Modeling, Characterizing and Reconstructing Mesoscale Microstructural Evolution in Particulate Processing and Solid-State Sintering

abstract: In material science, microstructure plays a key role in determining properties, which further determine utility of the material. However, effectively measuring microstructure evolution in real time remains an challenge. To date, a wide range of advanced experimental techniques have been developed and applied to characterize material microstructure and structural evolution on different length and time scales. Most of these methods can only resolve 2D structural features within a narrow range of length scale and for a single or a series of snapshots. The currently available 3D microstructure characterization techniques are usually destructive and require slicing and polishing the samples each time a picture is taken. Simulation methods, on the other hand, are cheap, sample-free and versatile without the special necessity of taking care of the physical limitations, such as extreme temperature or pressure, which are prominent issues for experimental methods. Yet the majority of simulation methods are limited to specific circumstances, for example, first principle computation can only handle several thousands of atoms, molecular dynamics can only efficiently simulate a few seconds of evolution of a system with several millions particles, and finite element method can only be used in continuous medium, etc. Such limitations make these individual methods far from satisfaction to simulate macroscopic processes that a material sample undergoes up to experimental level accuracy. Therefore, it is highly desirable to develop a framework that integrate different simulation schemes from various scales to model complicated microstructure evolution and corresponding properties. Guided by such an objective, we have made our efforts towards incorporating a collection of simulation methods, including finite element method (FEM), cellular automata (CA), kinetic Monte Carlo (kMC), stochastic reconstruction method, Discrete Element Method (DEM), etc, to generate an integrated computational material engineering platform (ICMEP), which could enable us to effectively model microstructure evolution and use the simulated microstructure to do subsequent performance analysis. In this thesis, we will introduce some cases of building coupled modeling schemes and present the preliminary results in solid-state sintering. For example, we use coupled DEM and kinetic Monte Carlo method to simulate solid state sintering, and use coupled FEM and cellular automata method to model microstrucutre evolution during selective laser sintering of titanium alloy. Current results indicate that joining models from different length and time scales is fruitful in terms of understanding and describing microstructure evolution of a macroscopic physical process from various perspectives.Dissertation/ThesisDoctoral Dissertation Materials Science and Engineering 201

Simulation of pore-scale flow using finite element-methods

I present a new finite element (FE) simulation method to simulate pore-scale flow. Within the pore-space, I solve a simplified form of the incompressible Navier-Stoke’s equation, yielding the velocity field in a two-step solution approach. First, Poisson’s equation is solved with homogeneous boundary conditions, and then the pore pressure is computed and the velocity field obtained for no slip conditions at the grain boundaries. From the computed velocity field I estimate the effective permeability of porous media samples characterized by thin section micrographs, micro-CT scans and synthetically generated grain packings. This two-step process is much simpler than solving the full Navier Stokes equation and therefore provides the opportunity to study pore geometries with hundreds of thousands of pores in a computationally more cost effective manner than solving the full Navier-Stoke’s equation. My numerical model is verified with an analytical solution and validated on samples whose permeabilities and porosities had been measured in laboratory experiments (Akanji and Matthai, 2010). Comparisons were also made with Stokes solver, published experimental, approximate and exact permeability data. Starting with a numerically constructed synthetic grain packings, I also investigated the extent to which the details of pore micro-structure affect the hydraulic permeability (Garcia et al., 2009). I then estimate the hydraulic anisotropy of unconsolidated granular packings. With the future aim to simulate multiphase flow within the pore-space, I also compute the radii and derive capillary pressure from the Young-Laplace equation (Akanji and Matthai,2010

Organ printing as an information technology

Funding Information: This work has been sponsored by the São Paulo Research Foundation (FAPESP), The Brazilian Institute of Biofabrication (INCT-BIOFABRIS) and National Council for Scientific and Technological Development (CNPq). Publisher Copyright: © 2015 Published by Elsevier Ltd.Organ printing is defined as a layer by layer additive robotic computer-aided biofabrication of functional 3D organ constructs with using self-assembling tissue spheroids according to digital model. Information technology and computer-aided design softwares are instrumental in the transformation of virtual 3D bioimaging information about human tissue and organs into living biological reality during 3D bioprinting. Information technology enables design blueprints for bioprinting of human organs as well as predictive computer simulation both printing and post-printing processes. 3D bioprinting is now considered as an emerging information technology and the effective application of existing information technology tools and development of new technological platforms such as human tissue and organ informatics, design automation, virtual human organs, virtual organ biofabrication line, mathematical modeling and predictive computer simulations of bioprinted tissue fusion and maturation is an important technological imperative for advancing organ bioprinting.publishersversionPeer reviewe

Extraction robuste de primitives géométriques 3D dans un nuage de points et alignement basé sur les primitives

Dans ce projet, nous étudions les problèmes de rétro-ingénierie et de contrôle de la qualité qui jouent un rôle important dans la fabrication industrielle. La rétro-ingénierie tente de reconstruire un modèle 3D à partir de nuages de points, qui s’apparente au problème de la reconstruction de la surface 3D. Le contrôle de la qualité est un processus dans lequel la qualité de tous les facteurs impliqués dans la production est abordée. En fait, les systèmes ci-dessus nécessitent beaucoup d’intervention de la part d’un utilisateur expérimenté, résultat souhaité est encore loin soit une automatisation complète du processus. Par conséquent, de nombreux défis doivent encore être abordés pour atteindre ce résultat hautement souhaitable en production automatisée. La première question abordée dans la thèse consiste à extraire les primitives géométriques 3D à partir de nuages de points. Un cadre complet pour extraire plusieurs types de primitives à partir de données 3D est proposé. En particulier, une nouvelle méthode de validation est proposée pour évaluer la qualité des primitives extraites. À la fin, toutes les primitives présentes dans le nuage de points sont extraites avec les points de données associés et leurs paramètres descriptifs. Ces résultats pourraient être utilisés dans diverses applications telles que la reconstruction de scènes on d’édifices, la géométrie constructive et etc. La seconde question traiée dans ce travail porte sur l’alignement de deux ensembles de données 3D à l’aide de primitives géométriques, qui sont considérées comme un nouveau descripteur robuste. L’idée d’utiliser les primitives pour l’alignement arrive à surmonter plusieurs défis rencontrés par les méthodes d’alignement existantes. Ce problème d’alignement est une étape essentielle dans la modélisation 3D, la mise en registre, la récupération de modèles. Enfin, nous proposons également une méthode automatique pour extraire les discontinutés à partir de données 3D d’objets manufacturés. En intégrant ces discontinutés au problème d’alignement, il est possible d’établir automatiquement les correspondances entre primitives en utilisant l’appariement de graphes relationnels avec attributs. Nous avons expérimenté tous les algorithmes proposés sur différents jeux de données synthétiques et réelles. Ces algorithmes ont non seulement réussi à accomplir leur tâches avec succès mais se sont aussi avérés supérieus aux méthodes proposées dans la literature. Les résultats présentés dans le thèse pourraient s’avérér utilises à plusieurs applications.In this research project, we address reverse engineering and quality control problems that play significant roles in industrial manufacturing. Reverse engineering attempts to rebuild a 3D model from the scanned data captured from a object, which is the problem similar to 3D surface reconstruction. Quality control is a process in which the quality of all factors involved in production is monitored and revised. In fact, the above systems currently require significant intervention from experienced users, and are thus still far from being fully automated. Therefore, many challenges still need to be addressed to achieve the desired performance for automated production. The first proposition of this thesis is to extract 3D geometric primitives from point clouds for reverse engineering and surface reconstruction. A complete framework to extract multiple types of primitives from 3D data is proposed. In particular, a novel validation method is also proposed to assess the quality of the extracted primitives. At the end, all primitives present in the point cloud are extracted with their associated data points and descriptive parameters. These results could be used in various applications such as scene and building reconstruction, constructive solid geometry, etc. The second proposition of the thesis is to align two 3D datasets using the extracted geometric primitives, which is introduced as a novel and robust descriptor. The idea of using primitives for alignment is addressed several challenges faced by existing registration methods. This alignment problem is an essential step in 3D modeling, registration and model retrieval. Finally, an automatic method to extract sharp features from 3D data of man-made objects is also proposed. By integrating the extracted sharp features into the alignment framework, it is possible implement automatic assignment of primitive correspondences using attribute relational graph matching. Each primitive is considered as a node of the graph and an attribute relational graph is created to provide a structural and relational description between primitives. We have experimented all the proposed algorithms on different synthetic and real scanned datasets. Our algorithms not only are successful in completing their tasks with good results but also outperform other methods. We believe that the contribution of them could be useful in many applications

Slice and Dice: A Physicalization Workflow for Anatomical Edutainment

During the last decades, anatomy has become an interesting topic in education---even for laymen or schoolchildren. As medical imaging techniques become increasingly sophisticated, virtual anatomical education applications have emerged. Still, anatomical models are often preferred, as they facilitate 3D localization of anatomical structures. Recently, data physicalizations (i.e., physical visualizations) have proven to be effective and engaging---sometimes, even more than their virtual counterparts. So far, medical data physicalizations involve mainly 3D printing, which is still expensive and cumbersome. We investigate alternative forms of physicalizations, which use readily available technologies (home printers) and inexpensive materials (paper or semi-transparent films) to generate crafts for anatomical edutainment. To the best of our knowledge, this is the first computer-generated crafting approach within an anatomical edutainment context. Our approach follows a cost-effective, simple, and easy-to-employ workflow, resulting in assemblable data sculptures (i.e., semi-transparent sliceforms). It primarily supports volumetric data (such as CT or MRI), but mesh data can also be imported. An octree slices the imported volume and an optimization step simplifies the slice configuration, proposing the optimal order for easy assembly. A packing algorithm places the resulting slices with their labels, annotations, and assembly instructions on a paper or transparent film of user-selected size, to be printed, assembled into a sliceform, and explored. We conducted two user studies to assess our approach, demonstrating that it is an initial positive step towards the successful creation of interactive and engaging anatomical physicalizations

Algorithm-aided Information Design: Hybrid Design approach on the edge of associative methodologies in AEC

Dissertação de mestrado em European Master in Building Information ModellingLast three decades have brought colossal progress to design methodologies within the common pursuit toward a seamless fusion between digital and physical worlds and augmenting it with the of computation power and network coverage. For this historically short period, two generations of methodologies and tools have emerged: Additive generation and parametric Associative generation of CAD. Currently, designers worldwide engaged in new forms of design exploration. From this race, two prominent methodologies have developed from Associative Design approach – Object-Oriented Design (OOD) and Algorithm-Aided Design (AAD). The primary research objective is to investigate, examine, and push boundaries between OOD and AAD for new design space determination, where advantages of both design methods are fused to produce a new generation methodology which is called in the present study AID (Algorithm-aided Information Design). The study methodology is structured into two flows. In the first flow, existing CAD methodologies are investigated, and the conceptual framework is extracted based on the state of art analysis, then analysed data is synthesized into the subject proposal. In the second flow, tools and workflows are elaborated and examined on practice to confirm the subject proposal. In compliance, the content of the research consists of two theoretical and practical parts. In the first theoretical part, a literature review is conducted, and assumptions are made to speculate about AID methodology, its tools, possible advantages and drawbacks. Next, case studies are performed according to sequential stages of digital design through the lens of practical AID methodology implementation. Case studies are covering such design aspects as model & documentation generation, design automation, interoperability, manufacturing control, performance analysis and optimization. Ultimately, a set of test projects is developed with the AID methodology applied. After the practical part, research returns to the theory where analytical information is gathered based on the literature review, conceptual framework, and experimental practice reports. In summary, the study synthesizes AID methodology as part of Hybrid Design, which enables creative use of tools and elaborating of agile design systems integrating additive and associative methodologies of Digital Design. In general, the study is based on agile methods and cyclic research development mixed between practice and theory to achieve a comprehensive vision of the subject.Last three decades have brought colossal progress to design methodologies within the common pursuit toward a seamless fusion between digital and physical worlds and augmenting it with the of computation power and network coverage. For this historically short period, two generations of methodologies and tools have emerged: Additive generation and parametric Associative generation of CAD. Currently, designers worldwide engaged in new forms of design exploration. From this race, two prominent methodologies have developed from Associative Design approach – Object-Oriented Design (OOD) and Algorithm-Aided Design (AAD). The primary research objective is to investigate, examine, and push boundaries between OOD and AAD for new design space determination, where advantages of both design methods are fused to produce a new generation methodology which is called in the present study AID (Algorithm-aided Information Design). The study methodology is structured into two flows. In the first flow, existing CAD methodologies are investigated, and the conceptual framework is extracted based on the state of art analysis, then analysed data is synthesized into the subject proposal. In the second flow, tools and workflows are elaborated and examined on practice to confirm the subject proposal. In compliance, the content of the research consists of two theoretical and practical parts. In the first theoretical part, a literature review is conducted, and assumptions are made to speculate about AID methodology, its tools, possible advantages and drawbacks. Next, case studies are performed according to sequential stages of digital design through the lens of practical AID methodology implementation. Case studies are covering such design aspects as model & documentation generation, design automation, interoperability, manufacturing control, performance analysis and optimization. Ultimately, a set of test projects is developed with the AID methodology applied. After the practical part, research returns to the theory where analytical information is gathered based on the literature review, conceptual framework, and experimental practice reports. In summary, the study synthesizes AID methodology as part of Hybrid Design, which enables creative use of tools and elaborating of agile design systems integrating additive and associative methodologies of Digital Design. In general, the study is based on agile methods and cyclic research development mixed between practice and theory to achieve a comprehensive vision of the subject