线宽展宽L波段掺铒光纤光源特性研究

提出了一种两级级联的掺铒光纤超荧光光纤光源(SFS)的新结构,采用耦合器将一个1 480 nm半导体(LD)泵浦源按照一定的分光比对第二级进行双向泵浦,第一段光纤未泵浦。通过研究两级光纤长度的比例、耦合器的分光比对结构性能的影响,优化结构参数后线宽扩展13 nm,输出效率提高6%,并且该结构的中心波长也具有对泵浦功率不敏感的特性

Green Synthesis of Potassium Diformate

以甲酸和氢氧化钾为原料,不外加任何溶剂一步合成二甲酸钾。通过单因素实验,考察了原料配比、反应温度和反应时间对产品质量与收率的影响。采用正交实验进一步优化了合成工艺,确定了最佳工艺条件:n(HCOOH)/n(KOH)=2.2、反应温度70℃、反应时间30 m in,在该条件下,二甲酸钾产品收率达98%以上。所得产品经红外光谱分析及熔点测定,其结果与文献报道一致。反应过程绿色化,有很好的原子经济性。Potassium diformate was synthesized without solvent,using formic acid and potassium hydroxide as raw materials.The optimal conditions for the reaction were:molar ratio of HCOOH to KOH 2.2∶1,reaction temperature 70 ℃ and reaction time 30 min.Yield of the process was over 98% under the optimal conditions.The infrared spectrum and melting range of the product were in good agreement with those reported in literature.The technology developed in this study could be an environmentally benign synthesis route with efficient atom economy

Effects of nutritional conditions and intermittent aeration on accumulation of PHB in activated sludge

考察了营养条件与间歇曝气方式对好氧培养的活性污泥累积聚-3-羟基丁酸酯(PHB)的影响。结果表明,在营养平衡的条件下PHB的最大累积量占活性污泥(MLSS)质量分数的12.5%;而在只添加碳源的条件下,PHB的最大积累量可提高到MLSS质量分数的19.2%;高碳源浓度有利于活性污泥累积PHB,以4.5g/L的乙酸钠为碳源,PHB的最大累积量达MLSS质量分数的41.7%,PHB的生成速率为265mg/(L.h)。以曝气30min停曝30min为循环的间歇曝气方式能有效提高活性污泥中PHB的累积量。与连续曝气相比,该间歇曝气方式使污泥最大累积PHB量占MLSS的质量分数提高了9%。The effects of nutritional conditions and intermittent aeration of operation cycles on poly-3-hydroxybutyrate (PHB) production by activated sludge were studied.The results showed that,activated sludge from aerobic reactors accumulated PHB was around 12.5% of Mixed Liquor Suspended Solid (MLSS) under eutrophy conditions while it was up to 19.2% of MLSS under only carbon source provided conditions.High carbon source concentration was helpful to PHB accumulation.The maximum PHB content of MLSS reached 41.7% of MLSS when 4.5 g/L of sodium acetate was used as the unique carbon source,with PHB production rate being 265 mg/(L·h).The optimum intermittent aeration pf operational cycle was:30 minutes’ aeration followed by 30 minutes’ intermission.Compared with continuous aeration process,the PHB content of MLSS increased by 9% with the optimized intermittent aeration of operational cycle.国家自然科学基金资助项目(20076037