Luminescence Dating of Fluvial Deposits from the Weser Valley, Germany

Luminescence dating was applied on coarse-grained monomineralic potassium-rich feld-spar and polymineralic fine-grained minerals of five samples derived from fluvial deposits of the Riv-er Weser in northwestern Germany. We used a pulsed infrared stimulated luminescence (IRSL) single aliquot regenerative (SAR) dose protocol with an IR stimulation at 50°C for 400 s (50 μs on-time and 200 μs off-time). In order to obtain a stable luminescence signal, only off-time IRSL signal was rec-orded. Performance tests gave solid results. Anomalous fading was intended to be reduced by using the pulsed IRSL signal measured at 50°C (IR50), but fading correction was in most cases necessary due to moderate fading rates. Fading uncorrected and corrected pulsed IR50 ages revealed two major fluvial aggradation phases during the Late Pleistocene, namely during marine isotope stage (MIS) 5d (100 ± 5 ka) and from late MIS 5b to MIS 4 (77 ± 6 ka to 68 ± 5 ka). The obtained luminescence ages are consistent with previous 230Th/U dating results from underlying interglacial deposits of the same pit, which are correlated with MIS 7c to early MIS 6

Post-IR IRSL dating of K-feldspar from last interglacial marine terrace deposits on the Kamikita coastal plain, northeastern Japan

To establish a suitable luminescence dating protocol for marine terrace deposits in Japan, we tested the applicability of K-feldspar post-infrared (IR) infrared stimulated luminescence (IRSL) (pIRIR) dating using a marine isotope stage (MIS) 5e terrace deposit from the Kamikita coastal plain (NE Japan), where independent age control from a tephra is available. One of the most commonly used pIRIR signals, measured at 290°C with the first IR stimulation temperature at 50°C (pIRIR50/290), faded with a mean g2days value of 1.94 ± 0.19%/decade. In contrast, the pIRIR signal with a higher first IR stimulation temperature of 200°C (pIRIR200/290) had a much lower fading rate (g2days = 0.16 ± 0.49%/decade). The average fading-uncorrected and -corrected pIRIR200/290 ages of MIS 5e subtidal sediments obtained from two sampling sites were 126 ± 3 ka and 132 ± 2 ka, which is in good agreement with the independent age control. We conclude that is it is now possible to use pIRIR protocol to estimate the ages of not only marine terraces formed during MIS 5 substages (5a, 5c) but also of older marine terraces, for which age evidence is limited

Erratum: Post-IR IRSL dating of K-feldspar from last interglacial marine terrace deposits on the kamikita coastal plain, northeastern Japan

[no abstract available

Luminescence Dating of Fluvial Deposits from the Weser Valley, Germany

Luminescence dating was applied on coarse-grained monomineralic potassium-rich feld-spar and polymineralic fine-grained minerals of five samples derived from fluvial deposits of the Riv-er Weser in northwestern Germany. We used a pulsed infrared stimulated luminescence (IRSL) single aliquot regenerative (SAR) dose protocol with an IR stimulation at 50°C for 400 s (50 μs on-time and 200 μs off-time). In order to obtain a stable luminescence signal, only off-time IRSL signal was rec-orded. Performance tests gave solid results. Anomalous fading was intended to be reduced by using the pulsed IRSL signal measured at 50°C (IR50), but fading correction was in most cases necessary due to moderate fading rates. Fading uncorrected and corrected pulsed IR50 ages revealed two major fluvial aggradation phases during the Late Pleistocene, namely during marine isotope stage (MIS) 5d (100 ± 5 ka) and from late MIS 5b to MIS 4 (77 ± 6 ka to 68 ± 5 ka). The obtained luminescence ages are consistent with previous 230Th/U dating results from underlying interglacial deposits of the same pit, which are correlated with MIS 7c to early MIS 6

Quartz OSL and K-feldspar post-IR IRSL dating of sand accumulation in the Lower Liao Plain (Liaoning, NE China)

The timing of the formation of extensively distributed sand dunes in the Bohai coastal area and its forcing factors are poorly understood. In this study, the chronology of a well-preserved sand dune located in Panjin Forest Park (PJ) in the Lower Liao Plain (LLP) is investigated using quartz optically stimulated luminescence (OSL) and K-feldspar postinfrared (IR) infrared stimulated luminescence (IRSL) (pIRIR) dating. For the pIRIR measurements, the combination of preheating at 180°C and pIRIR stimulation at 150°C (pIRIR150) is exploited. The quartz results show that the sand dune accumulated from c. 120 a (1890 AD) to c. 70 a (1940 AD) before present, and the underlying sandy soil sediments deposited from c. 5.0 ka to c. 0.13 ka as marsh sediment after the sea level highstand since the mid-Holocene. From the evidence in historical coastline records, the PJ sand dune is an inland sand dune and not a coastal sand dune. Based on further information of climate and temperature change after the Little Ice Age (LIA) and human activity in northeastern China, we conclude that the PJ sand dune accumulation was very likely impacted by the immigrants and land reclamation at the end of Qing dynasty. The fading corrected IR50 ages, the apparent and fading corrected pIRIR150 ages are consistent with quartz ages for two sandy soil samples but overestimate those for six sand samples. The overestimation of the feldspar ages is derived from the residual signal which has not been bleached before burial. The offset obtained from the difference between the quartz OSL and the feldspar pIRIR150 ages are ~20-160 a (predicted residual dose: ~0.08-0.60 Gy), whereas the measured residual dose after bleaching 4 h in a solar simulator yielded age overestimation of ~10-40 a (~0.05-0.16 Gy). The age discrepancy calculated from the predicted residual was larger than those obtained from the laboratory measured residuals. We conclude that the pIRIR150 of aeolian sediment is applicable for samples older than ~1000 years where the effect of the residual dose become negligible. © 2016 Y. Li et al

Quaternary Seismic Slip in the Eastern Alps: Dating Fault Gouges from the Periadriatic Fault System Using Trapped Charge Dating Methods

The Periadriatic Fault System (PAF) is among the largest post-collisional structures of the Alps. Recent studies using GPS velocities suggest that Adria-Europe convergence is still being accommodated in the Eastern Alps. However, according to instrumental and historical seismicity records, earthquake activity is mostly concentrated along structures in the adjacent Southern Alps and adjacent Dinarides. Apart from ambiguous historical events, the PAF has little to no earthquake record. Electron spin resonance (ESR) and Optically Stimulated Luminescence (OSL) are dating methods that can be applied as ultra-low temperature thermochronometers (closing temperature below 100 °C), with a Quaternary dating range of a few decades up to ~2 Ma. Both are potentially applicable to date shear heating during earthquakes in slowly deforming fault zones. Since the saturation dose of the quartz ESR signals is larger than that of quartz and feldspar OSL, ESR enables establishing a maximum age of the events (assuming the resetting during seismic events was at least partial), while OSL allows finding their minimum age when the signal is in saturation. We analyzed fault gouge samples from 4 localities along the easternmost segment of the PAF (east of the Giudicarie Fault), and 5 localities along the southernmost segment of the Lavanttal Fault. For ESR, we measured the signals from the Al center in quartz, comparing the results from the single aliquot additive dose (SAAD) and single aliquot regenerative dose (SAR) protocols. Different grain size fractions were measured (SAR protocol) to establish a grain-size age plateau. For OSL, we measured the Infrared Stimulated Luminescence (IRSL) signal at 50 °C (IR50) and the post-IR IRSL signal at 225 °C (pIRIR225) on potassium feldspar. Additionally, experiments of thermal activation of the OSL signal in quartz were performed to observe the shear heating effect in different grain size fractions. For the PAF, the OSL shear heating sensitivity experiments show that quartz has been thermally activated to temperatures below 300 °C, corroborating that shear heating was sufficient for at least a partial system reset. The ESR grain size plateaus suggest that the most effectively reset fraction is 100-150 µm. In general, our dating results indicate that the studied segment of the PAF system accommodated seismotectonic deformation within a maximum age ranging from 1075 ± 48 to 349 ± 17 ka (ESR SAR) and a minimum age in the range of 196 ± 12 to 281 ± 16 ka (pIRIR225). The obtained ages and the current configuration of the structure suggest that the studied segment of the PAF could be considered a potentially active fault at least. In the case of the Lavanttal fault, the ESR dose-response curves were either close to or in saturation, allowing to obtain only minimum ages of ca. 4 Ma for the last total reset of the system. This could be the result of insufficient shear heating by low magnitude earthquakes, or the fault has not seen significant activity since then. Altogether, our results show that large structures in the Eastern Alps such as the PAF have accommodated part of the Adria-Europe convergence during the Quaternary and can potentially host earthquakes in the future

K-feldspar pIRIR150 dating of the Late Pleistocene sediments in the NW Khangai Mountains (Mongolia) using a standardized dose-response curve approach

K-feldspar luminescence dating has been widely applied to constrain the timing of Quaternary sedimentation in different environments. However, the measurements are time-consuming. Meanwhile, anomalous fading and partial bleaching are the two potential problems inducing dating uncertainty. In this study, sand-size K-feldspar grains extracted from 32 luminescence samples from the northern slope of the Khangai Mountains, Mongolia, were dated using the post-infrared (IR) infrared stimulated luminescence protocol (pIRIR150. subscript shows the second stimulation temperature). The standardized dose-response curves (sDRCs) for luminescence dating, which could improve the measurement efficiency, were constructed. The K-feldspar luminescence chronology has been established after careful investigations of fading correction and bleaching degree of the signals. The sDRCs and individual DRC yield consistent ages, indicating that sDRCs are applicable for luminescence dating with an improvement in measurement efficiency. The fading corrected ages using the two fading correction models are generally in agreement. Based on age comparisons between the radiocarbon dates, the fading corrected pIRIR150 and IR50 ages, the pIRIR150 signal was not fully bleached for several samples. In contrast, some IR50 ages were overestimated due to fading over-correction. The investigated profiles have documented the sedimentary information since the last deglaciation

Esr and radiocarbon dating of gut strings from early plucked instruments

Early European plucked instruments have recently experienced a great revival, but a few aspects remain unknown (e.g., the gauge of gut strings). Here we report, for the first time, that the electron spin resonance (ESR) signal intensity of oxidized iron, Fe(III), from gut strings at g = 2 increases linearly with age within a few hundred years. The signal increase in the remaining old strings on early instruments can be used to judge if they are as old as or younger than the instrument. Obtaining the authenticity information of gut strings contributes to the revival of the old instruments and the music. © 2020 by the authors. Licensee MDPI, Basel, Switzerland

New investigations at Kalambo Falls, Zambia:Luminescence chronology, site formation, and archaeological significance

AbstractFluvial deposits can provide excellent archives of early hominin activity but may be complex to interpret, especially without extensive geochronology. The Stone Age site of Kalambo Falls, northern Zambia, has yielded a rich artefact record from dominantly fluvial deposits, but its significance has been restricted by uncertainties over site formation processes and a limited chronology. Our new investigations in the centre of the Kalambo Basin have used luminescence to provide a chronology and have provided key insights into the geomorphological and sedimentological processes involved in site formation. Excavations reveal a complex assemblage of channel and floodplain deposits. Single grain quartz optically stimulated luminescence (OSL) measurements provide the most accurate age estimates for the youngest sediments, but in older deposits the OSL signal from some grains is saturated. A different luminescence signal from quartz, thermally transferred OSL (TT-OSL), can date these older deposits. OSL and TT-OSL results are combined to provide a chronology for the site. Ages indicate four phases of punctuated deposition by the dominantly laterally migrating and vertically aggrading Kalambo River (∼500–300 ka, ∼300–50 ka, ∼50–30 ka, ∼1.5–0.49 ka), followed by deep incision and renewed lateral migration at a lower topographic level. A conceptual model for site formation provides the basis for improved interpretation of the generation, preservation, and visibility of the Kalambo archaeological record. This model highlights the important role of intrinsic meander dynamics in site formation and does not necessarily require complex interpretations that invoke periodic blocking of the Kalambo River, as has previously been suggested. The oldest luminescence ages place the Mode 2/3 transition between ∼500 and 300 ka, consistent with other African and Asian sites where a similar transition can be found. The study approach adopted here can potentially be applied to other fluvial Stone Age sites throughout Africa and beyond

The Memory of a Fault Gouge: An Example from the Simplon Fault Zone (Central Alps)

Faut gouge forms at the core of the fault as the result of a slip in the upper brittle crust. Therefore, the deformation mechanisms and conditions under which the fault gouge was formed can document the stages of fault movement in the crust. We carried out a microstructural analysis on a fault gouge from a hanging-wall branch fault of the Simplon Fault Zone, a major low-angle normal fault in the European Alps. We use thin-section analysis, together with backscattered electron imaging and X-ray diffractometry (XRD), to show that a multistage history from ductile to brittle deformation within the fault gouge. We argue that this multistage deformation history is the result of continuous exhumation history from high to low temperature, along the Simplon Fault Zone. Because of the predominance of pressure solution and veining, we associated a large part of the deformation in the fault gouge with viscous-frictional behaviour that occurred at the brittle-ductile transition. Phyllosilicates and graphite likely caused fault lubrication that we suggested played a role in localizing slip along this major low-angle normal fault