Size characterization of airborne SiO2 nanoparticles with on-line and off-line measurement techniques: Results of an interlaboratory comparison

Day after day, new applications using manufactured nanoparticles appear in industry. To evaluate the occupational risk associated with airborne nanoparticles, it is important to have reliable, accurate, and standardized measurement methods. It is therefore necessary to work on pre- standardization projects to develop reference methods to characterize different parameters such as the number and the size distribution of airborne nanoparticles

Size characterization of airborne SiO2 nanoparticles with on-line and off-line measurement techniques: an interlaboratory comparison study

Results of an interlaboratory comparison on size characterization of SiO2 airborne nanoparticles using on-line and off-line measurement techniques are discussed. This study was performed in the framework of Technical Working Area (TWA) 34\u2014\u2018\u2018Properties of Nanoparticle Populations\u2019\u2019 of the Versailles Project on Advanced Materials and Standards (VAMAS) in the project no. 3 \u2018\u2018Techniques for characterizing size distribution of airborne nanoparticles\u2019\u2019. Two types of nano-aerosols, consisting of (1) one population of nanoparticles with a mean diameter between 30.3 and 39.0 nm and (2) two populations of non-agglomerated nanoparticles with mean diameters between, respectively, 36.2\u201346.6 nm and 80.2\u201389.8 nm, were generated for characterization measurements. Scanning mobility particle size spectrometers (SMPS) were used for on-line measurements of size distributions of the produced nano-aerosols. Transmission electron microscopy, scanning electron microscopy, and atomic force microscopy were used as off-line measurement techniques for nanoparticles characterization. Samples were deposited on appropriate supports such as grids, filters, andmica plates by electrostatic precipitation and a filtration technique using SMPS controlled generation upstream. The results of the main size distribution parameters (mean and mode diameters), obtained from several laboratories, were compared based on metrological approaches including metrological traceability, calibration, and evaluation of the measurement uncertainty. Internationally harmonized measurement procedures for airborne SiO2 nanoparticles characterization are proposed

The VULSACO project, vulnerability of sandy coast to climate change: method, results and lessons.

International audienc

The VULSACO project, vulnerability of sandy coast to climate change: method, results and lessons.

International audienc