Advanced materials development under NASA\u27s Hybrid Thermally Efficient Core (HyTEC) project

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Solid particle erosion of environmental barrier coatings and ceramic matrix composites

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The current status of advanced environmentanl barrier coatings for ceramic matrix composites at NASA

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Advancing Development of Environmental Barrier Coatings Resistant to Attack by Molten Calcium-Magnesium-Aluminosilicate (CMAS)

Ceramic matrix composites (CMCs) are a leading material system to replace metal-based parts in the hot-section of air-breathing turbine engines to improve fuel efficiency in aircraft engines. CMCs have higher temperature capabilities and lower density compared with traditional metallic structural materials. However, silicon-based CMCs are susceptible to oxidation in the harsh combustion environment encountered in turbine engines. Consequently, environmental barrier coatings (EBCs) are being developed to protect CMC components to improve durability and extend service life of CMCs. Sand, volcanic ash and other particulate debris, which are generally comprised of calcium-magnesium-aluminosilicate (CMAS) and other trace oxides, are routinely ingested by aircraft engines. At temperatures above 1200C, CMAS particulates melt. Near target operating temperatures (~1500C) of future CMC-based aircraft engines, molten CMAS behaves like a viscous melt that can infiltrate and chemically interact with protective coatings. These interactions can cause premature failure of the EBC system and ultimately the overall CMC engine component. Degradation of candidate EBC materials by molten CMAS will be presented with a focus on recent work, as well as methods of evaluating the complex high-temperature materials interactions, underway at NASA Glenn Research Center

Pre-sleep feeding, sleep quality, and markers of recovery in division I NCAA female soccer players

Pre-sleep nutrition habits in elite female athletes have yet to be evaluated. A retrospective analysis was performed with 14 NCAA Division I female soccer players who wore a WHOOP, Inc. band – a wearable device that quantifies recovery by measuring sleep, activity, and heart rate metrics through actigraphy and photoplethysmography, respectively – 24 h a day for an entire competitive season to measure sleep and recovery. Pre-sleep food consumption data were collected via surveys every 3 days. Average pre-sleep nutritional intake (mean ± sd: kcals 330 ± 284; cho 46.2 ± 40.5 g; pro 7.6 ± 7.3 g; fat 12 ± 10.5 g) was recorded. Macronutrients and kcals were grouped into high and low categories based upon the 50th percentile of the mean to compare the impact of a high versus low pre-sleep intake on sleep and recovery variables. Sleep duration (p = 0.10, 0.69, 0.16, 0.17) and sleep disturbances (p = 0.42, 0.65, 0.81, 0.81) were not affected by high versus low kcal, PRO, fat, CHO intake, respectively. Recovery (p = 0.81, 0.06, 0.81, 0.92), RHR (p = 0.84, 0.64, 0.26, 0.66), or HRV (p = 0.84, 0.70, 0.76, 0.93) were also not affected by high versus low kcal, PRO, fat, or CHO consumption, respectively. Consuming a small meal before bed may have no impact on sleep or recovery

Thermomechanical Characterization of SiC/SiC Ceramic Matrix Composites in a Combustion Facility

A combustion facility which includes uniaxial mechanical loading was implemented that enables environmental conditions more akin to jet engine environments compared to conventional static environment tests. Two types of woven SiC/SiC ceramic matrix composites (CMCs), melt-infiltrated (MI) and chemical vapor infiltrated (CVI), were subjected to fatigue loading in the combustion facility and under isothermal furnace conditions. Some CVI test coupons were coated with a multilayer environmental barrier coating (EBC) of mullite + ytterbium monosilicate using slurry infiltration process to demonstrate the performance with a coating. Combustion conditions were applied using a high velocity oxy fuel gun on the front side of the specimen and mechanical loading was applied using a horizontal hydraulic MTS machine. All the specimens considered were subjected to tension-tension fatigue loading at 100 MPa, stress ratio of 0.1 and specimen front-side surface temperature of 1200 ± 20 °C. Nondestructive evaluation (NDE) methods, such as electrical resistance (ER), was used as an in-situ health monitoring technique. Similar fatigue tests were performed in an isothermal furnace for comparison. A much lower fatigue life was observed for the uncoated specimens tested under combustion conditions in comparison to isothermal furnace condition. This difference in fatigue life was attributed to damage associated with added thermal stress due to the thermal gradient and higher rate of oxidative embrittlement due to the presence of high velocity combustion gases in the combustion environment. EBC coating increased the fatigue life in combustion environment. However, EBC coated specimens experienced spallation in the high-velocity flame due to the presence of micro cracks in the coating surface. Fracture surfaces of the failed specimens were investigated under the scanning electron microscope (SEM) to determine the extent of oxidation and damage

Pre-sleep feeding, sleep quality, and markers of recovery in division I NCAA female soccer players

Pre-sleep nutrition habits in elite female athletes have yet to be evaluated. A retrospective analysis was performed with 14 NCAA Division I female soccer players who wore a WHOOP, Inc. band – a wearable device that quantifies recovery by measuring sleep, activity, and heart rate metrics through actigraphy and photoplethysmography, respectively – 24 h a day for an entire competitive season to measure sleep and recovery. Pre-sleep food consumption data were collected via surveys every 3 days. Average pre-sleep nutritional intake (mean ± sd: kcals 330 ± 284; cho 46.2 ± 40.5 g; pro 7.6 ± 7.3 g; fat 12 ± 10.5 g) was recorded. Macronutrients and kcals were grouped into high and low categories based upon the 50th percentile of the mean to compare the impact of a high versus low pre-sleep intake on sleep and recovery variables. Sleep duration (p = 0.10, 0.69, 0.16, 0.17) and sleep disturbances (p = 0.42, 0.65, 0.81, 0.81) were not affected by high versus low kcal, PRO, fat, CHO intake, respectively. Recovery (p = 0.81, 0.06, 0.81, 0.92), RHR (p = 0.84, 0.64, 0.26, 0.66), or HRV (p = 0.84, 0.70, 0.76, 0.93) were also not affected by high versus low kcal, PRO, fat, or CHO consumption, respectively. Consuming a small meal before bed may have no impact on sleep or recovery