Initial Study and Verification of a Distributed Fiber Optic Corrosion Monitoring System for Transportation Structures

For this study, a novel optical fiber sensing system was developed and tested for the monitoring of corrosion in transportation systems. The optical fiber sensing system consists of a reference long period fiber gratings (LPFG) sensor for corrosive environmental monitoring and a LPFG sensor coated with a thin film of nano iron and silica particles for steel corrosion monitoring. The environmental effects (such as pH and temperature) are compensated by the use of the reference LPFG sensor. The sensor design, simulation, and experimental validation were performed in this study to investigate the feasibility of the proposed sensing system for corrosion and environment monitoring. The detailed investigations of the proposed sensing system showed that within the detection limitation of the thin coated layer, the proposed sensor could monitor both the initial and stable corrosion rate consistently. Compared to the traditional electrochemical method, the proposed optical fiber sensing system has a converter coefficient of 1 nm/day=3.746×10-3 A/cm2. Therefore, the proposed nano iron/silica particles dispersed polyurethane coated optical fiber sensor can monitor the critical corrosion information of the host members in real time and remotely. With multiple LPFGs in a single fiber, it is possible to provide a costeffective, distributed monitoring solution for corrosion monitoring of large scale transportation structures

A progressive collapse evaluation of steel structures in high temperature environment with optical fiber sensors

In the process of a progressive failure of steel structures in a post-earthquake fire, real-time assessment and prediction of structural behaviors are of paramount significance to an emergency evacuation and rescue effort. However, existing measurement technologies cannot provide the needed critical data such as large strains at high temperature. To bridge this gap, a novel optical fiber sensor network and an adaptive multi-scale finite element model (FEM) are proposed and developed in this study. The sensor network consists of long period fiber gratings (LPFG) sensors and extrinsic Fabry-Perot interferometer (EFPI) sensors or their integration. Each sensor is designed with a three-tier structure for an accurate and reliable measurement of large strains and for ease of installation. To maintain a balance between the total cost of computation and instrumentation and the accuracy in numerical simulation, a structure is divided into representative/critical components instrumented densely and the remaining components simulated computationally. The critical components and the remaining were modeled in different scales with fiber elements and beam/plate elements, respectively, so that the material behavior and load information measured from the critical components are representative to the remaining components and can be used to update the temperature distribution of the structure in real time. Sensitivity studies on the number of sensors and the initial selection of an updating temperature parameter were conducted. Both the sensor network and the FEM were validated with laboratory tests of a single-bay, one-story steel frame under simulated post-earthquake fire conditions. The validated FEM was applied to a two-bay, four-story steel building under the 1995 Kobe earthquake excitations. Based on extensive tests and analyses, the proposed sensor can measure a strain of 12% at as high as 800⁰C (1472⁰F) in temperature. Within the application range, the LPFG wavelength and the EFPI gap change linearly with the applied strain and temperature. The proposed updating criterion and algorithm in the adaptive FEM are proven to be effective. The number of sensors is sufficient in engineering applications as long as the sensors can adequately represent the material behavior of the instrumented components. The predicted structural behavior is unaffected by any change in a low temperature range and thus insensitive to the initial selection of the updating parameter --Abstract, page iii

Review of Fiber Optic Sensors for Structural Fire Engineering

Reliable and accurate measurements of temperature and strain in structures subjected to fire can be difficult to obtain using traditional sensing technologies based on electrical signals. Fiber optic sensors, which are based on light signals, solve many of the problems of monitoring structures in high temperature environments; however, they present their own challenges. This paper, which is intended for structural engineers new to fiber optic sensors, reviews various fiber optic sensors that have been used to make measurements in structure fires, including the sensing principles, fabrication, key characteristics, and recently-reported applications. Three categories of fiber optic sensors are reviewed: Grating-based sensors, interferometer sensors, and distributed sensors

Long period fiber grating, thin coating of graphene and silver nanowires, and corrosion sensing for life-cycle assessment of steel structures

This study aims to develop and validate a compact, integrated lab-on-sensor system for simultaneous measurement of strain, temperature and corrosion-induced mass loss in steel structures and concrete reinforcement elements in order to assess their life-cycle performance. The sensing system operates based on the principle of long period fiber gratings (LPFG) that are responsive to both thermal and mechanical deformation, and the change in refractive index of any medium surrounding the optical fiber. To fabricate a LPFG sensor for strain and temperature measurement, a CO2 laser aided fiber grating system was assembled. To enable mass loss measurement, a low pressure chemical vapor deposition (LPCVD) system was built to synthesize a graphene/silver nanowire composite film as flexible transparent electrode for the electroplating of a thin Fe-C layer on the curve surface of a LPFG sensor. Together with two LPFG sensors in LP06 and LP07 modes for simultaneous strain and temperature measurement, three Fe-C coated LPFG sensors were multiplexed and deployed inside three miniature, coaxial steel tubes to measure critical mass losses through the penetration of tube walls and their corresponding corrosion rates in the life cycle of an instrumented steel component. A Fe-C coated LPFG sensor was submerged in a NaCl solution and calibrated for stress corrosion cracking under three strain levels. The corrosion mechanism of the Fe-C layer was investigated and the distribution of cracks (width, length and spacing) were characterized and correlated with the wavelength change of the sensor. Thermal, loading and accelerated corrosion tests were conducted to validate the functionality, sensitivity, accuracy, and robustness of the proposed sensing system and demonstrate its feasibility in in situ applications --Abstract, page iii

Femtosecond Laser Micromachining of Advanced Fiber Optic Sensors and Devices

Research and development in photonic micro/nano structures functioned as sensors and devices have experienced significant growth in recent years, fueled by their broad applications in the fields of physical, chemical and biological quantities. Compared with conventional sensors with bulky assemblies, recent process in femtosecond (fs) laser three-dimensional (3D) micro- and even nano-scale micromachining technique has been proven an effective and flexible way for one-step fabrication of assembly-free micro devices and structures in various transparent materials, such as fused silica and single crystal sapphire materials. When used for fabrication, fs laser has many unique characteristics, such as negligible cracks, minimal heat-affected-zone, low recast, high precision, and the capability of embedded 3D fabrication, compared with conventional long pulse lasers. The merits of this advanced manufacturing technique enable the unique opportunity to fabricate integrated sensors with improved robustness, enriched functionality, enhanced intelligence, and unprecedented performance. Recently, fiber optic sensors have been widely used for energy, defense, environmental, biomedical and industry sensing applications. In addition to the well-known advantages of miniaturized in size, high sensitivity, simple to fabricate, immunity to electromagnetic interference (EMI) and resistance to corrosion, all-optical fiber sensors are becoming more and more desirable when designed with characteristics of assembly free and operation in the reflection configuration. In particular, all-optical fiber sensor is a good candidate to address the monitoring needs within extreme environment conditions, such as high temperature, high pressure, toxic/corrosive/erosive atmosphere, and large strain/stress. In addition, assembly-free, advanced fiber optic sensors and devices are also needed in optofluidic systems for chemical/biomedical sensing applications and polarization manipulation in optical systems. Different fs laser micromachining techniques were investigated for different purposes, such as fs laser direct ablating, fs laser irradiation with chemical etching (FLICE) and laser induced stresses. A series of high performance assembly-free, all-optical fiber sensor probes operated in a reflection configuration were proposed and fabricated. Meanwhile, several significant sensing measurements (e.g., high temperature, high pressure, refractive index variation, and molecule identification) of the proposed sensors were demonstrated in this dissertation as well. In addition to the probe based fiber optic sensors, stress induced birefringence was also created in the commercial optical fibers using fs laser induced stresses technique, resulting in several advanced polarization dependent devices, including a fiber inline quarter waveplate and a fiber inline polarizer based on the long period fiber grating (LPFG) structure

Photonic Biosensor Assays to Detect and Distinguish Subspecies of Francisella tularensis

The application of photonic biosensor assays to diagnose the category-A select agent Francisella tularensis was investigated. Both interferometric and long period fiber grating sensing structures were successfully demonstrated; both these sensors are capable of detecting the optical changes induced by either immunological binding or DNA hybridization. Detection was made possible by the attachment of DNA probes or immunoglobulins (IgG) directly to the fiber surface via layer-by-layer electrostatic self-assembly. An optical fiber biosensor was tested using a standard transmission mode long period fiber grating of length 15 mm and period 260 μm, and coated with the IgG fraction of antiserum to F. tularensis. The IgG was deposited onto the optical fiber surface in a nanostructured film, and the resulting refractive index change was measured using spectroscopic ellipsometry. The presence of F. tularensis was detected from the decrease of peak wavelength caused by binding of specific antigen. Detection and differentiation of F. tularensis subspecies tularensis (type A strain TI0902) and subspecies holarctica (type B strain LVS) was further accomplished using a single-mode multi-cavity fiber Fabry-Perot interferometric sensor. These sensors were prepared by depositing seven polymer bilayers onto the fiber tip followed by attaching one of two DNA probes: (a) a 101-bp probe from the yhhW gene unique to type-A strains, or (b) a 117-bp probe of the lpnA gene, common to both type-A and type-B strains. The yhhW probe was reactive with the type-A, but not the type-B strain. Probe lpnA was reactive with both type-A and type-B strains. Nanogram quantities of the target DNA could be detected, highlighting the sensitivity of this method for DNA detection without the use of PCR. The DNA probe reacted with 100% homologous target DNA, but did not react with sequences containing 2-bp mismatches, indicating the high specificity of the assay. These assays will fill an important void that exists for rapid, culture-free, and field-compatible diagnosis of F. tularensis

High temperature tolerant optical fiber inline microsensors by laser fabrication

Fiber sensors are particularly attractive for harsh environment defined by high temperature, high pressure, corrosive/erosive, and strong electromagnetic interference, where conventional electronic sensors do not have a chance to survive. However, the key issue has been the robustness of the sensor probe (not the fiber itself) mostly due to the problems stemmed from the traditional assembly based approaches used to construct fiber optic sensors. For example, at high temperatures (e.g., above 500°C), the thermal expansion coefficient mismatch between different composited parts has a high chance to lead to sensors\u27 malfunction by breaking the sensor as a result of the excessive thermo-stress building up inside the multi-component sensor structure. To survive the high temperature harsh environment, it is thus highly desired that the sensor probes are made assembly-free. We are proposing to fabricate assembly-free fiber sensor probes by manufacturing various microstructures directly on optical fibers. This dissertation aims to design, develop and demonstrate robust, miniaturized fiber sensor probes for harsh environment applications through assembly-free, laser fabrication. Working towards this objective, the dissertation explored three types of fiber inline microsensors fabricated by two types of laser systems. Using a CO₂ laser, long period fiber grating (LPFG) and core-cladding mode interferometer sensors were fabricated. Using a femto-second laser, an extrinsic Fabry-Perot interferometric (EFPI) sensor with an open cavity was fabricated. The scope of the dissertation work consists of device design, device modeling/simulation, laser fabrication system setups, signal processing method development and sensor performance evaluation and demonstration. This research work provides theoretical and experimental evidences that laser fabrication technique is a valid tool to fabricate previously undoable miniaturized photonic sensor structures, which can avoid complicated assembly processes and, as a result, enhance robustness, functionality and survivability of the sensor for applications in harsh environments. In addition, a number of novel optical fiber sensor platforms are proposed, studied and demonstrated for sensing and monitoring of various physical and chemical parameters in high temperature harsh environments --Abstract, page iii

Long-period fiber grating corrosion sensors for life-cycle monitoring and assessment of reinforced concrete structures

This study aims to: (1) explore, develop, calibrate and validate Fe-C coated, long period fiber grating (LPFG) sensors for short-term mass loss measurement of the Fe-C coating; (2) develop, calibrate, and validate steel tube-encapsulated, fiber optic probes and LPFG sensors for long-term mass loss detection of the steel tube; (3) correlate the corrosion process of packaging metal materials with that of steel bars in direct contact with the packaged probe or sensor except for a thin insulation tape; and (4) apply both types of corrosion sensors into reinforced concrete (RC) structures for reinforcing bar corrosion monitoring and structural condition assessment. For short-term monitoring, the corrosion mechanism of the Fe-C coating and the corrosion sensitivity of the Fe-C coated LPFG were investigated and characterized in 3.5 wt. % NaCl solution. For long-term detection, the probe or sensor was used to measure the pitting corrosion growth of steel tubes in simulated concrete pore solution. To validate them in an application setting, two types of LPFG corrosion sensors were embedded in three RC beams under accelerated corrosion test. The resonant wavelength of a Fe-C coated LPFG sensor can be linearly related to the mass loss of Fe-C coating up to 60~90%. When tested in 3.5wt. % NaCl solution, the LPFG sensor coated with an 8~20 μm thick Fe-C layer has a sensitivity of 0.15~0.23 nm/1% Fe-C mass loss. This sensitivity is translated into approximately 1300 nm/g in mass loss of reinforcing steel bars. In RC beam applications, the resonant wavelength of an Fe-C coated LPFG sensor is reduced by 0.49 nm/hour when installed along a steel bar under accelerated corrosion conditions and 0.95 nm/day when installed near the bottom surface of a beam under natural corrosion condition. The corrosion penetration rate through the wall of a steel tube is approximately 8.6 μm/day --Abstract, page iii