20 research outputs found
Thin-layer chromatography of inorganic ions. V. A study of the acetone-sulphuric acid eluent system
No full textExchange Current Densities for Fe(II)-Fe(III) Solutions in Sulfuric Acid and Perchloric Acid
No full textIron Oxidation and Precipitation of Ferric Hydroxysulfates by Resting Thiobacillus ferrooxidans
No full textDesign and synthesis of florylpicoxamid, a fungicide derived from renewable raw materials
No full textN′N′N pincer and N′N bidentate(pyrazolylpyridyl) Rh(I) complexes as catalyst precursors for hydroformylation of olefins
No full textNMR Chemical Shifts of Trace Impurities: Industrially Preferred Solvents Used in Process and Green Chemistry
No full textThe <sup>1</sup>H and <sup>13</sup>C NMR chemical shifts of 48
industrially preferred solvents in six commonly used deuterated NMR
solvents (CDCl<sub>3</sub>, acetone-<i>d</i><sub>6</sub>, DMSO-<i>d</i><sub>6</sub>, acetonitrile-<i>d</i><sub>3</sub>, methanol-<i>d</i><sub>4</sub>, and D<sub>2</sub>O) are reported. This work supplements the compilation of
NMR data published by Gottlieb, Kotlyar, and Nudelman (J. Org. Chem. 1997, 62, 7512) by providing
spectral parameters for solvents that were not commonly utilized at
the time of their original report. Data are specifically included
for solvents, such as 2-Me-THF, <i>n</i>-heptane, and <i>iso</i>-propyl acetate, which are being used more frequently
as the chemical industry aims to adopt greener, safer, and more sustainable
solvents. These spectral tables simplify the identification of these
solvents as impurities in NMR spectra following their use in synthesis
and workup protocols
