone size. The alloys of lesser Al content have reduced oxidation resistance and formed oxide scales of predominantly Cr2O3. Alloys with Ti content of 2.7 at. pct and greater formed Ti-rich oxide phases in their oxide scales as well as TiN subscale. A trade-off between alloy processability and oxidation resistance is identified, dictated by the deleterious effect of Al content on the ductility dip and the benefit of Al for oxidation resistance. A property space along the pareto front is highlighted which is ideal for having oxidation resistance and processability
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