Layer-by-layer laser synthesis of Cu–Al–Ni intermetallic compounds and shape memory effect

Published ArticleWe have studied conditions for the synthesis of intermetallic phases in the Cu–Al–Ni system by selective laser sintering/melting, in particular by heating a powder mixture to 300°C. The effects of laser synthesis and heating on the microstructure of the intermetallic phases in the samples obtained have been studied using electron microscopy, optical metallography, and X-ray diffraction analysis. The results demonstrate high sinterability of stoichiometric mixtures. Resistivity measurements indicate that the samples exhibit a shape memory effect. We discuss the feasibility of producing biomicroelectromechanical systems using layerby- layer synthesis

Application of the optical fiber to generation and measurement of low phase noise microwaves

International audienceThe optical delay line proved to be a method to measure the phase noise of microwave oscillators with high sensitivity. The delay, inherently, turns frequency fluctuations into phase fluctuations. Hence, a mixer is used to compare the phase of the oscillator signal to a delayed copy, from which we measure the oscillator phase noise. This article reports on the progress in this type of instruments in our laboratory. For practical reasons, the delay is implemented with an optical-fiber channel, either at 1.3 or 1.55 µm wavelength, modulated in intensity. The laser Relative Intensity Noise (RIN) turns out to be a critical parameter because it converts the RIN into near DC noise through the mixer offset sensitivity to power. The best semiconductor lasers we can find show a RIN of about -155 dB/Hz. Additionally, in our experience the simple microwave photodiodes are to be preferred to the photodiodes with integrated transconductance amplifier because of the lower noise. This seems to be a technical issue, rather than a general property. Thus, we used a separate amplifier, based on SiGe technology for lowest flicker. The optical fiber is temperature stabilized by an Aluminum mass and a sub-milliKelvin electronic control. Other components, like the Mach Zehnder intensity modulator, seem to be less critical for noise. A single channel version was realized and tested with a microwave synthesizer and with a sapphire whispering gallery oscillator at 10 GHz carrier frequency. Using a 2 km delay line (Τ=10 µs) the measured 1/f3 noise is b-3 = -12 dB.rad²/Hz, which matches the a-priori knowledge of the oscillator 1/f3 noise. This means that the instrument sensitivity is higher than this value, thus it is sufficient to measure a room-temperature sapphire oscillator without need of correlation. At higher Fourier frequencies, the instrument background noise is of -145 dBrad²/Hz at 10 kHz off the carrier. Unfortunately, with other source types (eg, a synthesizer) the background noise can be higher because of the effect of am noise. Another test of the noise floor consists of shortening the optical delay to a negligible value. In this way, the oscillator noise is rejected. Unfortunately, this is only a qualitative test because it hides the noise of the optical fiber, due to Rayleigh scattering and other optical phenomena. The background noise is reduced proportionally to 1/√m, where m is the number of averaged spectra, by correlation and averaging on two fully independent channels that measure the same oscillator. Using 2 km optical fibers and averaging on 200 spectra, the background noise is of -110 dBrad²/Hz at 100 Hz off the carrier, and of -160 dBrad²/Hz at 10 kHz. Re-using the parts of the two-channel system, we assemble single-channel system with matched 10 µs optical delays at the two inputs of the mixer, which rejects the noise of the oscillator. The 1/f noise measured in this condition, b-1 = -113 dBrad²/Hz referred to one channel, is the background noise of the system without correlation, which includes amplifiers, detector and optical fiber

Optical mini-disk resonator integrated into a compact optoelectronic oscillator

Original de l'article en libre accès sur le site d'Acta Polonica Physica A http://przyrbwn.icm.edu.pl/APP/SPIS/a116-4.html au lien suivant: http://przyrbwn.icm.edu.pl/APP/PDF/116/a116z465.pdfInternational audienceThis work consists in the design, fabrication and characterization of mini-disk MgF2 resonators for integration into optoelectronic oscillator and first experimental results of implementation in microwave free spectral range oscillator with taper coupling optoelectronic oscillator

On phase noise in optoelectronic oscillator

International audienceThe optoelectronic microwave oscillator has large potential of application in telecommunication, space, radar systems due to its low phase noise level and high tunability. It usually consists of a pump laser, optical intensity modulator, optical delay line, photodetector, mode selection filter, and amplifier. We consider phase noise properties of different architectures of optoelectronic microwave oscillator. Influences of different components constituting the oscillator on its phase noise are shown. Results of phase noise estimation with using phase diffusion approach and results of measurements are presented

Copper(II), iron(III), and chromium(III) complexes with 5,10-dioxo-4,5,9,10-tetrahydro-4,9-diazapyrene derivatives

Six copper(II), iron(III), and chromium(III) complexes with 5,10-dioxo-4,5,9,10-tetrahydro-4,9-diazapyrene derivatives (H2L 1-H2L3) have been synthesized and studied by physical methods (IR and electronic absorption spectroscopy, quantum-chemical calculations). The composition of the complexes has been determined and their stability constants in aqueous dimethylformamide solutions have been calculated. The energy characteristics, electronic structure and geometry of isolated diazapyrenes and their tautomeric forms have been calculated by the PM6 method, and their complexes have been modeled. © Pleiades Publishing, Ltd., 2010

Copper(II), iron(III), and chromium(III) complexes with 5,10-dioxo-4,5,9,10-tetrahydro-4,9-diazapyrene derivatives

Six copper(II), iron(III), and chromium(III) complexes with 5,10-dioxo-4,5,9,10-tetrahydro-4,9-diazapyrene derivatives (H2L 1-H2L3) have been synthesized and studied by physical methods (IR and electronic absorption spectroscopy, quantum-chemical calculations). The composition of the complexes has been determined and their stability constants in aqueous dimethylformamide solutions have been calculated. The energy characteristics, electronic structure and geometry of isolated diazapyrenes and their tautomeric forms have been calculated by the PM6 method, and their complexes have been modeled. © Pleiades Publishing, Ltd., 2010

The LHCb Silicon Tracker Performance Studies

LHCb is one of the experiments for the Large Hadron Collider at CERN and is dedicated to B-physics and CP-violation measurements. To exploit its physics potential good tracking performance with high efficiency in a high particle density environment close to the beam pipe is required. Silicon strip detectors with large read-out pitch and long strips will be used for the LHCb Inner Tracker behind the magnet and the Trigger Tracker station in front of the magnet. We report here about the design of the Silicon Tracker, test beam results and the electrical tests foreseen during productio